ChemicalBook > CAS DataBase List > 5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE

5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE

Product Name: 5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE
CAS No.: 96799-04-1
Chemical Name: 5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE
Synonyms: 3-Amino-5-(3-methoxyphenyl)-1H-pyrazole;1H-Pyrazol-3-amine, 5-(3-methoxyphenyl)-;3-(3-Methoxy-phenyl)-2H-pyrazol-3-ylamine;5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE;[5-(3-methoxyphenyl)-1H-pyrazol-3-yl]amine;3-(3-methoxyphenyl)-1H-pyrazol-5-amine 1HCl;JR-13696, 3-(3-Methoxyphenyl)-1H-pyrazol-5-amine, 96%;3-(3-methoxyphenyl)-1H-pyrazol-5-amine(SALTDATA: HCl)
CBNumber: CB5219256
Molecular Formula: C10H11N3O
Formula Weight: 189.21
MOL File: 96799-04-1.mol

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5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE Property

Boiling point:: 456.7±35.0 °C(Predicted)
Density: 1.240±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 14.54±0.10(Predicted)

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Safety

Hazard Codes: Xn
Risk Statements: 22

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M350200
Product name: 3-(3-Methoxyphenyl)-1H-pyrazol-5-amine
Packaging: 50mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 075822
Product name: 5-(3-Methoxyphenyl)-2H-pyrazol-3-ylamine
Purity: 95+%
Packaging: 1g
Price: $347
Updated: 2021/12/16

AK Scientific

Product number: W9817
Product name: 5-(3-Methoxyphenyl)-2H-pyrazol-3-ylamine
Packaging: 5g
Price: $212
Updated: 2021/12/16

Matrix Scientific

Product number: 075822
Product name: 5-(3-Methoxyphenyl)-2H-pyrazol-3-ylamine
Purity: 95+%
Packaging: 5g
Price: $958
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0068738
Product name: 1H-PYRAZOL-3-AMINE, 5-(3-METHOXYPHENYL)-
Purity: 95.00%
Packaging: 1G
Price: $958.65
Updated: 2021/12/16

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5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE Chemical Properties,Usage,Production

Synthesis

21667-60-7

96799-04-1

b) Synthesis of 5-(3-methoxyphenyl)-2H-pyrazol-3-amine To a solution of 3-(3-methoxyphenyl)-3-oxopropanenitrile (8.96 mmol) in anhydrous ethanol (20 mL) was added hydrazine monohydrate (0.52 mL, 15 mmol), and the reaction mixture was heated and refluxed for 18 hours. After completion of the reaction, the mixture was cooled to room temperature and concentrated under reduced pressure to remove the solvent. The crude product was washed with ether and filtered to give 1.4 g of the title compound in 83% yield. Product Characterization: Molecular formula: C10H11N3O Theoretical mass-to-charge ratio (m/z): 189 Measured mass-to-charge ratio (m/z): [M + H+] = 190 Liquid chromatography retention time (LC Rt): 1.13 min (5 min method) 1H-NMR (400 MHz, MeOH-d4) δ: 3.82 (3H, s, OCH3); 5.93 (1H, s, CH); 6.86-6.88 (1H, m, ArH); 7.19-7.31 (3H, m, ArH).

References

[1] Patent: WO2008/87529, 2008, A1. Location in patent: Page/Page column 105
[2] Patent: WO2010/9290, 2010, A1. Location in patent: Page/Page column 136
[3] Patent: WO2007/98826, 2007, A2. Location in patent: Page/Page column 71
[4] Beilstein Journal of Organic Chemistry, 2018, vol. 14, p. 122 - 1228
[5] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 22, p. 7501 - 7511

5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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96799-04-1, 5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINERelated Search:

5-(3-METHOXY-PHENYL)-2H-PYRAZOL-3-YLAMINE

3-Amino-5-(3-methoxyphenyl)-1H-pyrazole

1H-Pyrazol-3-amine, 5-(3-methoxyphenyl)-

3-(3-methoxyphenyl)-1H-pyrazol-5-amine(SALTDATA: HCl)

3-(3-methoxyphenyl)-1H-pyrazol-5-amine 1HCl

[5-(3-methoxyphenyl)-1H-pyrazol-3-yl]amine

JR-13696, 3-(3-Methoxyphenyl)-1H-pyrazol-5-amine, 96%

3-(3-Methoxy-phenyl)-2H-pyrazol-3-ylamine

96799-04-1