ChemicalBook > CAS DataBase List > 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE

2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE

Product Name
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE
CAS No.
18648-66-3
Chemical Name
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE
Synonyms
1,1-Diphenyl-2-(4-bromophenyl)ethene;2-(4-Bromophenyl)-1,1-diphenylethene;1-Bromo-4-(2,2-diphenylvinyl)benzene;2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE;1-Bromo-4-(2,2-diphenylethenyl)-benzene;2-(p-Bromophenyl)-1,1-diphenyl-ethylene;Benzene, 1-bromo-4-(2,2-diphenylethenyl)-;2-(4-Bromophenyl)-1,1-diphenylethylene >(2-(4-bromophenyl)ethene-1,1-diyl)dibenzene;1-(2-(4-Bromophenyl)-1-phenylvinyl)benzene ,98%
CBNumber
CB51479141
Molecular Formula
C20H15Br
Formula Weight
335.24
MOL File
18648-66-3.mol
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2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Property

Melting point:
79 °C
Boiling point:
404.4±14.0 °C(Predicted)
Density 
1.313±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Toluene
form 
powder to crystal
color 
White to Almost white
InChI
InChI=1S/C20H15Br/c21-19-13-11-16(12-14-19)15-20(17-7-3-1-4-8-17)18-9-5-2-6-10-18/h1-15H
InChIKey
HUCFDUOIMSRYAA-UHFFFAOYSA-N
SMILES
C1(Br)=CC=C(/C=C(/C2=CC=CC=C2)\C2=CC=CC=C2)C=C1
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Safety

HS Code 
2903.99.8001
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TCI Chemical
Product number
B3090
Product name
2-(4-Bromophenyl)-1,1-diphenylethylene
Packaging
5G
Price
$196
Updated
2024/03/01
TCI Chemical
Product number
B3090
Product name
2-(4-Bromophenyl)-1,1-diphenylethylene
Packaging
25G
Price
$734
Updated
2022/04/27
TRC
Product number
B700328
Product name
2-(4-Bromophenyl)-1,1-diphenylethylene
Packaging
500mg
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
090370
Product name
2-(4-Bromophenyl)-1,1-diphenylethylene
Purity
95+%
Packaging
1g
Price
$152
Updated
2021/12/16
Matrix Scientific
Product number
090370
Product name
2-(4-Bromophenyl)-1,1-diphenylethylene
Purity
95+%
Packaging
5g
Price
$404
Updated
2021/12/16
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2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Chemical Properties,Usage,Production

Synthesis

119-61-9

589-15-1

18648-66-3

General procedure for the synthesis of 2-(4-bromophenyl)-1,1-diphenylethylene from benzophenone and p-bromobenzyl bromide: 40.00 g of p-bromobenzyl bromide (0.16 mol) and 83.6 mL of triethyl phosphite (0.48 mol) were added to a 500 mL three-necked flask, and the reaction was heated under argon protection in an oil bath at 150 °C for 24 h with magnetic stirring, and then the reaction was The reaction was cooled to room temperature to obtain the Yerid reagent. To another three-necked flask was added 450 mL of tetrahydrofuran (THF) followed by 21.87 g of benzophenone (0.12 mol) and 40.39 g of potassium tert-butanolate (t-BuOK, 0.36 mol). The mixture was stirred for 24 hours. Upon termination of the reaction, the reaction solution was poured into water, which produced a large white precipitate, which was collected by diafiltration. The precipitate was washed three times with ethanol and dried under vacuum at 60 °C for 24 h to give the white intermediate Tri-Br.

References

[1] Patent: CN104341311, 2016, B. Location in patent: Paragraph 0028; 0029; 0030
[2] Chinese Journal of Chemistry, 2015, vol. 33, # 8, p. 939 - 947

2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Preparation Products And Raw materials

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Preparation Products

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View Lastest Price from 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE manufacturers

Career Henan Chemical Co
Product
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE 18648-66-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2019-12-26

18648-66-3, 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENERelated Search:


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