3-IODOINDAZOLE -5-CARBOXYLIC ACID
- Product Name
- 3-IODOINDAZOLE -5-CARBOXYLIC ACID
- CAS No.
- 885521-46-0
- Chemical Name
- 3-IODOINDAZOLE -5-CARBOXYLIC ACID
- Synonyms
- 3-Iodoindazole-5-carboxyl...;3-IODOINDAZOLE -5-CARBOXYLIC ACID;3-iodo-2H-indazole-5-carboxylic acid;3-Iodo-5-(1H)indazole carbocylic acid;1H-Indazole-5-carboxylic acid, 3-iodo-
- CBNumber
- CB51505752
- Molecular Formula
- C8H5IN2O2
- Formula Weight
- 288.04
- MOL File
- 885521-46-0.mol
3-IODOINDAZOLE -5-CARBOXYLIC ACID Property
- Boiling point:
- 512.1±30.0 °C(Predicted)
- Density
- 2.220±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 3.86±0.30(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- warning
- Hazard statements
-
H302Harmful if swallowed
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P330Rinse mouth.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- I706395
- Product name
- 3-Iodo-1H-indazole-5-carboxylicAcid
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4H21-H-04
- Product name
- 3-Iodo-1H-indazole-5-carboxylic acid
- Packaging
- 250mg
- Price
- $69
- Updated
- 2021/12/16
- Product number
- 4H21-H-04
- Product name
- 3-Iodo-1H-indazole-5-carboxylic acid
- Packaging
- 1g
- Price
- $239
- Updated
- 2021/12/16
- Product number
- 112271
- Product name
- 3-Iodoindazole-5-carboxylicacid
- Packaging
- 1g
- Price
- $262
- Updated
- 2021/12/16
- Product number
- HCH0044745
- Product name
- 3-IODO-5-(1H)INDAZOLE CARBOXYLIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.01
- Updated
- 2021/12/16
3-IODOINDAZOLE -5-CARBOXYLIC ACID Chemical Properties,Usage,Production
Synthesis
61700-61-6
885521-46-0
General procedure for the synthesis of 3-iodo-5-(1H)indazolecarboxylic acid from indazole-5-carboxylic acid hydrochloride: 1H-indazole-5-carboxylic acid (200 mg, 1.23 mmol), N,N-dimethylformamide (3 mL), potassium hydroxide (138 mg, 2.46 mmol), and iodine (470 mg, 1.85 mmol) were added to a 25 mL round bottomed flask. The reaction mixture was stirred at 25°C for 3 hours. After the reaction was completed, the reaction was quenched by adding 10 mL of Na2S2O3 solution. The pH of the reaction solution was adjusted with 10% hydrochloric acid solution to 6. The resulting solid was collected by filtration. Finally 300 mg (84% yield) of 3-iodo-1H-indazole-5-carboxylic acid was obtained as a white solid.
References
[1] Patent: WO2016/26549, 2016, A1. Location in patent: Page/Page column 91
3-IODOINDAZOLE -5-CARBOXYLIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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