7-NITRO-QUINOLINE

Product Name: 7-NITRO-QUINOLINE
CAS No.: 613-51-4
Chemical Name: 7-NITRO-QUINOLINE
Synonyms: AKOS 212-55;7-Nitroquinolint;7-NITRO-QUINOLINE;Quinoline, 7-nitro-;7-Nitro-tetrahydroquinoline
CBNumber: CB5170207
Molecular Formula: C9H6N2O2
Formula Weight: 174.16
MOL File: 613-51-4.mol

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7-NITRO-QUINOLINE Property

Melting point:: 132.5°C
Boiling point:: 305.12°C (rough estimate)
Density: 1.2190 (estimate)
refractive index: 1.6820 (rough estimate)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 1.25±0.14(Predicted)
color: Light yellow to yellow
InChI: InChI=1S/C9H6N2O2/c12-11(13)8-4-3-7-2-1-5-10-9(7)6-8/h1-6H
InChIKey: MXKZSCXYMSXOAO-UHFFFAOYSA-N
SMILES: N1C2C(=CC=C([N+]([O-])=O)C=2)C=CC=1

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: N900668
Product name: 7-Nitroquinoline
Packaging: 500mg
Price: $110
Updated: 2021/12/16

ChemScene

Product number: CS-W002561
Product name: 7-Nitroquinoline
Purity: 99.79%
Packaging: 10g
Price: $98
Updated: 2021/12/16

AK Scientific

Product number: J90674
Product name: 7-Nitroquinoline
Packaging: 1g
Price: $40
Updated: 2021/12/16

ChemScene

Product number: CS-W002561
Product name: 7-Nitroquinoline
Purity: 99.79%
Packaging: 5g
Price: $59
Updated: 2021/12/16

ChemScene

Product number: CS-W002561
Product name: 7-Nitroquinoline
Purity: 99.79%
Packaging: 25g
Price: $196
Updated: 2021/12/16

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7-NITRO-QUINOLINE Chemical Properties,Usage,Production

Synthesis

30450-62-5

613-51-4

7-Nitro-1,2,3,4-tetrahydroquinoline (60 g, 0.337 mol) was used as raw material and dissolved in dichloromethane (4.5 L). Dichlorodicyanobenzoquinone (152.9 g, 0.6734 mol) was added in batches at room temperature and the reaction was stirred for 1 hour. After completion of the reaction, filtration was carried out and the filter cake was washed with dichloromethane (500 mL x 2) and stirred for 5 min each time before filtration again. The organic phases were combined and washed sequentially with 10% sodium hydroxide solution (500 mL x 2) and saturated sodium chloride solution (500 mL). The organic phase was dried over anhydrous sodium sulfate and concentrated to dryness under reduced pressure. The resulting orange solid was stirred with a solvent mixture of petroleum ether:ethyl acetate (5:1, 250 mL) for 30 min, and 7-nitroquinoline (53 g, 90.3% yield) was obtained after filtration.

References

[1] Chemistry - A European Journal, 2017, vol. 23, # 57, p. 14167 - 14172
[2] Synthetic Communications, 2018, vol. 48, # 11, p. 1291 - 1298
[3] Angewandte Chemie - International Edition, 2018, vol. 57, # 35, p. 11262 - 11266
[4] Angew. Chem., 2018, vol. 130, # 35, p. 11432 - 11436,5
[5] Patent: CN107353245, 2017, A. Location in patent: Paragraph 0017; 0018

7-NITRO-QUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-NITRO-QUINOLINE Suppliers

China 107 Germany 4 India 2 The Netherlands 1 United States 11 Global 125

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View Lastest Price from 7-NITRO-QUINOLINE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 7-NITRO-QUINOLINE 613-51-4
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-12

Career Henan Chemical Co

Product: 7-NITRO-QUINOLINE 613-51-4
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-08-31

613-51-4, 7-NITRO-QUINOLINERelated Search:

7-NITRO-QUINOLINE 6-BROMO-5-NITROQUINOLINE 7-METHYL-8-NITROQUINOLINE 1,2,3,4-Tetrahydroquinoline 7-Nitro-1,2,3,4-tetrahydroquinoline Nitroxoline 4-Chloro-1-methyl-3-nitro-1H-quinolin-2-one 5-Amino-6-nitroquinoline 6-CHLORO-5-NITROQUINOLINE 4-Isobutylamino-3-Nitro-Quinoline 6-Nitro Quinoline - 50g 2-CHLORO-6-NITROQUINOLINE 8-BROMO-5-NITROQUINOLINE 4-NITROQUINOLINE N-OXIDE 2-NITROQUINOLINE 6-METHOXY-8-NITROQUINOLINE 4-NITROQUINOLINE 4-AMINO-3-NITROQUINOLINE

7-NITRO-QUINOLINE

7-Nitro-tetrahydroquinoline

AKOS 212-55

Quinoline, 7-nitro-

7-Nitroquinolint

613-51-4