2-CHLORO-6-METHOXY-BENZALDEHYDE
- Product Name
- 2-CHLORO-6-METHOXY-BENZALDEHYDE
- CAS No.
- 29866-54-4
- Chemical Name
- 2-CHLORO-6-METHOXY-BENZALDEHYDE
- Synonyms
- 2-CHLORO-6-METHOXY-BENZALDEHYDE;Benzaldehyde, 2-chloro-6-methoxy-
- CBNumber
- CB5224779
- Molecular Formula
- C8H7ClO2
- Formula Weight
- 170.59
- MOL File
- 29866-54-4.mol
2-CHLORO-6-METHOXY-BENZALDEHYDE Property
- Melting point:
- 56-58 °C
- Boiling point:
- 263.1±20.0 °C(Predicted)
- Density
- 1.244±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C381718
- Product name
- 2-Chloro-6-methoxybenzaldehyde
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 073265
- Product name
- 2-Chloro-6-methoxybenzaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $39
- Updated
- 2021/12/16
- Product number
- FC51944
- Product name
- 2-Chloro-6-methoxy-benzaldehyde
- Packaging
- 500mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- 073265
- Product name
- 2-Chloro-6-methoxybenzaldehyde
- Purity
- 95+%
- Packaging
- 5g
- Price
- $109
- Updated
- 2021/12/16
- Product number
- 073265
- Product name
- 2-Chloro-6-methoxybenzaldehyde
- Purity
- 95+%
- Packaging
- 10g
- Price
- $179
- Updated
- 2021/12/16
2-CHLORO-6-METHOXY-BENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
387-45-1
29866-54-4
Preparation of Example 12: 2-Chloro-6-fluorobenzaldehyde (51.5 g, 0.30 mol) was dissolved in 500 mL of methanol. Sodium hydroxide (14.4 g, 0.35 mol) was added to the solution and the reaction mixture was stirred and heated to reflux for 3 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the volume was concentrated to about 200 mL by vacuum distillation. Subsequently, water (400 mL) and dichloromethane (200 mL) were added to the concentrate to form a two-phase system. The organic phase was separated and the aqueous phase was extracted twice with dichloromethane (100 mL each). All organic layers were combined, dried with anhydrous sodium sulfate, filtered and the dichloromethane was removed by distillation under atmospheric pressure. The solvent was replaced with hexane (450 mL) to a final volume of 300 mL. The product was initially present as an oil and began to crystallize at 45°C. The mixture was cooled to room temperature, allowed to stand for 16 hours for granulation, and then filtered to give 2-chloro-6-methoxybenzaldehyde [35.6 g, 64.2% yield; Rf 0.2 (CHCl3)].
References
[1] Patent: US4367234, 1983, A
2-CHLORO-6-METHOXY-BENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
2-CHLORO-6-METHOXY-BENZALDEHYDE Suppliers
- Tel
- --
- Fax
- --
- y.barysheva@ukrorgsynth.com
- Country
- Ukraine
- ProdList
- 6230
- Advantage
- 38
View Lastest Price from 2-CHLORO-6-METHOXY-BENZALDEHYDE manufacturers
- Product
- 2-CHLORO-6-METHOXY-BENZALDEHYDE 29866-54-4
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02