6-(HYDROXYMETHYL)MORPHOLIN-3-ONE

Product Name: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE
CAS No.: 929019-95-4
Chemical Name: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE
Synonyms: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE;3-Morpholinone, 6-(hydroxymethyl)-;6-(Hydroxymethyl)morpholin-3-one - [H41263]
CBNumber: CB51517724
Molecular Formula: C5H9NO3
Formula Weight: 131.13
MOL File: 929019-95-4.mol

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6-(HYDROXYMETHYL)MORPHOLIN-3-ONE Property

Boiling point:: 397.1±27.0 °C(Predicted)
Density: 1?+-.0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 13.98±0.40(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A415390
Product name: 6-(Hydroxymethyl)morpholin-3-one
Packaging: 100mg
Price: $265
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0386224
Product name: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE
Purity: 95.00%
Packaging: 5MG
Price: $502.49
Updated: 2021/12/16

AK Scientific

Product number: 8252DK
Product name: 6-(Hydroxymethyl)morpholin-3-one
Packaging: 500mg
Price: $1136
Updated: 2021/12/16

Chemenu

Product number: CM163289
Product name: 6-(hydroxymethyl)morpholin-3-one
Purity: 95%
Packaging: 5g
Price: $1472
Updated: 2021/12/16

Ambeed

Product number: A303237
Product name: 6-(Hydroxymethyl)morpholin-3-one
Purity: 95%
Packaging: 100mg
Price: $77
Updated: 2021/12/16

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6-(HYDROXYMETHYL)MORPHOLIN-3-ONE Chemical Properties,Usage,Production

Synthesis

71064-34-1

929019-95-4

Step-2: Potassium tert-butoxide (23.4 g, 299.4 mmol) was dissolved in 200 mL of tert-amyl alcohol under nitrogen protection and stirred at room temperature. Subsequently, a solution of 2-chloro-N-(2,3-dihydroxypropyl)acetamide (Step-1 product of Intermediate-9) (20 g, 119.6 mmol) dissolved in 460 mL of tert-amyl alcohol was added to this solution and the reaction lasted for 2 hours. After 1 hour of reaction, methanol (100 mL) and water (3 mL) were added and stirring was continued for 20 minutes. Upon completion of the reaction, the reaction mixture was concentrated under vacuum and purified by rapid chromatography on silica gel using methanol/ethyl acetate (20:80) as eluent to afford 6-(hydroxymethyl)morpholin-3-one as a white solid (14.4 g). Mass spectral data: m/z 132.1.

References

[1] Patent: US2011/82138, 2011, A1. Location in patent: Page/Page column 80
[2] Patent: WO2012/120476, 2012, A1. Location in patent: Page/Page column 62
[3] Patent: US2013/345213, 2013, A1. Location in patent: Paragraph 0366
[4] Journal of Medicinal Chemistry, 2018, vol. 61, # 11, p. 4832 - 4850

6-(HYDROXYMETHYL)MORPHOLIN-3-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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6-(HYDROXYMETHYL)MORPHOLIN-3-ONE Suppliers

China 36 India 1 United States 3 Global 40

ForeChem (Nantong) Technology Co.,Ltd.

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View Lastest Price from 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE manufacturers

Nanjing jinheyou Trading Co., Ltd.

Product: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE 929019-95-4
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 20kg/month
Release date: 2019-11-19

Career Henan Chemical Co

Product: 6-(HYDROXYMETHYL)MORPHOLIN-3-ONE 929019-95-4
Price: US $5.00/KG
Min. Order: 1KG
Purity: 95%-98%
Supply Ability: 100kg
Release date: 2019-09-03

929019-95-4, 6-(HYDROXYMETHYL)MORPHOLIN-3-ONERelated Search:

(R )-6-Hydroxymethyl-morpholin-3-one 3-HYDROXYMETHYL-MORPHOLINE-4-CARBOXYLIC ACID TERT-BUTYL ESTER tert-Butyl (3R)-3-(hydroxymethyl)morpholine-4-carboxylate 3(S)-HYDROXYMETHYL-4-BOCMORPHOLINE (S)-6-Hydroxymethyl-morpholin-3-one

6-(HYDROXYMETHYL)MORPHOLIN-3-ONE

3-Morpholinone, 6-(hydroxymethyl)-

6-(Hydroxymethyl)morpholin-3-one - [H41263]

929019-95-4