BUTTPARK 83\09-70
- Product Name
- BUTTPARK 83\09-70
- CAS No.
- 16154-62-4
- Chemical Name
- BUTTPARK 83\09-70
- Synonyms
- BUTTPARK 83\09-70;1-(2-Chloro-4-nitrophenyl);1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPER;1-(2-CHLORO-4-NITROPHENYL)-4-METHYLPIPERAZINE;Piperazine, 1-(2-chloro-4-nitrophenyl)-4-methyl-;1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine,97%
- CBNumber
- CB5140622
- Molecular Formula
- C11H14ClN3O2
- Formula Weight
- 255.7
- MOL File
- Mol file
BUTTPARK 83\09-70 Property
- Melting point:
- 106 °C
- Boiling point:
- 384.9±42.0 °C(Predicted)
- Density
- 1.300±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- Solid
- pka
- 7.18±0.42(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FC143774
- Product name
- 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
- Packaging
- 500mg
- Price
- $105
- Updated
- 2021/12/16
- Product number
- FC143774
- Product name
- 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
- Packaging
- 250mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- W3507
- Product name
- 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
- Packaging
- 1g
- Price
- $72
- Updated
- 2021/12/16
- Product number
- 092578
- Product name
- 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
- Purity
- 95+%
- Packaging
- 5g
- Price
- $95
- Updated
- 2021/12/16
- Product number
- FC143774
- Product name
- 1-(2-Chloro-4-nitrophenyl)-4-methylpiperazine
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
BUTTPARK 83\09-70 Chemical Properties,Usage,Production
Synthesis
109-01-3
350-30-1
16154-62-4
Preparative Example 1 Synthesis of 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine: in a dry reaction flask, 3-chloro-4-fluoronitrobenzene (10.05 g, 57.2 mmol) was mixed with N-methylpiperazine (17.2 g, 172 mmol). Exothermic phenomenon was observed during the reaction and after 1 h of continuous stirring, the reaction mixture was quenched by adding water to the reaction mixture. The resulting brown solid precipitate was collected by filtration and washed with plenty of water to remove unreacted raw materials and by-products. Finally, the product was dried in air to afford 1-(2-chloro-4-nitrophenyl)-4-methylpiperazine (14.1 g, 96% yield). The product was confirmed by 1H NMR (400 MHz, DMSO-d6) and mass spectrometry (MS) characterization: 1H NMR δ 2.24 (s, 3H), 2.43-2.55 (m, 4H), 3.11-3.24 (m, 4H), 7.28 (d, J = 9.03 Hz, 1H), 8.14 (dd, J = 9.03,2.76 Hz, 1H) , 8.21 (d, J = 2.51Hz, 1H); MS m/z 255 (M+).
References
[1] Patent: WO2011/120026, 2011, A1. Location in patent: Page/Page column 34-35
[2] Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1997, vol. 36, # 4, p. 347 - 348
[3] Patent: WO2016/22460, 2016, A1. Location in patent: Page/Page column 137
[4] Patent: WO2017/66428, 2017, A1. Location in patent: Page/Page column 249
BUTTPARK 83\09-70 Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from BUTTPARK 83\09-70 manufacturers
- Product
- BUTTPARK 83\09-70 16154-62-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2020-01-08