METHYL 2-FLUORO-3-METHYLBENZOATE

Product Name: METHYL 2-FLUORO-3-METHYLBENZOATE
CAS No.: 586374-04-1
Chemical Name: METHYL 2-FLUORO-3-METHYLBENZOATE
Synonyms: 2-fluoro-3-methylbenzoate;METHYL 2-FLUORO-3-METHYLBENZOATE;2-Fluoro-3-methyl benzoate methyl;2-Fluoro-3-methylbenzoic acid methyl ester;Benzoic acid, 2-fluoro-3-methyl-, methyl ester;2-fluoro-3-methyl-Benzoic acid methyl ester (9CI ACI);Benzoic acid, 2-fluoro-3-methyl-, methyl ester (9CI, ACI)
CBNumber: CB52454716
Molecular Formula: C9H9FO2
Formula Weight: 168.16
MOL File: 586374-04-1.mol

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METHYL 2-FLUORO-3-METHYLBENZOATE Property

Boiling point:: 229.0±28.0℃ (760 Torr)
Density: 1.137±0.06 g/cm3 (20 ºC 760 Torr)
Flash point:: 89.8±18.9℃
storage temp.: Sealed in dry,Room Temperature
Appearance: Colorless to light pink Liquid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Oakwood

Product number: 209485
Product name: Methyl 2-fluoro-3-methylbenzoate
Packaging: 250mg
Price: $25
Updated: 2021/12/16

Oakwood

Product number: 209485
Product name: Methyl 2-fluoro-3-methylbenzoate
Packaging: 1g
Price: $48
Updated: 2021/12/16

Oakwood

Product number: 209485
Product name: Methyl 2-fluoro-3-methylbenzoate
Packaging: 5g
Price: $148
Updated: 2021/12/16

Oakwood

Product number: 209485
Product name: Methyl 2-fluoro-3-methylbenzoate
Packaging: 25g
Price: $499
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0369203
Product name: METHYL-2-FLUORO-3-METHYLBENZOATE
Purity: 95.00%
Packaging: 5MG
Price: $504.85
Updated: 2021/12/16

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METHYL 2-FLUORO-3-METHYLBENZOATE Chemical Properties,Usage,Production

Chemical Properties

off-white powder

Synthesis

67-56-1

315-31-1

586374-04-1

Step A: Thionyl chloride (2.8 mL, 39.0 mmol) was added slowly and dropwise to a stirred solution of 2-fluoro-3-methylbenzoic acid (4.0 g, 26.0 mmol) in anhydrous methanol (52 mL) at 0 °C. The reaction mixture was stirred overnight under reflux conditions. Upon completion of the reaction, the mixture was diluted with methanol and the excess thionyl chloride was subsequently removed by concentration under reduced pressure. The residue was dissolved in ethyl acetate, the organic layer was washed with saturated aqueous sodium bicarbonate, dried over anhydrous sodium sulfate, filtered, and concentrated under reduced pressure to afford methyl 2-fluoro-3-methylbenzoate (3.6 g, 83% yield) as a clear oil. The product could be used in subsequent steps without further purification.1H NMR (500 MHz, CDCl3) δ 7.75-7.72 (m, 1H), 7.38-7.35 (m, 1H), 7.26-7.06 (m, 1H), 3.91 (s, 3H), 2.31 (s, 3H).

References

[1] Patent: WO2011/8572, 2011, A2. Location in patent: Page/Page column 62
[2] Patent: WO2005/18557, 2005, A2. Location in patent: Page/Page column 304
[3] Patent: WO2005/18557, 2005, A2. Location in patent: Page/Page column 304

METHYL 2-FLUORO-3-METHYLBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 2-FLUORO-3-METHYLBENZOATE Suppliers

China 69 India 1 United Kingdom 1 United States 3 Global 74

Shijiazhuang Sdyano Fine Chemical Co., Ltd.

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Bide Pharmatech Ltd.

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Tianjin Anhao Biological Technology Co., Ltd.

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View Lastest Price from METHYL 2-FLUORO-3-METHYLBENZOATE manufacturers

Honest Joy Holdings Limited

Product: Methyl 2-fluoro-3-methylbenzoate 586374-04-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 97.0%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: METHYL 2-FLUORO-3-METHYLBENZOATE 586374-04-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-08

586374-04-1, METHYL 2-FLUORO-3-METHYLBENZOATERelated Search:

2,5-DIFLUORO-3-METHYLBENZOIC ACID ETHYL ESTER METHYL 2-FLUORO-3-METHYLBENZOATE RARECHEM AL BI 0317 RARECHEM AL BF 0317 RARECHEM AL BF 0492 2,5-DIFLUORO-3-METHYLBENZOIC ACID METHYL ESTER 2,4-DIFLUORO-3-METHYLBENZOICACID METHYL ESTER RARECHEM AL BI 0295 RARECHEM AL BI 0492 RARECHEM AL BF 0295 2,4-DIFLUORO-3-METHYLBENZOIC ACID ETHYL ESTER RARECHEM AL BF 0496 RARECHEM AL BI 0496

METHYL 2-FLUORO-3-METHYLBENZOATE

2-fluoro-3-methylbenzoate

2-Fluoro-3-methyl benzoate methyl

Benzoic acid, 2-fluoro-3-methyl-, methyl ester

2-Fluoro-3-methylbenzoic acid methyl ester

Benzoic acid, 2-fluoro-3-methyl-, methyl ester (9CI, ACI)

2-fluoro-3-methyl-Benzoic acid methyl ester (9CI ACI)

586374-04-1