4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER
- Product Name
- 4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER
- CAS No.
- 51498-33-0
- Chemical Name
- 4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER
- Synonyms
- Ethyl 4-aMinocyclohexanecarboxylate;4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER;Cyclohexanecarboxylic acid, 4-aMino-, ethyl ester;ethyl 4-aminocyclohexane-1-carboxylate, Mixture of diastereomers;4-amino-Cyclohexanecarboxylic acid ethyl ester (6CI 7CI 9CI ACI);Cyclohexanecarboxylic acid, 4-amino-, ethyl ester (6CI, 7CI, 9CI, ACI)
- CBNumber
- CB52463969
- Molecular Formula
- C9H17NO2
- Formula Weight
- 171.24
- MOL File
- 51498-33-0.mol
4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER Property
- Boiling point:
- 114-117 °C(Press: 10 Torr)
- Density
- 1.018±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 10.36±0.70(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 7177AB
- Product name
- Ethyl4-aminocyclohexanecarboxylate
- Packaging
- 250mg
- Price
- $185
- Updated
- 2021/12/16
- Product number
- 135116
- Product name
- Ethyl 4-aminocyclohexane-1-carboxylate
- Purity
- 95%+
- Packaging
- 1g
- Price
- $380
- Updated
- 2021/12/16
- Product number
- CHM0119348
- Product name
- ETHYL 4-AMINOCYCLOHEXANE-1-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $765.23
- Updated
- 2021/12/16
- Product number
- 135116
- Product name
- Ethyl 4-aminocyclohexane-1-carboxylate
- Purity
- 95%+
- Packaging
- 2.500g
- Price
- $830
- Updated
- 2021/12/16
- Product number
- CHM0119348
- Product name
- ETHYL 4-AMINOCYCLOHEXANE-1-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1065.66
- Updated
- 2021/12/16
4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER Chemical Properties,Usage,Production
Synthesis
1776-53-0
64-17-5
51498-33-0
GENERAL STEPS: 4-Aminocyclohexanecarboxylic acid (5.0 g, 34.92 mmol) was dissolved in ethanol (20 mL) and cooled to 0 °C. Thionyl chloride (7.60 mL, 104.76 mmol) was slowly added dropwise with stirring. After the dropwise addition, the reaction mixture was heated to 80 °C and maintained for 2-3 hours. The reaction process was monitored by thin layer chromatography (TLC). After completion of the reaction, the solvent was removed by evaporation under reduced pressure to give ethyl 4-aminocyclohexane-1-carboxylate in quantitative yield.
References
[1] Patent: US2012/88750, 2012, A1. Location in patent: Page/Page column 41
[2] Patent: WO2006/77424, 2006, A1. Location in patent: Page/Page column 162-163
[3] Patent: WO2006/77425, 2006, A1. Location in patent: Page/Page column 162-163
[4] Patent: WO2006/77428, 2006, A1. Location in patent: Page/Page column 140
[5] Patent: US2013/252938, 2013, A1. Location in patent: Paragraph 0502
4-AMINO-CYCLOHEXANECARBOXYLIC ACID ETHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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