6-methoxypyridine-2-carbonitrile
- Product Name
- 6-methoxypyridine-2-carbonitrile
- CAS No.
- 83621-01-6
- Chemical Name
- 6-methoxypyridine-2-carbonitrile
- Synonyms
- 133750;6-methoxypicolinonitrile;2-Cyano-6-methoxypyridine;6-Methoxy-2-Pyridinecarbonitrile;2-Pyridinecarbonitrile,6-methoxy-;6-Methoxy-2-pyridinecarbonitrile 97%
- CBNumber
- CB51094166
- Molecular Formula
- C7H6N2O
- Formula Weight
- 134.14
- MOL File
- 83621-01-6.mol
6-methoxypyridine-2-carbonitrile Property
- Melting point:
- 62-67°C
- Boiling point:
- 115-120 °C(Press: 19 Torr)
- Density
- 1.16±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- solid
- pka
- -2.15±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-37/38-41
- Safety Statements
- 26-36/37/39
- RIDADR
- UN 3439 6.1 / PGIII
- WGK Germany
- 3
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H312Harmful in contact with skin
H315Causes skin irritation
H318Causes serious eye damage
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M332903
- Product name
- 6-Methoxypyridine-2-carbonitrile
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- M332903
- Product name
- 6-Methoxypyridine-2-carbonitrile
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- OR901728
- Product name
- 6-Methoxypyridine-2-carbonitrile
- Purity
- 95%
- Packaging
- 1g
- Price
- $145
- Updated
- 2021/12/16
- Product number
- OR901728
- Product name
- 6-Methoxypyridine-2-carbonitrile
- Purity
- 95%
- Packaging
- 10g
- Price
- $646
- Updated
- 2021/12/16
- Product number
- CHM0094369
- Product name
- 2-PYRIDINECARBONITRILE,6-METHOXY-
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $669.31
- Updated
- 2021/12/16
6-methoxypyridine-2-carbonitrile Chemical Properties,Usage,Production
Synthesis
98276-69-8
83621-01-6
GENERAL STEPS: To a solution of 6-methoxypyridine-2-carboxamide (300 mg, 1.97 mmol) in tetrahydrofuran (THF, 3 mL) was added triethylamine (1.25 mL, 8.68 mmol), followed by the slow dropwise addition of trifluoroacetic anhydride (TFAA, 0.61 mL, 4.34 mmol), under ice-bath conditions. The reaction mixture was gradually warmed to room temperature and stirred overnight. Upon completion of the reaction, the volatile solvent was removed by distillation under reduced pressure and the remaining liquid residue was slowly added dropwise to vigorously stirred, ice-cold pH 7 phosphate buffer solution (5 mL). After continued stirring for 15 min, the resulting pale yellow solid was collected by filtration and dried in air for 1 h. 6-Methoxypyridine-2-carbonitrile (250 mg, 95% yield) was obtained as a pale yellow solid with a mass spectrum (m/z): 135.4 [M + 1]+.
References
[1] Patent: WO2009/70485, 2009, A1. Location in patent: Page/Page column 105
6-methoxypyridine-2-carbonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-methoxypyridine-2-carbonitrile manufacturers
- Product
- 6-Methoxypyridine-2-carbonitrile 83621-01-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- Min98% HPLC
- Supply Ability
- g/kg/ton
- Release date
- 2020-02-04