N-(6-aminopyridin-2-yl)acetamide
- Product Name
- N-(6-aminopyridin-2-yl)acetamide
- CAS No.
- 1075-62-3
- Chemical Name
- N-(6-aminopyridin-2-yl)acetamide
- Synonyms
- N-ACETYL-1,6-DIAMINOPYRIDINE;2-acetylamino-6-aminopyridine;N-(6-Aminopyridin-2-yl)acetamid;2-Acetamido-6-aminopyridine >N-(6-aminopyridin-2-yl)acetamide;N-(6-AMINO-2-PYRIDINYL)-ACETAMIDE;AcetaMide, N-(6-aMino-2-pyridinyl)-;N-(6-aminopyridin-2-yl)acetamide ISO 9001：2015 REACH
- CBNumber
- CB51991904
- Molecular Formula
- C7H9N3O
- Formula Weight
- 151.17
- MOL File
- 1075-62-3.mol
N-(6-aminopyridin-2-yl)acetamide Property
- Melting point:
- 158.0 to 162.0 °C
- Boiling point:
- 419.4±30.0 °C(Predicted)
- Density
- 1.280±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- soluble in Methanol
- form
- powder to crystal
- pka
- 13.52±0.70(Predicted)
- color
- White to Almost white
Safety
- HS Code
- 2933.39.9200
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
N-Bromosuccinimide Price
- Product number
- A2707
- Product name
- 2-Acetamido-6-aminopyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $96
- Updated
- 2025/07/31
- Product number
- A2707
- Product name
- 2-Acetamido-6-aminopyridine
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $313
- Updated
- 2024/03/01
- Product number
- A168353
- Product name
- 2-Acetamido-6-aminopyridine
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FA150997
- Product name
- N-Acetyl-1,6-diaminopyridine
- Packaging
- 100mg
- Price
- $81
- Updated
- 2021/12/16
- Product number
- 1571AA
- Product name
- N-(6-Aminopyridin-2-yl)acetamide
- Packaging
- 10g
- Price
- $154
- Updated
- 2021/12/16
N-(6-aminopyridin-2-yl)acetamide Chemical Properties,Usage,Production
Synthesis
141-86-6
75-36-5
1075-62-3
GENERAL STEPS: Preparation of N-(6-aminopyridin-2-yl)acetamide; 2,6-diaminopyridine (9.822 g, 90 mmol) was dissolved in dioxane (100 mL) and cooled to 0 °C. Acetyl chloride (2.355 g, 2.1 mL, 30 mmol) was added slowly dropwise and stirred at 0 °C for 1 hour. The ice bath was removed and the reaction mixture was allowed to stir overnight at room temperature. Upon completion of the reaction, the reaction was quenched with saturated NaHCO3 solution and subsequently extracted three times with ethyl acetate. The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated under reduced pressure to give the crude product. Purification by silica gel column chromatography using 60-70% ethyl acetate/hexane gradient elution afforded the target compound N-(6-aminopyridin-2-yl)acetamide (3.45 g, 76% yield). Mass spectrum (ESI-MS): m/z = 152.1 [M+H]+; 1H NMR (CDCl3, ppm): δ 7.49 (m, 3H), 6.28 (d, 1H), 4.31 (s, br, 2H), 2.19 (s, 3H).
References
[1] Journal of Organic Chemistry, 2014, vol. 79, # 2, p. 711 - 719
[2] Patent: WO2005/35499, 2005, A1. Location in patent: Page/Page column 46
[3] Journal of the American Chemical Society, 2016, vol. 138, # 50, p. 16228 - 16231
[4] Journal of the American Chemical Society, 1947, vol. 69, p. 1147,1148
N-(6-aminopyridin-2-yl)acetamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-(6-aminopyridin-2-yl)acetamide manufacturers
- Product
- N-(6-Aminopyridin-2-yl)acetamid 1075-62-3
- Price
- US $8.80-1.10/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 500kg
- Release date
- 2025-09-16
- Product
- N-(6-aminopyridin-2-yl)acetamide 1075-62-3
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-02-24
- Product
- N-(6-aminopyridin-2-yl)acetamide 1075-62-3
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-02-24