2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE
- Product Name
- 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE
- CAS No.
- 18648-66-3
- Chemical Name
- 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE
- Synonyms
- 1,1-Diphenyl-2-(4-bromophenyl)ethene;2-(4-Bromophenyl)-1,1-diphenylethene;1-Bromo-4-(2,2-diphenylvinyl)benzene;2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE;1-Bromo-4-(2,2-diphenylethenyl)-benzene;2-(p-Bromophenyl)-1,1-diphenyl-ethylene;Benzene, 1-bromo-4-(2,2-diphenylethenyl)-;2-(4-Bromophenyl)-1,1-diphenylethylene >(2-(4-bromophenyl)ethene-1,1-diyl)dibenzene;1-(2-(4-Bromophenyl)-1-phenylvinyl)benzene ,98%
- CBNumber
- CB51479141
- Molecular Formula
- C20H15Br
- Formula Weight
- 335.24
- MOL File
- 18648-66-3.mol
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Property
- Melting point:
- 79 °C
- Boiling point:
- 404.4±14.0 °C(Predicted)
- Density
- 1.313±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Almost white
- InChI
- InChI=1S/C20H15Br/c21-19-13-11-16(12-14-19)15-20(17-7-3-1-4-8-17)18-9-5-2-6-10-18/h1-15H
- InChIKey
- HUCFDUOIMSRYAA-UHFFFAOYSA-N
- SMILES
- C1(Br)=CC=C(/C=C(/C2=CC=CC=C2)\C2=CC=CC=C2)C=C1
Safety
- HS Code
- 2903.99.8001
N-Bromosuccinimide Price
- Product number
- B3090
- Product name
- 2-(4-Bromophenyl)-1,1-diphenylethylene
- Packaging
- 5G
- Price
- $196
- Updated
- 2024/03/01
- Product number
- B3090
- Product name
- 2-(4-Bromophenyl)-1,1-diphenylethylene
- Packaging
- 25G
- Price
- $734
- Updated
- 2022/04/27
- Product number
- B700328
- Product name
- 2-(4-Bromophenyl)-1,1-diphenylethylene
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 090370
- Product name
- 2-(4-Bromophenyl)-1,1-diphenylethylene
- Purity
- 95+%
- Packaging
- 1g
- Price
- $152
- Updated
- 2021/12/16
- Product number
- 090370
- Product name
- 2-(4-Bromophenyl)-1,1-diphenylethylene
- Purity
- 95+%
- Packaging
- 5g
- Price
- $404
- Updated
- 2021/12/16
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Chemical Properties,Usage,Production
Synthesis
119-61-9
589-15-1
18648-66-3
General procedure for the synthesis of 2-(4-bromophenyl)-1,1-diphenylethylene from benzophenone and p-bromobenzyl bromide: 40.00 g of p-bromobenzyl bromide (0.16 mol) and 83.6 mL of triethyl phosphite (0.48 mol) were added to a 500 mL three-necked flask, and the reaction was heated under argon protection in an oil bath at 150 °C for 24 h with magnetic stirring, and then the reaction was The reaction was cooled to room temperature to obtain the Yerid reagent. To another three-necked flask was added 450 mL of tetrahydrofuran (THF) followed by 21.87 g of benzophenone (0.12 mol) and 40.39 g of potassium tert-butanolate (t-BuOK, 0.36 mol). The mixture was stirred for 24 hours. Upon termination of the reaction, the reaction solution was poured into water, which produced a large white precipitate, which was collected by diafiltration. The precipitate was washed three times with ethanol and dried under vacuum at 60 °C for 24 h to give the white intermediate Tri-Br.
References
[1] Patent: CN104341311, 2016, B. Location in patent: Paragraph 0028; 0029; 0030
[2] Chinese Journal of Chemistry, 2015, vol. 33, # 8, p. 939 - 947
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Preparation Products And Raw materials
Raw materials
Preparation Products
2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE Suppliers
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View Lastest Price from 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE manufacturers
- Product
- 2-(4-BROMOPHENYL)-1,1-DIPHENYLETHYLENE 18648-66-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-26