6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE
- Product Name
- 6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE
- CAS No.
- 108281-79-4
- Chemical Name
- 6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE
- Synonyms
- 6-Bromo[1,2,4]triazolo[4,...;6-BROMO-TRIAZOLO[4,3-A]PYRIDINE;6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE;6-BROMO-[1,2,4]TRIAZOLO[4,3-A]PYRIDINE;1,2,4-Triazolo[4,3-a]pyridine, 6-bromo-;6-Bromo-[1,2,4]triazolo[4,3-a]pyridine 98%;6-Bromo-[1,2,4]triazolo[4,3-a]pyridine;6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE ISO 9001:2015 REACH
- CBNumber
- CB4840875
- Molecular Formula
- C6H4BrN3
- Formula Weight
- 198.02
- MOL File
- 108281-79-4.mol
6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE Property
- Melting point:
- 151-153
- Density
- 1.89±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 2.38±0.50(Predicted)
- form
- Solid
- Appearance
- Light yellow to green yellow Solid
- InChI
- InChI=1S/C6H4BrN3/c7-5-1-2-6-9-8-4-10(6)3-5/h1-4H
- InChIKey
- PFKZKSHKBBUZKU-UHFFFAOYSA-N
- SMILES
- C12=NN=CN1C=C(Br)C=C2
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- SYX00142
- Product name
- 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $330
- Updated
- 2025/07/31
- Product number
- B415498
- Product name
- 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- B415498
- Product name
- 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- OR3548
- Product name
- 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine
- Purity
- 98%
- Packaging
- 250mg
- Price
- $29
- Updated
- 2021/12/16
- Product number
- B12844
- Product name
- 6-Bromo-[1,2,4]triazolo[4,3-a]pyridine
- Purity
- 98%
- Packaging
- 1g
- Price
- $30
- Updated
- 2021/12/16
6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE Chemical Properties,Usage,Production
Synthesis
77992-44-0
122-51-0
108281-79-4
General procedure for the synthesis of 6-bromo-1,2,4-triazolo[4,3-1]pyridine from 2-hydrazino-5-bromopyridine and triethyl orthoformate: to a solution of 5-bromo-2-hydrazinopyridine (7.87 g, 42 mmol) in 200 mL of diethoxymethoxyethane was added p-toluenesulfonic acid (0.30 g, 1.7 mmol), the mixture was heated to 110 °C and stirred for 20 hours. After completion of the reaction, the mixture was cooled to room temperature and concentrated under vacuum. The residue was diluted with 150 mL of water, washed with saturated aqueous NaHCO3 (40 mL), and extracted with dichloromethane (300 mL × 3). The organic phases were combined, dried with anhydrous Na2SO4, and concentrated under vacuum. Purification of the residue by fast silica gel chromatography (petroleum ether/ethyl acetate, v/v = 2/1) afforded 6-bromo-1,2,4-triazolo[4,3-1]pyridine as a yellow solid (6.60 g, 79.77% yield). Mass spectrum (ESI, cation mode) m/z: 197.9 [M + H]+; 1H NMR (600 MHz, CDCl3): δ 8.82 (s, 1H), 8.34 (s, 1H), 7.75 (d, J = 9.7 Hz, 1H), 7.36 (d, J = 9.7 Hz, 1H).
References
[1] Patent: US2014/134133, 2014, A1. Location in patent: Paragraph 0451
6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE Suppliers
- Tel
- 021-31261262/ 49 (0)17662837245
- Fax
- (0)21-33250524
- sales@novochemy.com
- Country
- Germany
- ProdList
- 6328
- Advantage
- 58
View Lastest Price from 6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE manufacturers
- Product
- 6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE 108281-79-4
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-28
- Product
- 6-BROMO-1,2,4-TRIAZOLO[4,3-1]PYRIDINE 108281-79-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2019-07-10