ChemicalBook > CAS DataBase List > 4-chloro-3-iodobenzaldehyde

4-chloro-3-iodobenzaldehyde

Product Name
4-chloro-3-iodobenzaldehyde
CAS No.
276866-90-1
Chemical Name
4-chloro-3-iodobenzaldehyde
Synonyms
4-chloro-3-iodobenzaldehyde;4-dhloro-3-iodobenzaldehyde;Benzaldehyde, 4-chloro-3-iodo-
CBNumber
CB51559467
Molecular Formula
C7H4ClIO
Formula Weight
266.46
MOL File
276866-90-1.mol
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4-chloro-3-iodobenzaldehyde Property

Melting point:
117 °C
Boiling point:
304.0±27.0 °C(Predicted)
Density 
1.971±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
Appearance
White to off-white Solid
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Ark Pharm
Product number
AK177782
Product name
4-Chloro-3-iodobenzaldehyde
Purity
95+%
Packaging
1g
Price
$119
Updated
2021/12/16
SynQuest Laboratories
Product number
2615-M-06
Product name
4-Chloro-3-iodobenzaldehyde
Packaging
250mg
Price
$157
Updated
2021/12/16
AK Scientific
Product number
5972CS
Product name
4-Chloro-3-iodobenzaldehyde
Packaging
250mg
Price
$242
Updated
2021/12/16
SynQuest Laboratories
Product number
2615-M-06
Product name
4-Chloro-3-iodobenzaldehyde
Packaging
1g
Price
$336
Updated
2021/12/16
AK Scientific
Product number
5972CS
Product name
4-Chloro-3-iodobenzaldehyde
Packaging
5g
Price
$1327
Updated
2021/12/16
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4-chloro-3-iodobenzaldehyde Chemical Properties,Usage,Production

Synthesis

104-88-1

276866-90-1

The general procedure for the synthesis of 3-iodo-4-chlorobenzaldehyde from 4-chlorobenzaldehyde was as follows: iodine (1.12 g, 4.4 mmol) and sodium iodate (400 mg, 2.2 mmol) were added to a reaction vessel containing sulphuric acid (30 ml), and stirred at room temperature for 30 minutes. Subsequently, 4-chlorobenzaldehyde (1.40 g, 10.0 mmol) was added to the reaction mixture and stirring was continued for 1 hour at room temperature. After completion of the reaction, the reaction mixture was poured into ice water and the resulting solid was separated by filtration. After washing the solid with water to neutral, the solid was dissolved in ethanol and recrystallized to give 1.06 g (4.00 mmol, 40% yield) of 3-iodo-4-chlorobenzaldehyde.

References

[1] Bulletin of the Chemical Society of Japan, 2000, vol. 73, # 4, p. 951 - 956
[2] Tetrahedron, 2004, vol. 60, # 41, p. 9113 - 9119
[3] Synthesis, 2006, # 7, p. 1195 - 1199
[4] Patent: KR2016/149561, 2016, A. Location in patent: Paragraph 0125; 0126; 0127
[5] European Journal of Medicinal Chemistry, 2016, vol. 123, p. 180 - 190

4-chloro-3-iodobenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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4-chloro-3-iodobenzaldehyde Suppliers

Carbott PharmTech Inc.
Tel
0535-6385396
Fax
+86 (535) 638-9971
Email
info@carbottpharm.com
Country
China
ProdList
957
Advantage
56
SuZhou ShiYa Biopharmaceuticals, Inc.
Tel
86(512)5235 8471 17715136450
Fax
86(512)5235 6881
Email
sales@shiyabiopharm.com
Country
China
ProdList
4169
Advantage
58
Changzhou Anxuan Chemical, Co., Ltd.
Tel
13912302692 13912302692;
Fax
0519-88064678
Email
sales@anxuanchem.com
Country
China
ProdList
4828
Advantage
58
Hubei Chuangliankangcheng Pharmaceutical Co., Ltd.
Tel
027-65388397 18164111589
Fax
027-65388397
Email
3321478047@qq.com
Country
China
ProdList
2007
Advantage
55
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Capot Chemical Co.,Ltd.
Tel
+86-(0)57185586718; +8613336195806
Fax
+86-571-85864795
Email
sales@capot.com
Country
China
ProdList
29735
Advantage
60
Aikon International Limited
Tel
025-58859352 18068836627
Fax
02557626880
Email
sales01@aikonchem.com
Country
China
ProdList
16027
Advantage
58
Suzhou Xiya Pharmaceutical Co., Ltd.
Tel
0512-87819718 18912655635
Email
2587879032@qq.com
Country
China
ProdList
1403
Advantage
58
Cool Pharm, Ltd
Tel
021-58581007 18019463053
Fax
021-50966098
Email
sales@coolpharm.com
Country
China
ProdList
12878
Advantage
58
Henan Lien Chemical Products Co., Ltd.
Tel
03716091-9097 13383857418
Fax
03716091-9097
Email
1520689222@qq.com
Country
China
ProdList
4862
Advantage
58

276866-90-1, 4-chloro-3-iodobenzaldehydeRelated Search:


  • 4-chloro-3-iodobenzaldehyde
  • Benzaldehyde, 4-chloro-3-iodo-
  • 4-dhloro-3-iodobenzaldehyde
  • 276866-90-1