METHYL M-NITROPHENYL CARBINOL

Product Name: METHYL M-NITROPHENYL CARBINOL
CAS No.: 5400-78-2
Chemical Name: METHYL M-NITROPHENYL CARBINOL
Synonyms: NITRO HYDROXY;1-(3-NITROPHENYL)ETHANOL;1-(3-NIitrophenyl)ethanol;1-(3-Nitrophenyl)ethan-1-ol;3-NITROPHENYLMETHYLCARBINOL;METHYL M-NITROPHENYL CARBINOL;2-methyl-3-nitroBenzenemethanol;Benzenemethanol, a-methyl-3-nitro-;Benzenemethanol, α-methyl-3-nitro-
CBNumber: CB5101713
Molecular Formula: C8H9NO3
Formula Weight: 167.16
MOL File: 5400-78-2.mol

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METHYL M-NITROPHENYL CARBINOL Property

Melting point:: 62.5 °C
Boiling point:: 154-155 °C(Press: 9 Torr)
Density: 1.2049 g/cm3(Temp: 31 °C)
storage temp.: Sealed in dry,Room Temperature
pka: 13.89±0.20(Predicted)
Appearance: Off-white to light yellow Solid

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Safety

RTECS: DJ3100438
HS Code: 2906290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S489697
Product name: 1-(3-NITRO-PHENYL)-ETHANOL
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $185
Updated: 2025/07/31

Sigma-Aldrich

Product number: S489697
Product name: 1-(3-NITRO-PHENYL)-ETHANOL
Purity: Aldrich
Packaging: 25mg
Price: $179
Updated: 2024/03/01

TRC

Product number: N545390
Product name: 1-(3-Nitrophenyl)ethanol
Packaging: 250mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 155375
Product name: 1-(3-Nitrophenyl)ethanol
Packaging: 0.500g
Price: $160
Updated: 2021/12/16

AK Scientific

Product number: V6505
Product name: 1-(3-Nitrophenyl)ethanol
Packaging: 25g
Price: $195
Updated: 2021/12/16

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METHYL M-NITROPHENYL CARBINOL Chemical Properties,Usage,Production

Synthesis

121-89-1

5400-78-2

1. Sodium borohydride (NaBH4, 2.20 g, 58.1 mmol) was slowly added to a solution of methanol (MeOH, 100 mL) containing 1-(3-nitrophenyl)ethanone (ID29, 2.32 g, 14.0 mmol) at 0°C. 2. The reaction mixture was stirred continuously at 0 °C for 1 hour. 3. After completion of the reaction, most of the methanol was removed by concentration under reduced pressure. 4. 4. The residue was diluted with ethyl acetate (EtOAc, 150 mL) and water (50 mL) and the organic layer was separated. 5. The organic layer was washed sequentially with water (50 mL) and saturated saline (50 mL) and then dried over anhydrous sodium sulfate (Na2SO4). 6. The desiccant was removed by filtration, and the filtrate was concentrated under reduced pressure to obtain the crude product. 7. The crude product was dried under vacuum to afford 1-(3-nitrophenyl)ethanol (ID30) as a pale yellow oil (2.23 g, 95% yield). 8. The structure of the product was determined by 1H NMR. 8. The structure of the product was confirmed by 1H NMR (CDCl3, 600 MHz): δ 8.25 (s, 1H), 8.12 (ddd, J = 8.4, 1.2, 1.2 Hz, 1H), 7.72 (d, J = 7.2 Hz, 1H), 7.52 (dd, J = 8.1, 8.1 Hz, 1H), 5.02 (q, J = 6.6 Hz, 1H), 2.07 (s, J = 6.6 Hz, 1H), 5.02 (q, J = 6.6 Hz, 1H), 5.02 (q, J = 6.6 Hz, 1H), 2.02 (q, J = 6.6 Hz, 1H), 2.07 (s), 2.07 (s), 1H). ), 2.07 (s, 1H), 1.54 (d, J = 6.6 Hz, 3H).

References

[1] Green Chemistry, 2018, vol. 20, # 9, p. 2118 - 2124
[2] Journal of the Iranian Chemical Society, 2015, vol. 12, # 7, p. 1221 - 1226
[3] Synthetic Communications, 1990, vol. 20, # 6, p. 849 - 854
[4] Chemistry Letters, 1987, p. 181 - 184
[5] Synthesis, 2009, # 23, p. 4058 - 4062

METHYL M-NITROPHENYL CARBINOL Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL M-NITROPHENYL CARBINOL Suppliers

China 44 Germany 1 India 1 Ukraine 1 United Kingdom 2 United States 8 Global 57

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METHYL M-NITROPHENYL CARBINOL

3-NITROPHENYLMETHYLCARBINOL

1-(3-NITROPHENYL)ETHANOL

1-(3-NIitrophenyl)ethanol

2-methyl-3-nitroBenzenemethanol

1-(3-Nitrophenyl)ethan-1-ol

Benzenemethanol, α-methyl-3-nitro-

Benzenemethanol, a-methyl-3-nitro-

NITRO HYDROXY

5400-78-2

Benzhydrols, Benzyl & Special Alcohols