ChemicalBook > CAS DataBase List > ETHYL 2-(3-BROMOPHENYL)ACETATE

ETHYL 2-(3-BROMOPHENYL)ACETATE

Product Name: ETHYL 2-(3-BROMOPHENYL)ACETATE
CAS No.: 14062-30-7
Chemical Name: ETHYL 2-(3-BROMOPHENYL)ACETATE
Synonyms: Ethyl 2-(3-bromophenyl);Ethyl 3-Bromophenylacetate;ETHYL 2-(3-BROMOPHENYL)ACETATE;Benzeneacetic acid, 3-broMo-, ethyl ester
CBNumber: CB52453193
Molecular Formula: C10H11BrO2
Formula Weight: 243.1
MOL File: 14062-30-7.mol

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ETHYL 2-(3-BROMOPHENYL)ACETATE Property

Boiling point:: 132-134 °C(Press: 8 Torr)
Density: 1.3810 g/cm3
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Oil
color: Colourless

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B124678
Product name: Ethyl2-(3-Bromophenyl)acetate
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Oakwood

Product number: 078862
Product name: Ethyl3-bromophenylacetate
Purity: 95+%
Packaging: 1g
Price: $12
Updated: 2021/12/16

AK Scientific

Product number: J94756
Product name: Ethyl3-Bromophenylacetate
Packaging: 5g
Price: $32
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB61410
Product name: Ethyl 3-Bromophenylacetate
Packaging: 2g
Price: $40
Updated: 2021/12/16

Matrix Scientific

Product number: 075367
Product name: Ethyl 3-bromophenylacetate
Purity: 95+%
Packaging: 5g
Price: $44
Updated: 2021/12/16

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ETHYL 2-(3-BROMOPHENYL)ACETATE Chemical Properties,Usage,Production

Synthesis Reference(s)

Journal of Medicinal Chemistry, 43, p. 1508, 2000 DOI: 10.1021/jm990448e

Synthesis

64-17-5

1878-67-7

14062-30-7

To a 250 mL round bottom flask was added 3-bromophenylacetic acid (5 g, 23.25 mmol, 1.00 equiv) and ethanol (80 mL). With stirring at 0 °C, thionyl chloride (5.6 g, 46.28 mmol, 2.00 eq.) was added slowly and dropwise. The reaction mixture was heated to reflux and kept for 2 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure to remove the solvent. Subsequently, the reaction was quenched by the addition of water. The aqueous phase was extracted with ethyl acetate (3 × 30 mL) and the organic layers were combined. The organic layer was washed with saturated saline (50 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. 5.5 g (97% yield) of ethyl 2-(3-bromophenyl)acetate was finally obtained as a colorless oil.

References

[1] Journal of Medicinal Chemistry, 2000, vol. 43, # 8, p. 1508 - 1518
[2] Patent: US2013/190290, 2013, A1. Location in patent: Paragraph 1328; 1329; 1330
[3] Patent: WO2015/130957, 2015, A1. Location in patent: Page/Page column 77
[4] Patent: WO2010/127440, 2010, A1. Location in patent: Page/Page column 39-40
[5] Patent: WO2010/127448, 2010, A1. Location in patent: Page/Page column 26-27

ETHYL 2-(3-BROMOPHENYL)ACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from ETHYL 2-(3-BROMOPHENYL)ACETATE manufacturers

Career Henan Chemical Co

Product: ETHYL 2-(3-BROMOPHENYL)ACETATE 14062-30-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-25

14062-30-7, ETHYL 2-(3-BROMOPHENYL)ACETATERelated Search:

(3-BROMOPHENYL)ACETIC ACID METHYL ESTER ETHYL 2-(3-BROMOPHENYL)ACETATE ETHYL AMINO(5-BROMO-2-METHOXYPHENYL)ACETATE HYDROCHLORIDE RARECHEM AK ML 0192 ETHYL 3-BROMOBENZOYL FORMATE RARECHEM AL BI 1371 Ethyl (5-bromo-2-methoxyphenyl)-acetate

ETHYL 2-(3-BROMOPHENYL)ACETATE

Ethyl 2-(3-bromophenyl)

Ethyl 3-Bromophenylacetate

Benzeneacetic acid, 3-broMo-, ethyl ester

14062-30-7