4-NITRO-1-PHENYLIMIDAZOLE
- Product Name
- 4-NITRO-1-PHENYLIMIDAZOLE
- CAS No.
- 41384-83-2
- Chemical Name
- 4-NITRO-1-PHENYLIMIDAZOLE
- Synonyms
- 4-NITRO-1-PHENYLIMIDAZOLE;4-nitro-1-phenyl-1H-iMidazole;1H-Imidazole, 4-nitro-1-phenyl-
- CBNumber
- CB4849843
- Molecular Formula
- C9H7N3O2
- Formula Weight
- 189.17
- MOL File
- 41384-83-2.mol
4-NITRO-1-PHENYLIMIDAZOLE Property
- Melting point:
- 187 °C(Solv: methanol (67-56-1))
- Boiling point:
- 374.6±15.0 °C(Predicted)
- Density
- 1.33±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- -1.24±0.61(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 2786AL
- Product name
- 4-Nitro-1-phenyl-1H-imidazole
- Packaging
- 1g
- Price
- $358
- Updated
- 2021/12/16
- Product number
- CHM0034863
- Product name
- 4-NITRO-1-PHENYLIMIDAZOLE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $1357.07
- Updated
- 2021/12/16
- Product number
- A103958
- Product name
- 4-Nitro-1-phenyl-1H-imidazole
- Purity
- 95%
- Packaging
- 250mg
- Price
- $70
- Updated
- 2021/12/16
- Product number
- A103958
- Product name
- 4-Nitro-1-phenyl-1H-imidazole
- Purity
- 95%
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
- Product number
- 41384832
- Product name
- 4-Nitro-1-phenyl-1h-imidazole
- Packaging
- 1g
- Price
- $190.16
- Updated
- 2021/12/16
4-NITRO-1-PHENYLIMIDAZOLE Chemical Properties,Usage,Production
Synthesis
3034-38-6
98-80-6
41384-83-2
1. 1.6 mmol of 4-nitroimidazole (1a-e), 2.6 mmol of phenylboronic acid (2a-n), 1.6 mmol of sodium hydroxide, 0.2 mmol of CuCl2 and 15 mL of methanol were added to the reaction flask. 2. The reaction mixture was heated and refluxed under air bulge conditions. 3. The progress of the reaction was monitored by TLC, and after completion of the reaction the solvent was removed under reduced pressure using a rotary evaporator to remove the solvent under reduced pressure.4. The crude product was purified by silica gel column chromatography using 5:95 (v/v) methanol/chloroform as eluent to obtain the target product 4-nitro-1-phenylimidazole.5. The final product was purified by crystallization through a solvent mixture of methanol/water.
References
[1] Beilstein Journal of Organic Chemistry, 2013, vol. 9, p. 1517 - 1525
[2] Patent: WO2017/109488, 2017, A1. Location in patent: Page/Page column 41
[3] Patent: WO2018/65768, 2018, A1. Location in patent: Page/Page column 89
4-NITRO-1-PHENYLIMIDAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
4-NITRO-1-PHENYLIMIDAZOLE Suppliers
- Tel
- 025-58395930
- Fax
- 025-5861-9182
- sales@acornpharma.com
- Country
- China
- ProdList
- 982
- Advantage
- 60
- Tel
- +86-15251749953
- Fax
- -
- pl_pharmatech@163.com
- Country
- China
- ProdList
- 82
- Advantage
- 55
- Tel
- 18114022054; 18114022054
- Fax
- +86-25-58857385
- 3317707757@qq.com
- Country
- China
- ProdList
- 301
- Advantage
- 55
- Tel
- 025-57043319 15261831516
- Fax
- 025-57043319
- 307514552@qq.com
- Country
- China
- ProdList
- 251
- Advantage
- 50
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- +86-（0）57185586718; +8613336195806
- Fax
- +86-571-85864795
- sales@capot.com
- Country
- China
- ProdList
- 29735
- Advantage
- 60
- Tel
- 025-66061636 18013972705
- Fax
- (3)02557626880
- qqyang@aikonchem.com
- Country
- China
- ProdList
- 15814
- Advantage
- 58
- Tel
- 021-37653318; 15221675714
- 515366396@qq.com
- Country
- China
- ProdList
- 2089
- Advantage
- 58
- Tel
- 025-58786926 18951781718
- Fax
- 025-58786926
- zbbgz2009@163.com
- Country
- China
- ProdList
- 300
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58