ChemicalBook > CAS DataBase List > 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene

2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene

Product Name
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
CAS No.
82632-80-2
Chemical Name
2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
Synonyms
2,3,6,7,10,11-HEXABROMOTRIPHENYLENE;Triphenylene, 2,3,6,7,10,11-hexabromo-;2,3,6,7,10,11-Hexabromotriphenylene>2,3,6,7,10,11-Hexabromobenzophenanthrene;2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene
CBNumber
CB4505826
Molecular Formula
C18H6Br6
Formula Weight
701.66
MOL File
82632-80-2.mol
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2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Property

Boiling point:
689.8±50.0 °C(Predicted)
Density 
2.428±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Water Solubility 
Insoluble in water
form 
powder to crystal
color 
White to Light yellow to Light red
InChI
InChI=1S/C18H6Br6/c19-13-1-7-8(2-14(13)20)10-4-17(23)18(24)6-12(10)11-5-16(22)15(21)3-9(7)11/h1-6H
InChIKey
GLHQUXLCQLQNPZ-UHFFFAOYSA-N
SMILES
C1=C2C(C3C(C4C2=CC(Br)=C(Br)C=4)=CC(Br)=C(Br)C=3)=CC(Br)=C1Br
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Safety

HS Code 
29039990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TCI Chemical
Product number
H1201
Product name
2,3,6,7,10,11-Hexabromotriphenylene
Purity
>98.0%(T)
Packaging
1g
Price
$486
Updated
2025/07/31
TCI Chemical
Product number
H1201
Product name
2,3,6,7,10,11-Hexabromotriphenylene
Purity
>98.0%(T)
Packaging
100mg
Price
$47
Updated
2025/07/31
TRC
Product number
H290913
Product name
2,3,6,7,10,11-Hexabromotriphenylene
Packaging
100mg
Price
$60
Updated
2021/12/16
Usbiological
Product number
279843
Product name
2,3,6,7,10,11-Hexabromotriphenylene
Packaging
1g
Price
$350
Updated
2021/12/16
TRC
Product number
H290913
Product name
2,3,6,7,10,11-Hexabromotriphenylene
Packaging
50mg
Price
$45
Updated
2021/12/16
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2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Chemical Properties,Usage,Production

Synthesis

217-59-4

82632-80-2

Bromine (9.0 mL, 349 mmol) was added dropwise to a solution of 9,10-benzophenanthrene (3.95 g, 17.3 mmol) and iron powder (410 mg, 7.34 mmol) in nitrobenzene (200 mL) under nitrogen protection with stirring at room temperature for 20 min, and the reaction was subsequently heated up to 210°C for 3 hours. After completion of the reaction, the mixture was cooled to room temperature and the product was precipitated by the addition of ether (Et2O). The precipitate was collected by filtration and washed thoroughly with ether, acetone and chloroform (CHCl3) sequentially to afford the white powdery product 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene (11.5 g, 16.4 mmol, 94.8% yield). The melting point of the product was above 300°C; 1H NMR (300 MHz, CDCl3): δ = 8.72 (s, 6H, Ar-H); IR (KBr): νmax = 1585, 1551, 1454, 1365, 1119, 873, 863 cm-1.

References

[1] Journal of the American Chemical Society, 2017, vol. 139, # 48, p. 17229 - 17232
[2] Tetrahedron, 2015, vol. 71, # 29, p. 4714 - 4721
[3] Journal of Materials Chemistry, 2000, vol. 10, # 7, p. 1519 - 1525
[4] Journal of the American Chemical Society, 2017, vol. 139, # 46, p. 16759 - 16767
[5] Inorganic Chemistry, 2014, vol. 53, # 18, p. 9876 - 9896

2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Preparation Products And Raw materials

Raw materials

Preparation Products

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2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene Suppliers

Americas 1 China 118 Europe 1 India 2 Japan 1 United States 5 Global 128
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View Lastest Price from 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene manufacturers

Henan Fengda Chemical Co., Ltd
Product
2,3,6,7,10,11-Hexabromotriphenylene 82632-80-2
Price
US $200.00-1.00/KG
Min. Order
1KG
Purity
99%, 99.5% Sublimated
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-31
Career Henan Chemical Co
Product
2,3,6,7,10,11-HEXABROMOTRIPHENYLENE 82632-80-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2018-08-06

82632-80-2, 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthreneRelated Search:

2,3,6,7,10,11-hexa(4'-aminophenyl) trimethylene 2,3,6,7,10,11-hexa(pyridine-3-yl)triphenylene 2,3,6,7,10,11-hexa(4'-carboxyphenyl) trimethylene 2,3,6,7,10,11-hexaaminotriphenylene 2,3,6,7,10,11-HEXAACETOXYTRIPHENYLENE 2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene 2,3-DIBROMONAPHTHALENE 2,7-Dibromophenanthrene 3-BROMOPHENANTHRENE

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