2-ACETYLBENZENECARBONITRILE

Product Name: 2-ACETYLBENZENECARBONITRILE
CAS No.: 91054-33-0
Chemical Name: 2-ACETYLBENZENECARBONITRILE
Synonyms: 2-acetylbenzenitrile;2-ACETYLBENZONITRILE;2'-CYANOACETOPHENONE;Benzonitrile,2-acetyl-;2-ACETYLBENZENECARBONITRILE;Benzonitrile, 2-acetyl- (9CI)
CBNumber: CB5133554
Molecular Formula: C9H7NO
Formula Weight: 145.16
MOL File: 91054-33-0.mol

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2-ACETYLBENZENECARBONITRILE Property

Melting point:: 46-48°C
Boiling point:: 264.27°C (rough estimate)
Density: 1.1555 (rough estimate)
refractive index: 1.4500 (estimate)
storage temp.: Inert atmosphere,Room Temperature
form: solid
color: Off-white to light yellow
CAS DataBase Reference: 91054-33-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xn
Risk Statements: 20/21/22-36/37/38-22
Safety Statements: 26-36/37/39
RIDADR: 3439
HazardClass: IRRITANT
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A171018
Product name: 2-Acetylbenzenecarbonitrile
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: A171018
Product name: 2-Acetylbenzenecarbonitrile
Packaging: 250mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC66501
Product name: 2'-Cyanoacetophenone
Packaging: 2g
Price: $100
Updated: 2021/12/16

Matrix Scientific

Product number: 043581
Product name: 2-Acetylbenzenecarbonitrile
Purity: >95%
Packaging: 1g
Price: $49
Updated: 2021/12/16

AK Scientific

Product number: W9358
Product name: 2-Acetylbenzonitrile
Packaging: 1g
Price: $54
Updated: 2021/12/16

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2-ACETYLBENZENECARBONITRILE Chemical Properties,Usage,Production

Synthesis

557-21-1

2142-68-9

91054-33-0

Under argon protection, NiCl2-6H2O (0.05 mmol, 11.9 mg), dppf (0.06 mmol, 33.3 mg), Zn (0.2 mmol, 13.0 mg), DMAP (1.0 mmol, 122.2 mg), Zn(CN)2 (0.8 mmol, 93.9 mg), o-chloroacetophenone (1.0 mmol, 140.6 mg) and acetonitrile (5.0 mL) were added to a 25.0 mL sealed tube. The reaction mixture was placed in an oil bath at 60°C for 6 hours. After completion of the reaction, it was cooled to room temperature and the reaction solution was filtered directly through a short silica gel column and washed with dichloromethane. The filtrate was concentrated and purified by silica gel column chromatography (wet sampling was used to avoid sample loss). The eluent ratio was petroleum ether/ethyl acetate=20:1, and 117.2 mg of 2-acetylbenzonitrile was obtained as a white solid with 88% yield, and the 1H NMR showed a purity of more than 98%.

References

[1] Organic Letters, 2017, vol. 19, # 8, p. 2118 - 2121
[2] Patent: CN108623495, 2018, A. Location in patent: Paragraph 0043; 0045; 0139-0141

2-ACETYLBENZENECARBONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-ACETYLBENZENECARBONITRILE Suppliers

China 75 Europe 1 Germany 3 India 1 Switzerland 1 United Kingdom 9 United States 14 Global 104

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View Lastest Price from 2-ACETYLBENZENECARBONITRILE manufacturers

Career Henan Chemical Co

Product: 2-ACETYLBENZENECARBONITRILE 91054-33-0
Price: US $2.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2018-12-24

91054-33-0, 2-ACETYLBENZENECARBONITRILERelated Search:

2-(2-BROMOACETYL)BENZONITRILE 2-ACETYLBENZENECARBONITRILE 4-Acetylbenzonitrile 3-ACETYLBENZONITRILE 2-CYANO-4'-IODOBENZOPHENONE 3-BROMO-2'-CYANOBENZOPHENONE 2-CYANOBENZOPHENONE 97 2-(2-BROMOPHENYL)-2'-CYANOACETOPHENONE 2-CYANO-2'-IODOBENZOPHENONE 2-CYANO-3'-IODOBENZOPHENONE 2-CYANO-3'-METHOXYBENZOPHENONE TRANS-2-(2-CYANOBENZOYL)CYCLOPENTANE-1-CARBOXYLIC ACID 2-CYANO-4'-METHOXYBENZOPHENONE 2-CYANO-2'-METHOXYBENZOPHENONE 2-CHLORO-3-(2-CYANOBENZOYL)PYRIDINE 2'-CYANO-2-PHENYLACETOPHENONE 4-BROMO-2'-CYANOBENZOPHENONE 2-BROMO-2'-CYANOBENZOPHENONE

2'-CYANOACETOPHENONE

2-ACETYLBENZENECARBONITRILE

2-ACETYLBENZONITRILE

Benzonitrile,2-acetyl-

Benzonitrile, 2-acetyl- (9CI)

2-acetylbenzenitrile

91054-33-0

NITRILE

ACETYLGROUP

Aromatic Nitriles