antioxidant 1024
Handing and Safety- Product Name
- antioxidant 1024
- CAS No.
- 32687-78-8
- Chemical Name
- antioxidant 1024
- Synonyms
- hydrazide;IRGANOX MD 1024;LABOTEST-BB LT00261277;bis(3,5-di-tert-Butyl-4-hydroxyhydrocinnamoyl)hydrazine;1,2-BIS(3,5-DI-TERT-BUTYL-4-HYDROXYHYDROCINNAMOYL)HYDRAZINE;At 1024;MD-1024;AO-1024;HRao-1024;ThanoxMd-1024
- CBNumber
- CB4761970
- Molecular Formula
- C34H52N2O4
- Formula Weight
- 552.79
- MOL File
- 32687-78-8.mol
antioxidant 1024 Property
- Melting point:
- 60-67°C
- Boiling point:
- 652.6±55.0 °C(Predicted)
- Density
- 1.054±0.06 g/cm3(Predicted)
- storage temp.
- Refrigerator, under inert atmosphere
- solubility
- Acetonitrile (Slightly), Chloroform (Slightly)
- pka
- 11.10±0.50(Predicted)
- form
- Solid
- color
- White to Off-White
- LogP
- 4.8 at 23℃
- CAS DataBase Reference
- 32687-78-8(CAS DataBase Reference)
- EPA Substance Registry System
- 1,2-Bis[3,5-bis(tert-butyl)-4-hydroxyhydrocinnamoyl]hydrazide (32687-78-8)
Safety
- HS Code
- 2928009010
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H317May cause an allergic skin reaction
H319Causes serious eye irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D5516
- Product name
- 3-(3,5-Di-tert-butyl-4-hydroxyphenyl)-N'-[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoyl]propanehydrazide
- Purity
- >98.0%(HPLC)
- Packaging
- 5g
- Price
- $16
- Updated
- 2024/03/01
- Product number
- D5516
- Product name
- 3-(3,5-Di-tert-butyl-4-hydroxyphenyl)-N'-[3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoyl]propanehydrazide
- Purity
- >98.0%(HPLC)
- Packaging
- 25g
- Price
- $41
- Updated
- 2024/03/01
- Product number
- B592010
- Product name
- 1,2-Bis(3,5-di-tert-butyl-4-hydroxyhydrocinnamoyl)hydrazine
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- 098500
- Product name
- Antioxidant 1024
- Purity
- 95+%
- Packaging
- 25g
- Price
- $58
- Updated
- 2021/12/16
- Product number
- 098500
- Product name
- Antioxidant 1024
- Purity
- 95+%
- Packaging
- 100g
- Price
- $158
- Updated
- 2021/12/16
antioxidant 1024 Chemical Properties,Usage,Production
Handing and Safety
FDA approve antioxidant 1024 usage in packaging polymers, resins, and adhesives intended for food contact applications. It is approved in many countries for food contact applications.
Description
FDA approve antioxidant 1024 usage in packaging polymers, resins, and adhesives intended for food contact applications. It is approved in many countries for food contact applications.
Uses
Antioxidant 1024 is used in conjunction with phenolic antioxidants, phosphites/phosphonites, thio-synergists and other co-additives.
Application
Most suited for PA, PE, rubbers and PP applications. More efficient if it is added to the polymeric substance used in insulated electric wire and cable. Also it’s perfect melting nature makes it easily to mix with and into the substance mentioned above and other polymeric substance system without any dispersing problem.
Flammability and Explosibility
Not classified
Synthesis
1. Synthesis steps of β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionyl hydrazide
(1) Dissolve 54 g of hydrazine hydrate in 600 mL of a mixed solution of methanol and ethanol (V methanol: V ethanol = 1:2), then transfer to a dry three-necked flask, and then add 76 g of β-(3, 5-di-tert-butyl-4-hydroxyphenyl) methyl propionate, the three-necked flask is fixed on the iron stand, the ultrasonic time is 10min at room temperature, the intensity is 50KHz, and then the stirrer is placed, and at room temperature , Stir and react for 12h in a nitrogen protected environment, and wait until the reaction liquid is white and viscous;
(2) The white viscous reaction liquid obtained in step (1) is subjected to vacuum distillation. When a large amount of solids are deposited, the vacuum distillation is stopped, and then water is added to the reaction flask and stirred, that is, white crystals are deposited. After suction filtration , Recrystallize with n-hexane to obtain pure β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionyl hydrazide.
2. The synthesis steps of antioxidant 1024
(1) First, add 18 g of anhydrous β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionyl hydrazide, 10 g of ethyl acetoacetate, and 75 mL of dehydrated methanol and toluene into a three-necked flask. Solution (V methanol:V toluene=1:80), then add the rotor, and fix the thermometer, reflux condenser and nitrogen protection device on the three-necked flask;
(2) Place the three-necked flask containing the reactants in step (1) in an oil bath to slowly raise the temperature, and stop the reaction after reacting for 3 hours at 85°C;
(3) Cool the reaction solution of step (2) until crystals are precipitated, and then continue to drop to room temperature until the crystals are completely precipitated, and then perform suction filtration to obtain crystals. Wash the obtained crystals with water 3 times, and then use 5% hydrochloric acid Rinse, finally wash with water to neutrality, filter, and dry to obtain the final product Antioxidant 1024.
antioxidant 1024 Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from antioxidant 1024 manufacturers
- Product
- ANTIOXIDANT TRUELICHT AN1024 32687-78-8
- Price
- US $0.00/KG
- Min. Order
- 1drums
- Purity
- 98.0%
- Supply Ability
- 20 tons
- Release date
- 2021-11-23
- Product
- antioxidant 1024 32687-78-8
- Price
- US $10.00/kg
- Min. Order
- 1kg
- Purity
- 99.9
- Supply Ability
- 20 tons
- Release date
- 2023-11-14
- Product
- Antioxidant 1024 32687-78-8
- Price
- US $200.00-95.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20ton
- Release date
- 2024-04-24