ChemicalBook > CAS DataBase List > 2-CHLORO-6-METHOXY-BENZALDEHYDE

2-CHLORO-6-METHOXY-BENZALDEHYDE

Product Name
2-CHLORO-6-METHOXY-BENZALDEHYDE
CAS No.
29866-54-4
Chemical Name
2-CHLORO-6-METHOXY-BENZALDEHYDE
Synonyms
2-CHLORO-6-METHOXY-BENZALDEHYDE;Benzaldehyde, 2-chloro-6-methoxy-
CBNumber
CB5224779
Molecular Formula
C8H7ClO2
Formula Weight
170.59
MOL File
29866-54-4.mol
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2-CHLORO-6-METHOXY-BENZALDEHYDE Property

Melting point:
56-58 °C
Boiling point:
263.1±20.0 °C(Predicted)
Density 
1.244±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
White to yellow Solid
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Safety

HS Code 
2913000090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C381718
Product name
2-Chloro-6-methoxybenzaldehyde
Packaging
50mg
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
073265
Product name
2-Chloro-6-methoxybenzaldehyde
Purity
95+%
Packaging
1g
Price
$39
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC51944
Product name
2-Chloro-6-methoxy-benzaldehyde
Packaging
500mg
Price
$50
Updated
2021/12/16
Matrix Scientific
Product number
073265
Product name
2-Chloro-6-methoxybenzaldehyde
Purity
95+%
Packaging
5g
Price
$109
Updated
2021/12/16
Matrix Scientific
Product number
073265
Product name
2-Chloro-6-methoxybenzaldehyde
Purity
95+%
Packaging
10g
Price
$179
Updated
2021/12/16
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2-CHLORO-6-METHOXY-BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

387-45-1

29866-54-4

Preparation of Example 12: 2-Chloro-6-fluorobenzaldehyde (51.5 g, 0.30 mol) was dissolved in 500 mL of methanol. Sodium hydroxide (14.4 g, 0.35 mol) was added to the solution and the reaction mixture was stirred and heated to reflux for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the volume was concentrated to about 200 mL by vacuum distillation. Subsequently, water (400 mL) and dichloromethane (200 mL) were added to the concentrate to form a two-phase system. The organic phase was separated and the aqueous phase was extracted twice with dichloromethane (100 mL each). All organic layers were combined, dried with anhydrous sodium sulfate, filtered and the dichloromethane was removed by distillation under atmospheric pressure. The solvent was replaced with hexane (450 mL) to a final volume of 300 mL. The product was initially present as an oil and began to crystallize at 45°C. The mixture was cooled to room temperature, allowed to stand for 16 hours for granulation, and then filtered to give 2-chloro-6-methoxybenzaldehyde [35.6 g, 64.2% yield; Rf 0.2 (CHCl3)].

References

[1] Patent: US4367234, 1983, A

2-CHLORO-6-METHOXY-BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-6-METHOXY-BENZALDEHYDE Suppliers

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View Lastest Price from 2-CHLORO-6-METHOXY-BENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
2-CHLORO-6-METHOXY-BENZALDEHYDE 29866-54-4
Price
US $6.60/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg -1000kg
Release date
2020-01-02