ChemicalBook > CAS DataBase List > 6-FLUORO-2(3H)-BENZOTHIAZOLONE

6-FLUORO-2(3H)-BENZOTHIAZOLONE

Product Name: 6-FLUORO-2(3H)-BENZOTHIAZOLONE
CAS No.: 63754-96-1
Chemical Name: 6-FLUORO-2(3H)-BENZOTHIAZOLONE
Synonyms: 6-Fluorobenzothiazolone;6-Fluoro-3H-benzothiazol-2-one;6-Fluoro-1,3-benzothiazol-2-ol;6-FLUORO-2(3H)-BENZOTHIAZOLONE;6-Fluoro-2-hydroxybenzothiazole;2(3H)-Benzothiazolone, 6-fluoro-;6-fluorobenzo[d]thiazol-2(3H)-one;6-fluoro-3H-1,3-benzothiazol-2-one;2(3H)-Benzothiazolone,6-fluoro-(9CI)
CBNumber: CB51013307
Molecular Formula: C7H4FNOS
Formula Weight: 169.18
MOL File: 63754-96-1.mol

Less

6-FLUORO-2(3H)-BENZOTHIAZOLONE Property

Melting point:: 188.4 °C
Density: 1.474±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 9.26±0.20(Predicted)
Appearance: White to yellow Solid

Less

Safety

HS Code: 2934999090

Less

Hazard and Precautionary Statements (GHS)

Less

N-Bromosuccinimide Price

TRC

Product number: F600468
Product name: 6-Fluoro-2-hydroxy-benzothiazole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: F600468
Product name: 6-Fluoro-2-hydroxy-benzothiazole
Packaging: 100mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: Z4983
Product name: 6-Fluoro-2(3H)-benzothiazolone
Packaging: 250mg
Price: $124
Updated: 2021/12/16

Apolloscientific

Product number: PC904890
Product name: 6-Fluoro-2(3H)-benzothiazolone
Purity: 95%
Packaging: 1g
Price: $345
Updated: 2021/12/16

Matrix Scientific

Product number: 093265
Product name: 6-Fluoro-2(3H)-benzothiazolone
Purity: 95+%
Packaging: 250mg
Price: $378
Updated: 2021/12/16

Less

6-FLUORO-2(3H)-BENZOTHIAZOLONE Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

1373399-24-6

63754-96-1

General procedure for the synthesis of 6-fluorobenzothiazol-2-one using the compound (CAS:1373399-24-6) as starting material: ethyl 2-iodophenylcarbamate (1 mmol), cuprous iodide (CuI, 19 mg, 0.1 mmol), and sodium sulfide hydrate nine (Na2S-9H2O, 3 mmol) were added sequentially to a Schlenk tube. The reaction system was evacuated and displaced with argon (repeated 3 times), and then N,N-dimethylformamide (DMF, 2 mL) was added. The reaction mixture was stirred at 80 °C for 10 to 16 hours. Upon completion of the reaction, acetic acid (AcOH, 3 mL) was added to the cooled reaction mixture and the mixture was continued to be stirred at 130°C for 36 hours. At the end of the reaction, saturated sodium bicarbonate solution (10 mL) was added for neutralization, followed by extraction of the reaction mixture with ethyl acetate. The organic layers were combined, washed sequentially with water, saturated saline and dried with anhydrous sodium sulfate (Na2SO4). After the solvent was removed by distillation under reduced pressure, the resulting crude product was purified by silica gel column chromatography to finally obtain the target product 6-fluorobenzothiazol-2-one.

References

[1] Tetrahedron Letters, 2012, vol. 53, # 20, p. 2511 - 2513

6-FLUORO-2(3H)-BENZOTHIAZOLONE Preparation Products And Raw materials

Raw materials

Preparation Products

Less

6-FLUORO-2(3H)-BENZOTHIAZOLONE Suppliers

China 79 Europe 1 India 1 United States 5 Global 86

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
Fax: 86-021-50426522,50426273
Email: sales@jingyan-chemical.com
Country: China
ProdList: 9976
Advantage: 60

Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
Fax: 021-58099609
Email: bin.wu@shlschem.com
Country: China
ProdList: 9883
Advantage: 59

China DongFan Chemical Co.,LTD

Tel: 86-0571-85151182
Fax: 86-0571-85151182
Country: China
ProdList: 5691
Advantage: 66

China Langchem Inc.

Tel: 0086-21-58956006
Fax: 0086-21-58956100
Country: China
ProdList: 7811
Advantage: 57

chenyue Chemicals Co., Ltd.

Tel: +86-0519-85500896
Fax: +86-0519-85335069
Email: benzoxazolone@163.com
Country: China
ProdList: 178
Advantage: 58

Beijing Taiya Jie Technology Development Co., Ltd.

Tel: 021-33690831-8001 13552411790
Fax: 021-33690831
Email: postmaster@tyjchem.cn
Country: China
ProdList: 1542
Advantage: 55

Wuhan Fortuna Chemical Co., Ltd

Tel: 027-59207852 13308628970
Fax: QQ3130921841
Email: buy@fortunachem.com
Country: China
ProdList: 2744
Advantage: 58

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 86(512)5235 8471 17715136450
Fax: 86(512)5235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 4169
Advantage: 58

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Shanghai YuLue Chemical Co., Ltd.

Tel: 021-60345187 13671753212
Fax: 021-34702061
Email: lzz841106@aliyun.com
Country: China
ProdList: 10263
Advantage: 55

Shanghai ACT chemical Limited

Tel: 021-59904146 18001826933
Fax: +86-21-59904146
Email: sales@actchemical.com
Country: China
ProdList: 476
Advantage: 56

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Shanghai Yongye Biotechnology Co., Ltd.

Tel: 86-021-61559134 15921386130
Fax: 021-55068248
Email: 3423497944@qq.com
Country: China
ProdList: 8144
Advantage: 55

Nanjing Duolong Bio-tech Co.,Ltd.

Tel: 18905173768
Fax: 025-83263139
Email: 52513593@qq.com
Country: China
ProdList: 2331
Advantage: 50

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

NovoChemy Ltd.

Tel: 86-(0)21-31261262 373522135
Fax: 86-(0)21-33250524
Email: sales@novochemy.com
Country: China
ProdList: 6498
Advantage: 58

Shanghai WeiNie Chemical Technology Co., Ltd.

Tel: 15902145085
Fax: -
Email: 657990292@qq.com
Country: China
ProdList: 668
Advantage: 50

Nanjing Vital Chemical Co., Ltd.

Tel: 025-87193546 18652950785
Fax: 025-87193546
Email: chemweiao@163.com
Country: China
ProdList: 9021
Advantage: 60

Shanghai Shanyuan pharmaceutical technology co., LTD

Tel: 021-31761238 13167072949
Fax: 021-31761238
Email: 3146446224@qq.com
Country: China
ProdList: 1379
Advantage: 55

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Nanjing KaiMubo Pharmaceutical Co., Ltd.

Tel: 025-66162170
Fax: 025-66162170
Country: China
ProdList: 7181
Advantage: 55

Shanghai Qianlai Medical Technology Co., Ltd.

Tel: 482109853
Fax: 021-37288278
Email: info@qianlaiyiyao.com
Country: China
ProdList: 406
Advantage: 58

Shanghai CR Corporation Limited

Tel: 13062833949; 4006653949 4006653949
Fax: QQ: 2136646215
Email: fred.wen@crcorporation.cn
Country: China
ProdList: 9756
Advantage: 58

Hangzhou Molcore Biopharmatech Co.,Ltd

Tel: 400-711-5280 86-571-81025280
Fax: 86-571-85806285
Email: sales@molcore.com
Country: China
ProdList: 9967
Advantage: 58

Sichuan BaiPeng Biotechnology Co., Ltd.

Tel: 028-65791793 18140026355
Fax: QQ568470422
Email: 568470422@qq.com
Country: China
ProdList: 9997
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 400821072
Fax: 021-58955996
Email: malulu@leyan.com
Country: China
ProdList: 25000
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Allfluoro pharmaceutical co. ltd.

Tel: +86-400-0216110 +86-15958047586
Fax: 0086-21-33275002
Email: sales@allfluoro.com
Country: China
ProdList: 11385
Advantage: 58

Dayang Chem (Hangzhou) Co.,Ltd.

Tel: +86-0571-88938639 +8617705817739
Fax: +86-571-88938652，+86-571- 88492614
Email: info@dycnchem.com
Country: China
ProdList: 52846
Advantage: 58

Hefei Hirisun Pharmatech Co., Ltd

Tel: +8615056975894
Fax: 86-0551-62678551
Email: shawn@hirisunpharm.com
Country: CHINA
ProdList: 9911
Advantage: 58

SIMAGCHEM CORP

Tel: +86-5922680277 +86-13806087780
Email: sale@simagchem.com
Country: China
ProdList: 17346
Advantage: 58

Zhejiang Lianshuo Biotechnology Co., Ltd.

Tel: 18616526224
Email: lianshuo@vip.126.com
Country: China
ProdList: 9607
Advantage: 58

Shanghai Pleikon Chemical Technology Co., Ltd

Tel: 021-021-54321516 17717324060
Email: 2719672468@qq.com
Country: China
ProdList: 1880
Advantage: 58

Shanghai Hongshun Biological Technology Co., Ltd.

Tel: 15901914505 15901914505;
Fax: 021-54389085
Email: 3187892335@qq.com
Country: China
ProdList: 9889
Advantage: 58

Xinyi Guangbang Medical Technology Co., Ltd.

Tel: 13361936468
Email: 410756539@qq.com
Country: China
ProdList: 306
Advantage: 58

Shanghai Kaiwei Chemical Technology Co., Ltd.

Tel: 021-58461859 15821823057
Email: service@aiviche.com
Country: China
ProdList: 49312
Advantage: 58

career henan chemical co

Tel: +86-0371-86658258 +8613203830695
Fax: 0086-371-86658258
Email: factory@coreychem.com
Country: China
ProdList: 29798
Advantage: 58

Taizhou Nanfeng Pharmaceutical Research Institute

Tel: nanfengdrug@163.com; 18616377689
Email: nanfengdrug@163.com
Country: China
ProdList: 20009
Advantage: 58

Henan Weitesi Chemical Technology Co. LTD

Tel: 0371-0371-55135753 18003832934
Fax: QQ：2853979818
Email: 2853979818@qq.com
Country: China
ProdList: 9991
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing@energy-chemical.com
Country: China
ProdList: 44918
Advantage: 58

Mainchem Co., Ltd.

Tel: --
Fax: --
Email: sarah@mainchem.com
Country: China
ProdList: 6547
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-1647117 13681763483
Email: product02@bidepharm.com
Country: China
ProdList: 59936
Advantage: 58

Qi Qi hang Biotechnology Co., Ltd.

Tel: 15870833005
Email: 2232044025@qq.com
Country: China
ProdList: 8206
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39665
Advantage: 58

Henan Evonik Biotechnology Co. LTD

Tel: 15672878902
Email: hnyingchuang@163.com
Country: China
ProdList: 3905
Advantage: 58

Shandong Mingde Biotechnology Co., Ltd

Tel: 15553348166
Email: m15553348166@163.com
Country: China
ProdList: 9967
Advantage: 58

Beijing InnoChem Science & Technology Co., Ltd.

Tel: 15652467323
Email: sales@inno-chem.com.cn
Country: China
ProdList: 8293
Advantage: 58

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 18621169109
Email: market03@meryer.com
Country: China
ProdList: 27987
Advantage: 58

Shaanxi PharmaGHS Science Co., LTD

Tel: 13279368192
Email: pharmaghs@126.com
Country: China
ProdList: 2935
Advantage: 58

Less

View Lastest Price from 6-FLUORO-2(3H)-BENZOTHIAZOLONE manufacturers

Honest Joy Holdings Limited

Product: 6-Fluoro-2(3H)-Benzothiazolone 63754-96-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 97.9%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: 6-FLUORO-2(3H)-BENZOTHIAZOLONE 63754-96-1
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

63754-96-1, 6-FLUORO-2(3H)-BENZOTHIAZOLONERelated Search:

2-Amino-4,6-dichlorobenzothiazole 5-CHLOROBENZOTHIAZOLE 5-Bromo-2-mercaptobenzothiazole 2-Benzothiazolol 6-BROMO-2-BENZOTHIAZOLINONE 4-FLUORO-2(3H)-BENZOTHIAZOLONE 6-METHYL-3H-BENZOTHIAZOL-2-ONE 4-Choro-2(3H)-benzothiazolone 6-CHLORO-3H-BENZOTHIAZOL-2-ONE 5--fluoro-2(3H)-benzothiazolone 2-HYDROXY-4-METHYL-BENZOTHIOZOLE 5-BROMO-2(3H)-BENZOTHIAZOLONE 2(3H)-Benzothiazolone,7-chloro-(9CI) 6-METHOXY-2(3H)-BENZOTHIAZOLONE 6-FLUORO-2(3H)-BENZOTHIAZOLONE 2-AMINO-5-FLUOROBENZENETHIOL 2(3H)-Benzothiazolone,4,5,6,7-tetrafluoro-(9CI) 4,6-DIFLUORO-2(3H)-BENZOTHIAZOLONE

6-Fluoro-3H-benzothiazol-2-one

6-fluorobenzo[d]thiazol-2(3H)-one

6-Fluoro-2-hydroxybenzothiazole

6-FLUORO-2(3H)-BENZOTHIAZOLONE

2(3H)-Benzothiazolone,6-fluoro-(9CI)

6-fluoro-3H-1,3-benzothiazol-2-one

6-Fluorobenzothiazolone

2(3H)-Benzothiazolone, 6-fluoro-

6-Fluoro-1,3-benzothiazol-2-ol

63754-96-1

BENZOTHIAZOLE