6-bromo-1-methyl-1H-indazol-3-amine
- Product Name
- 6-bromo-1-methyl-1H-indazol-3-amine
- CAS No.
- 1214899-85-0
- Chemical Name
- 6-bromo-1-methyl-1H-indazol-3-amine
- Synonyms
- 6-bromo-1-methylindazol-3-amine;6-bromo-1-methyl-1H-indazol-3-amine;3-Amino-6-bromo-1-methyl-1H-indazole;1H-Indazol-3-amine, 6-bromo-1-methyl-;Piperidine,1-(3-chloropropyl)-,hydrochloride(1:5)
- CBNumber
- CB51560139
- Molecular Formula
- C8H8BrN3
- Formula Weight
- 226.07
- MOL File
- 1214899-85-0.mol
6-bromo-1-methyl-1H-indazol-3-amine Property
- Boiling point:
- 378.4±22.0 °C(Predicted)
- Density
- 1.76±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 3.12±0.50(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C8H8BrN3/c1-12-7-4-5(9)2-3-6(7)8(10)11-12/h2-4H,1H3,(H2,10,11)
- InChIKey
- SJCNMXPRXAGVMK-UHFFFAOYSA-N
- SMILES
- N1(C)C2=C(C=CC(Br)=C2)C(N)=N1
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B808375
- Product name
- 6-Bromo-1-methyl-1H-indazol-3-amine
- Packaging
- 100mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- B808375
- Product name
- 6-Bromo-1-methyl-1H-indazol-3-amine
- Packaging
- 250mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- B808375
- Product name
- 6-Bromo-1-methyl-1H-indazol-3-amine
- Packaging
- 500mg
- Price
- $165
- Updated
- 2021/12/16
- Product number
- 3H30-9-Y3
- Product name
- 6-Bromo-1-methyl-1H-indazol-3-amine
- Packaging
- 250mg
- Price
- $63
- Updated
- 2021/12/16
- Product number
- 3H30-9-Y3
- Product name
- 6-Bromo-1-methyl-1H-indazol-3-amine
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
6-bromo-1-methyl-1H-indazol-3-amine Chemical Properties,Usage,Production
Synthesis
404827-77-6
74-88-4
1214899-85-0
Intermediate 3. Synthesis of 6-bromo-1-methyl-1H-indazol-3-amine: 6-bromo-1H-indazol-3-amine (788 mg, 3.71 mmol) was dissolved in dimethylformamide (3 mL) and cooled to 0 °C. Sodium hydride (60% oil dispersion; 163 mg, 6.79 mmol) was added in batches under stirring. The reaction mixture was continued to be stirred at 0 °C for 30 min. Subsequently, iodomethane (225 μL, 4.09 mmol) was added dropwise to the mixture and the reaction was stirred for 2 h at room temperature. Upon completion of the reaction, water was added to the crude reaction mixture and a red solid was precipitated. The solid was collected by filtration and dried to afford the title compound in 80% yield. The product was analyzed by LRMS showing m/z: 226 (M)+, 228 (M + 2)+. 1H NMR (300 MHz, DMSO-d6) δ ppm: 3.75 (s, 3H); 5.7 (s, 2H); 7.01 (d, 1H); 7.59 (d, 1H); 7.6 (s, 1H).
References
[1] Patent: WO2016/150971, 2016, A1. Location in patent: Page/Page column 23
6-bromo-1-methyl-1H-indazol-3-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-bromo-1-methyl-1H-indazol-3-amine manufacturers
- Product
- 6-bromo-1-methyl-1H-indazol-3-amine 1214899-85-0
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-02
- Product
- 6-bromo-1-methyl-1H-indazol-3-amine 1214899-85-0
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200KG
- Release date
- 2020-02-20