2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
- Product Name
- 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
- CAS No.
- 82632-80-2
- Chemical Name
- 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
- Synonyms
- 2,3,6,7,10,11-HEXABROMOTRIPHENYLENE;Triphenylene, 2,3,6,7,10,11-hexabromo-;2,3,6,7,10,11-Hexabromotriphenylene>2,3,6,7,10,11-Hexabromobenzophenanthrene;2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
- CBNumber
- CB4505826
- Molecular Formula
- C18H6Br6
- Formula Weight
- 701.66
- MOL File
- 82632-80-2.mol
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Property
- Boiling point:
- 689.8±50.0 °C(Predicted)
- Density
- 2.428±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Water Solubility
- Insoluble in water
- form
- powder to crystal
- color
- White to Light yellow to Light red
- InChI
- InChI=1S/C18H6Br6/c19-13-1-7-8(2-14(13)20)10-4-17(23)18(24)6-12(10)11-5-16(22)15(21)3-9(7)11/h1-6H
- InChIKey
- GLHQUXLCQLQNPZ-UHFFFAOYSA-N
- SMILES
- C1=C2C(C3C(C4C2=CC(Br)=C(Br)C=4)=CC(Br)=C(Br)C=3)=CC(Br)=C1Br
Safety
- HS Code
- 29039990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- H1201
- Product name
- 2,3,6,7,10,11-Hexabromotriphenylene
- Purity
- >98.0%(T)
- Packaging
- 1g
- Price
- $486
- Updated
- 2025/07/31
- Product number
- H1201
- Product name
- 2,3,6,7,10,11-Hexabromotriphenylene
- Purity
- >98.0%(T)
- Packaging
- 100mg
- Price
- $47
- Updated
- 2025/07/31
- Product number
- H290913
- Product name
- 2,3,6,7,10,11-Hexabromotriphenylene
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 279843
- Product name
- 2,3,6,7,10,11-Hexabromotriphenylene
- Packaging
- 1g
- Price
- $350
- Updated
- 2021/12/16
- Product number
- H290913
- Product name
- 2,3,6,7,10,11-Hexabromotriphenylene
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Chemical Properties,Usage,Production
Synthesis
217-59-4
82632-80-2
Bromine (9.0 mL, 349 mmol) was added dropwise to a solution of 9,10-benzophenanthrene (3.95 g, 17.3 mmol) and iron powder (410 mg, 7.34 mmol) in nitrobenzene (200 mL) under nitrogen protection with stirring at room temperature for 20 min, and the reaction was subsequently heated up to 210°C for 3 hours. After completion of the reaction, the mixture was cooled to room temperature and the product was precipitated by the addition of ether (Et2O). The precipitate was collected by filtration and washed thoroughly with ether, acetone and chloroform (CHCl3) sequentially to afford the white powdery product 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene (11.5 g, 16.4 mmol, 94.8% yield). The melting point of the product was above 300°C; 1H NMR (300 MHz, CDCl3): δ = 8.72 (s, 6H, Ar-H); IR (KBr): νmax = 1585, 1551, 1454, 1365, 1119, 873, 863 cm-1.
References
[1] Journal of the American Chemical Society, 2017, vol. 139, # 48, p. 17229 - 17232
[2] Tetrahedron, 2015, vol. 71, # 29, p. 4714 - 4721
[3] Journal of Materials Chemistry, 2000, vol. 10, # 7, p. 1519 - 1525
[4] Journal of the American Chemical Society, 2017, vol. 139, # 46, p. 16759 - 16767
[5] Inorganic Chemistry, 2014, vol. 53, # 18, p. 9876 - 9896
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Preparation Products And Raw materials
Raw materials
Preparation Products
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene manufacturers
- Product
- 2,3,6,7,10,11-Hexabromotriphenylene 82632-80-2
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-31
- Product
- 2,3,6,7,10,11-HEXABROMOTRIPHENYLENE 82632-80-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2018-08-06