ChemicalBook > CAS DataBase List > BUTTPARK 83\09-70

BUTTPARK 83\09-70

Product Name
BUTTPARK 83\09-70
CAS No.
16154-62-4
Chemical Name
BUTTPARK 83\09-70
Synonyms
BUTTPARK 83\09-70;1-(2-Chloro-4-nitrophenyl);1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPER;1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPERAZINE;Piperazine, 1-(2-chloro-4-nitrophenyl)-4-methyl-;1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine,97%
CBNumber
CB5140622
Molecular Formula
C11H14ClN3O2
Formula Weight
255.7
MOL File
Mol file
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BUTTPARK 83\09-70 Property

Melting point:
106 °C
Boiling point:
384.9±42.0 °C(Predicted)
Density 
1.300±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
Solid
pka
7.18±0.42(Predicted)
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FC143774
Product name
1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging
500mg
Price
$105
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC143774
Product name
1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging
250mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
W3507
Product name
1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging
1g
Price
$72
Updated
2021/12/16
Oakwood
Product number
092578
Product name
1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Purity
95+%
Packaging
5g
Price
$95
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC143774
Product name
1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
Packaging
1g
Price
$180
Updated
2021/12/16
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BUTTPARK 83\09-70 Chemical Properties,Usage,Production

Synthesis

109-01-3

350-30-1

16154-62-4

Preparative Example 1 Synthesis of 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine: in a dry reaction flask, 3-chloro-4-fluoronitrobenzene (10.05 g, 57.2 mmol) was mixed with N-methylpiperazine (17.2 g, 172 mmol). Exothermic phenomenon was observed during the reaction and after 1 h of continuous stirring, the reaction mixture was quenched by adding water to the reaction mixture. The resulting brown solid precipitate was collected by filtration and washed with plenty of water to remove unreacted raw materials and by-products. Finally, the product was dried in air to afford 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine (14.1 g, 96% yield). The product was confirmed by 1H NMR (400 MHz, DMSO-d6) and mass spectrometry (MS) characterization: 1H NMR δ 2.24 (s, 3H), 2.43-2.55 (m, 4H), 3.11-3.24 (m, 4H), 7.28 (d, J = 9.03 Hz, 1H), 8.14 (dd, J = 9.03,2.76 Hz, 1H) , 8.21 (d, J = 2.51Hz, 1H); MS m/z 255 (M+).

References

[1] Patent: WO2011/120026, 2011, A1. Location in patent: Page/Page column 34-35
[2] Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997, vol. 36, # 4, p. 347 - 348
[3] Patent: WO2016/22460, 2016, A1. Location in patent: Page/Page column 137
[4] Patent: WO2017/66428, 2017, A1. Location in patent: Page/Page column 249

BUTTPARK 83\09-70 Preparation Products And Raw materials

Raw materials

Preparation Products

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BUTTPARK 83\09-70 Suppliers

Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
Advantage
59
Shanghai Longsheng chemical Co.,Ltd.
Tel
021-58099652-8005 13585536065
Fax
021-58099609
Email
bin.wu@shlschem.com
Country
China
ProdList
9883
Advantage
59
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
Advantage
64
Shanghai Ennopharm Co., Ltd.
Tel
+86 (21) 6435-5022
Country
China
ProdList
4267
Advantage
65
Wuhan ariel chemical Co., LTD.
Tel
18986259541
Fax
027-87840182
Email
sales@3stc.com
Country
China
ProdList
3763
Advantage
58
NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
Advantage
58
Shanghai Jian Chao Chemical Technology Co., Ltd.
Tel
150-2103-5486 18017383231
Fax
qq:2817624287
Email
983544897@qq.com
Country
China
ProdList
9342
Advantage
55
Wuhan Kaymke Chemical Co., Ltd.,
Tel
027-027-87342388 18086026008
Fax
027-87342388
Email
sales@kaymke.com
Country
China
ProdList
3732
Advantage
55
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View Lastest Price from BUTTPARK 83\09-70 manufacturers

Career Henan Chemical Co
Product
BUTTPARK 83\09-70 16154-62-4
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2020-01-08

16154-62-4, BUTTPARK 83\09-70Related Search:


  • BUTTPARK 83\09-70
  • 1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPERAZINE
  • 1-(2-Chloro-4-nitrophenyl)
  • 1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPER
  • Piperazine, 1-(2-chloro-4-nitrophenyl)-4-methyl-
  • 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine,97%
  • 16154-62-4