ChemicalBook > CAS DataBase List > 4-(4-NITROBENZYL)MORPHOLINE

4-(4-NITROBENZYL)MORPHOLINE

Product Name: 4-(4-NITROBENZYL)MORPHOLINE
CAS No.: 6425-46-3
Chemical Name: 4-(4-NITROBENZYL)MORPHOLINE
Synonyms: BUTTPARK 96\57-67;4-(4-NITROBENZYL)MORPHOLINE;4-(4-Nitrobenzyl)morpholine,97%;4-(4-NITROBENZYL)MORPHOLINE 95%;4-[(4-nitrophenyl)Methyl]Morpholine;Morpholine, 4-[(4-nitrophenyl)Methyl]-;4-[(4-nitrophenyl)methyl]morpholin-4-ium
CBNumber: CB5178218
Molecular Formula: C11H14N2O3
Formula Weight: 222.24
MOL File: 6425-46-3.mol

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4-(4-NITROBENZYL)MORPHOLINE Property

Melting point:: 79.6-80 °C
Boiling point:: 349.4±27.0 °C(Predicted)
Density: 1.243±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 5.82±0.10(Predicted)

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Safety

Hazard Codes: C
Risk Statements: 34
Safety Statements: 36/37/39-26-22
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 071887
Product name: 4-(4-Nitrobenzyl)morpholine
Purity: 95+%
Packaging: 1g
Price: $70
Updated: 2021/12/16

AK Scientific

Product number: W7600
Product name: 4-(4-Nitrobenzyl)morpholine
Packaging: 1g
Price: $71
Updated: 2021/12/16

Apolloscientific

Product number: OR110998
Product name: 4-(4-Nitrobenzyl)morpholine
Packaging: 1g
Price: $95
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-9Z
Product name: 4-(4-Nitrobenzyl)morpholine
Packaging: 1g
Price: $104
Updated: 2021/12/16

Apolloscientific

Product number: OR110998
Product name: 4-(4-Nitrobenzyl)morpholine
Packaging: 5g
Price: $145
Updated: 2021/12/16

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4-(4-NITROBENZYL)MORPHOLINE Chemical Properties,Usage,Production

Chemical Properties

yellow-orange to orange crystalline powder

Synthesis

110-91-8

100-11-8

6425-46-3

General steps: 1. 4-Nitrobenzyl bromide (72.084 g) and dichloromethane (470 mL, dried over molecular sieves) were added to a reaction flask under argon protection and stirred until completely dissolved. 2. Anhydrous potassium carbonate (91.909 g) was added as a base. 3. The reaction mixture was cooled in an ice bath for 20 minutes. 4. Slowly add morpholine dropwise (completion of dropwise addition in about 30 minutes). 5. After completion of the dropwise addition, the ice bath was removed and the reaction mixture was stirred at room temperature overnight. 6. Upon completion of the reaction, the reaction was quenched by the addition of water (150 mL). 7. The pH of the reaction mixture was adjusted to 4-5 with 5% aqueous citric acid. 8. After standing and layering, the organic phase was separated and washed once with deionized water (260 mL). 9. The organic phase was dried with anhydrous magnesium sulfate for 30 minutes, followed by filtration. 10. The filtrate was concentrated and dried under reduced pressure by an oil pump to afford 4-(4-nitrobenzyl)morpholine (71.9 g, 97.16% yield).

References

[1] Journal of Medicinal Chemistry, 2013, vol. 56, # 7, p. 2975 - 2990
[2] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010, vol. 49, # 6, p. 771 - 775
[3] Patent: EP2824108, 2015, A1. Location in patent: Paragraph 0101
[4] Patent: US2015/166595, 2015, A1. Location in patent: Paragraph 0219
[5] Patent: CN106432235, 2017, A. Location in patent: Paragraph 0089; 0090

4-(4-NITROBENZYL)MORPHOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-(4-NITROBENZYL)MORPHOLINE manufacturers

Career Henan Chemical Co

Product: 4-(4-NITROBENZYL)MORPHOLINE 6425-46-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10t
Release date: 2019-12-20

6425-46-3, 4-(4-NITROBENZYL)MORPHOLINERelated Search:

4-(4-[(4-METHYLPHENYL)SULFANYL]-3-NITROBENZYL)MORPHOLINE 4-(2-NITROBENZYL)MORPHOLINE 4-(4-[(4-CHLOROPHENYL)SULFANYL]-3-NITROBENZYL)MORPHOLINE 4-(3-NITROBENZYL)MORPHOLINE 4-[(4-METHYLPIPERAZIN-1-YL)METHYL]BENZALDEHYDE 3-FLUORO-4'-NITRO BENZYL MORPHOLINE MORPHOLINO(4-NITROPHENYL)METHANONE 4-(3-FLUORO-4-NITROBENZYL)MORPHOLINE (3-([(4-CHLOROPHENYL)SULFONYL]METHYL)-4-NITROPHENYL)(MORPHOLINO)METHANONE 2,4,6-TRINITROBENZOIC MORPHOLIDE MORPHOLIN-4-YL-(4-NITRO-PHENYL)-ACETIC ACID HYDROCHLORIDE 4-(4-NITROBENZYL)MORPHOLINE

4-[(4-nitrophenyl)Methyl]Morpholine

Morpholine, 4-[(4-nitrophenyl)Methyl]-

4-(4-NITROBENZYL)MORPHOLINE

BUTTPARK 96\57-67

4-(4-NITROBENZYL)MORPHOLINE 95%

4-(4-Nitrobenzyl)morpholine,97%

4-[(4-nitrophenyl)methyl]morpholin-4-ium

6425-46-3