7-NITRO-QUINOLINE
- Product Name
- 7-NITRO-QUINOLINE
- CAS No.
- 613-51-4
- Chemical Name
- 7-NITRO-QUINOLINE
- Synonyms
- AKOS 212-55;7-Nitroquinolint;7-NITRO-QUINOLINE;Quinoline, 7-nitro-;7-Nitro-tetrahydroquinoline
- CBNumber
- CB5170207
- Molecular Formula
- C9H6N2O2
- Formula Weight
- 174.16
- MOL File
- 613-51-4.mol
7-NITRO-QUINOLINE Property
- Melting point:
- 132.5°C
- Boiling point:
- 305.12°C (rough estimate)
- Density
- 1.2190 (estimate)
- refractive index
- 1.6820 (rough estimate)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- pka
- 1.25±0.14(Predicted)
- color
- Light yellow to yellow
- InChI
- InChI=1S/C9H6N2O2/c12-11(13)8-4-3-7-2-1-5-10-9(7)6-8/h1-6H
- InChIKey
- MXKZSCXYMSXOAO-UHFFFAOYSA-N
- SMILES
- N1C2C(=CC=C([N+]([O-])=O)C=2)C=CC=1
Safety
- HS Code
- 2933499090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- N900668
- Product name
- 7-Nitroquinoline
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- J90674
- Product name
- 7-Nitroquinoline
- Packaging
- 1g
- Price
- $40
- Updated
- 2021/12/16
- Product number
- CS-W002561
- Product name
- 7-Nitroquinoline
- Purity
- 99.79%
- Packaging
- 5g
- Price
- $59
- Updated
- 2021/12/16
- Product number
- CS-W002561
- Product name
- 7-Nitroquinoline
- Purity
- 99.79%
- Packaging
- 10g
- Price
- $98
- Updated
- 2021/12/16
- Product number
- CS-W002561
- Product name
- 7-Nitroquinoline
- Purity
- 99.79%
- Packaging
- 25g
- Price
- $196
- Updated
- 2021/12/16
7-NITRO-QUINOLINE Chemical Properties,Usage,Production
Synthesis
30450-62-5
613-51-4
7-Nitro-1,2,3,4-tetrahydroquinoline (60 g, 0.337 mol) was used as raw material and dissolved in dichloromethane (4.5 L). Dichlorodicyanobenzoquinone (152.9 g, 0.6734 mol) was added in batches at room temperature and the reaction was stirred for 1 hour. After completion of the reaction, filtration was carried out and the filter cake was washed with dichloromethane (500 mL x 2) and stirred for 5 min each time before filtration again. The organic phases were combined and washed sequentially with 10% sodium hydroxide solution (500 mL x 2) and saturated sodium chloride solution (500 mL). The organic phase was dried over anhydrous sodium sulfate and concentrated to dryness under reduced pressure. The resulting orange solid was stirred with a solvent mixture of petroleum ether:ethyl acetate (5:1, 250 mL) for 30 min, and 7-nitroquinoline (53 g, 90.3% yield) was obtained after filtration.
References
[1] Chemistry - A European Journal, 2017, vol. 23, # 57, p. 14167 - 14172
[2] Synthetic Communications, 2018, vol. 48, # 11, p. 1291 - 1298
[3] Angewandte Chemie - International Edition, 2018, vol. 57, # 35, p. 11262 - 11266
[4] Angew. Chem., 2018, vol. 130, # 35, p. 11432 - 11436,5
[5] Patent: CN107353245, 2017, A. Location in patent: Paragraph 0017; 0018
7-NITRO-QUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
7-NITRO-QUINOLINE Suppliers
- Tel
- --
- Fax
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- info@chemsworth.com
- Country
- India
- ProdList
- 6700
- Advantage
- 30
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 7-NITRO-QUINOLINE manufacturers
- Product
- 7-NITRO-QUINOLINE 613-51-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-12
- Product
- 7-NITRO-QUINOLINE 613-51-4
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-08-31