4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID

Product Name: 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID
CAS No.: 914636-20-7
Chemical Name: 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID
Synonyms: 5-Carboxy-2-iodobenzotrifluoride;4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID;4-Iodo-3-(trifluoromethyl)benzoicacid99%;Benzoic acid, 4-iodo-3-(trifluoromethyl)-;4-Iodo-3-(trifluoromethyl)benzoic acid 99%
CBNumber: CB4654010
Molecular Formula: C8H4F3IO2
Formula Weight: 316.02
MOL File: Mol file

More

Less

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Property

Boiling point:: 311.7±42.0 °C(Predicted)
Density: 2.005±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 3.59±0.10(Predicted)
form: crystalline needles
color: Tan/brown
Sensitive: Light Sensitive/Air Sensitive

More

Less

Safety

Hazard Codes: Xi
HS Code: 2916399090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

Apolloscientific

Product number: PC9306
Product name: 4-Iodo-3-(trifluoromethyl)benzoicacid
Purity: 98%
Packaging: 5g
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 5G
Price: $384
Updated: 2021/12/16

AK Scientific

Product number: 7983DC
Product name: 4-Iodo-3-(trifluoromethyl)benzoicacid
Packaging: 5g
Price: $465
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 10g
Price: $688
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2821-K-X2
Product name: 4-Iodo-3-(trifluoromethyl)benzoic acid
Purity: 98%
Packaging: 1g
Price: $104
Updated: 2021/12/16

More

Less

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Chemical Properties,Usage,Production

Synthesis

400-76-0

914636-20-7

General procedure for the synthesis of 4-iodo-3-(trifluoromethyl)benzoic acid from 3-trifluoromethyl-4-aminobenzoic acid: 4-amino-3-trifluoromethylbenzoic acid (1.8 g, 8.8 mmol) was suspended in 30 mL of hydrochloric acid. An aqueous solution (15 mL) of sodium nitrite (0.76 g, 11.0 mmol) was slowly added dropwise at 0°C. The reaction mixture was stirred at 0-10 °C for 30 min. Subsequently, an aqueous solution (25 mL) of potassium iodide (14.6 g, 88 mmol) was added dropwise. The mixture was stirred at room temperature for 1 hour. After completion of the reaction, the product was extracted with ethyl acetate (80 mL) and the organic layer was washed with brine (80 mL). The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by fast chromatography using a gradient elution with ethyl acetate/hexane, resulting in 4-iodo-3-(trifluoromethyl)benzoic acid (2.4 g, 86% yield) as a solid.LC-ES/MS analysis showed m/e 339.3 (M+23) and 315.0 (M-1).

References

[1] Patent: WO2007/140174, 2007, A2. Location in patent: Page/Page column 42

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID Suppliers

China 33 India 2 United Kingdom 1 United States 4 Global 40

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 86(512)5235 8471 17715136450
Fax: 86(512)5235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 4169
Advantage: 58

Nanjing ShengSai Chemical Co., Ltd.

Tel: 025-85205967 13951876367
Fax: 025-85205967
Email: shengsaichem@163.com
Country: China
ProdList: 818
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9757
Advantage: 58

Aikon International Limited

Tel: 025-66113011 13155353615
Fax: (7)02557626880
Email: qzhang@aikonchem.com
Country: China
ProdList: 15394
Advantage: 58

Dandong Gilkuhn Import&Export Co., Ltd.

Tel: +86-519-83607890 18921087080
Fax: +86-519-83607890
Country: China
ProdList: 346
Advantage: 58

Henan's chemical products co., LTD

Tel: 0371-60919097 15378766539
Fax: 0371-60919097
Email: 794449696@qq.com
Country: China
ProdList: 4996
Advantage: 58

Shanghai SPAR pharmaceutical technology co., LTD

Tel: 021-000000 13917643586;
Email: admin@jingshipharmatech.com
Country: China
ProdList: 9856
Advantage: 58

914636-20-7, 4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACIDRelated Search:

4-IODO-3-(TRIFLUOROMETHYL)BENZOIC ACID

4-Iodo-3-(trifluoromethyl)benzoic acid 99%

5-Carboxy-2-iodobenzotrifluoride

4-Iodo-3-(trifluoromethyl)benzoicacid99%

Benzoic acid, 4-iodo-3-(trifluoromethyl)-

914636-20-7