ChemicalBook > CAS DataBase List > N-BUTYL-2-CHLORO-ACETAMIDE

N-BUTYL-2-CHLORO-ACETAMIDE

Product Name: N-BUTYL-2-CHLORO-ACETAMIDE
CAS No.: 5349-24-6
Chemical Name: N-BUTYL-2-CHLORO-ACETAMIDE
Synonyms: TIMTEC-BB SBB010319;N-BUTYL-2-CHLORACETAMIDE;ASINEX-REAG BAS 02927056;N-BUTYL-2-CHLORO-ACETAMIDE;N-butyl-2-chloro-ethanamide;Acetamide, N-butyl-2-chloro-
CBNumber: CB5177802
Molecular Formula: C6H12ClNO
Formula Weight: 149.62
MOL File: 5349-24-6.mol

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N-BUTYL-2-CHLORO-ACETAMIDE Property

Melting point:: 96.5 °C(Solv: benzene (71-43-2))
Boiling point:: 110 °C(Press: 7.0 Torr)
Density: 1.032±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 14.38±0.46(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2924297099

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 018561
Product name: N-Butyl-2-chloro-acetamide
Packaging: 500mg
Price: $182
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0026847
Product name: N-BUTYL-2-CHLORO-ACETAMIDE
Purity: 95.00%
Packaging: 500MG
Price: $777.32
Updated: 2021/12/16

AK Scientific

Product number: W6790
Product name: N-Butyl-2-chloro-acetamide
Packaging: 25g
Price: $847
Updated: 2021/12/16

Ambeed

Product number: A225554
Product name: N-Butyl-2-chloroacetamide
Purity: 97%
Packaging: 250mg
Price: $26
Updated: 2021/12/16

Ambeed

Product number: A225554
Product name: N-Butyl-2-chloroacetamide
Purity: 97%
Packaging: 1g
Price: $64
Updated: 2021/12/16

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N-BUTYL-2-CHLORO-ACETAMIDE Chemical Properties,Usage,Production

Synthesis

109-73-9

79-04-9

5349-24-6

GENERAL STEPS: Chloroacetyl chloride (0.2 mol, 15.9 mL, CAS: 79-04-9) was slowly added dropwise to a solution of dichloromethane (50 mL) containing n-butylamine (0.2 mol, 14.83 g) in an ice bath. After the dropwise addition, 20% NaOH aqueous solution was added and the reaction mixture was warmed up to room temperature and stirring was continued for 2 hours. After completion of the reaction, the organic phase was separated and washed sequentially with 5% aqueous HCl and 5% aqueous NaHCO3 (3 x 25 mL each). The organic phase was dried and filtered, and then the solvent was removed by distillation under reduced pressure to give the intermediate N-butyl-2-chloroacetamide (92% yield). Subsequently, the intermediate (0.05 mol, 9.00 g) was mixed with 5,6,7,8-tetrahydropyrido[1,2-α]imidazole (0.05 mol, 6.11 g, CAS: 34167-66-3) in acetonitrile (50 mL) and the reaction was carried out at reflux for 18 hours. The reaction solution was recrystallized by ethyl acetate recrystallization operation to give the product [4C-imCH2CONHBu]Cl (89% yield). Finally, [4C-imCH2CONHBu]OH was obtained by treatment with anion exchange resin.

References

[1] Patent: CN104326949, 2016, B. Location in patent: Paragraph 0060; 0061; 0063
[2] Patent: WO2007/9083, 2007, A2. Location in patent: Page/Page column 68
[3] ACS Medicinal Chemistry Letters, 2017, vol. 8, # 6, p. 678 - 681
[4] ChemMedChem, 2018,
[5] Organic Letters, 2004, vol. 6, # 26, p. 4805 - 4808

N-BUTYL-2-CHLORO-ACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N-BUTYL-2-CHLORO-ACETAMIDE manufacturers

Career Henan Chemical Co

Product: N-BUTYL-2-CHLORO-ACETAMIDE 5349-24-6
Price: US $1.00/g
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-09

5349-24-6, N-BUTYL-2-CHLORO-ACETAMIDERelated Search:

N,N'-OCTAMETHYLENEBIS(DICHLOROACETAMIDE) CHLOROACETYL-DL-ISOLEUCINE CHLOROACETYL-L-LEUCINE CHLOROAC-ILE-OH N-CHLOROACETYLSUCCINIMIDE 2-CHLORO-N-CYCLOHEXYL-N-METHYLACETAMIDE 2-CHLORO-N-CYCLOHEXYL-ACETAMIDE CHLOROACETYL-DL-NORLEUCINE CHLOROAC-PRO-OH N-(6-AMINO-1-BUTYL-2,4-DIOXO-1,2,3,4-TETRAHYDRO-PYRIMIDIN-5-YL)-N-BUTYL-2-CHLORO-ACETAMIDE 4-(2-CHLOROACETAMIDO)-2,2,6,6-TETRAMETHYLPIPERIDINE 1-OXYL CHLOROAC-DL-NVA-OH CHLOROACETYL-DL-LEUCINE 2-CHLORO-N-HEXYLACETAMIDE 2-CHLORO-N-PENTYLACETAMIDE N,N-dibutyl-2-chloroacetamide 2-CHLORO-N-(1-METHYLHEXYL)ACETAMIDE 1-BUTYL-3-CHLORO-3-PHENYL-1,2,3,4-TETRAHYDROQUINOLINE-2,4-DIONE

ASINEX-REAG BAS 02927056

N-BUTYL-2-CHLORO-ACETAMIDE

TIMTEC-BB SBB010319

N-BUTYL-2-CHLORACETAMIDE

N-butyl-2-chloro-ethanamide

Acetamide, N-butyl-2-chloro-

5349-24-6