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tert-butyl azetidin-3-ylmethyl(methyl)carbamate

Product Name
tert-butyl azetidin-3-ylmethyl(methyl)carbamate
CAS No.
1053655-53-0
Chemical Name
tert-butyl azetidin-3-ylmethyl(methyl)carbamate
Synonyms
3-(N-Boc-Methylaminomethy...;3-[Boc(methyl)aminomethyl]azetidine,95%;3-[Boc(Methyl)aMinoMethyl]azetidine, 95%;N-Boc-1-(3-azetidinyl)-N-methylmethanamine;tert-butyl azetidin-3-ylmethyl(methyl)carbamate;tert-butyl N-(azetidin-3-ylmethyl)-N-methylcarbamate;1,1-Dimethylethyl N-(3-azetidinylmethyl)-N-methylcarbamate;N-(3-Azetidinylmethyl)-N-methylcarbamic acid tert-butyl ester;N-(3-azetidinylMethyl)-n-Methyl-carbaMic acid 1,1-diMethylethyl ester;Carbamic acid, N-(3-azetidinylmethyl)-N-methyl-, 1,1-dimethylethyl ester
CBNumber
CB52490295
Molecular Formula
C10H20N2O2
Formula Weight
200.28
MOL File
1053655-53-0.mol
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tert-butyl azetidin-3-ylmethyl(methyl)carbamate Property

Boiling point:
267℃
Density 
1.012
Flash point:
116℃
storage temp. 
2-8°C(protect from light)
pka
10.86±0.40(Predicted)
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Safety

HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Alfa Aesar
Product number
H60310
Product name
3-[Boc(methyl)aminomethyl]azetidine, 95%
Packaging
250mg
Price
$214
Updated
2023/06/20
Alfa Aesar
Product number
H60310
Product name
3-[Boc(methyl)aminomethyl]azetidine, 95%
Packaging
1g
Price
$612
Updated
2023/06/20
TRC
Product number
B789533
Product name
tert-ButylAzetidin-3-ylmethyl(methyl)carbamate
Packaging
10mg
Price
$45
Updated
2021/12/16
Matrix Scientific
Product number
059926
Product name
3-(N-Boc-Methylaminomethyl)azetidine
Purity
95%
Packaging
500mg
Price
$475
Updated
2021/12/16
Matrix Scientific
Product number
059926
Product name
3-(N-Boc-Methylaminomethyl)azetidine
Purity
95%
Packaging
1g
Price
$612
Updated
2021/12/16
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tert-butyl azetidin-3-ylmethyl(methyl)carbamate Chemical Properties,Usage,Production

Uses

Tert-butyl azetidin-3-ylmethyl(methyl)carbamate is an important organic reagent that can be used as a building block for the synthesis of tert-butyl ((1-((4-chloro-7H-pyrrolo[2,3-d]pyrimidin-5-yl)methyl)azetidin-3-yl)methyl)(methyl)carbamate which is an important intermediate of a selective small-molecule PLK inhibitors useful in the treatment of cell proliferative disorders.

Synthesis

A solution of tert-butyl ((1-benzhydrylazetidin-3-yl)methyl)carbamate (6.18 g, 17.53 mmol) in 50 mL of MeOH and 15 mL of EtOAc was purged with argon. Pd/C (10%, 50% in water) (929 mg) was added and the mixture was then purged again with argon and stirred in an H2 atmosphere for 18 h. The reaction was filtered through Ceitte and the filter was washed with EtOAc and MeOH, The resulting solvent was evaporated to dryness, providing 5.66 g of a mixture of tert-butyl azetidin-3-ylmethyl(methyl)carbamate together with one equivalent of diphenylmethane. The pure product tert-butyl azetidin-3-ylmethyl(methyl)carbamate was obtained after further purification.


tert-butyl azetidin-3-ylmethyl(methyl)carbamate Preparation Products And Raw materials

Raw materials

Preparation Products

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tert-butyl azetidin-3-ylmethyl(methyl)carbamate Suppliers

NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
Advantage
58

1053655-53-0, tert-butyl azetidin-3-ylmethyl(methyl)carbamateRelated Search:


  • tert-butyl azetidin-3-ylmethyl(methyl)carbamate
  • 3-(N-Boc-Methylaminomethy...
  • 3-[Boc(Methyl)aMinoMethyl]azetidine, 95%
  • N-(3-Azetidinylmethyl)-N-methylcarbamic acid tert-butyl ester
  • N-(3-azetidinylMethyl)-n-Methyl-carbaMic acid 1,1-diMethylethyl ester
  • tert-butyl N-(azetidin-3-ylmethyl)-N-methylcarbamate
  • Carbamic acid, N-(3-azetidinylmethyl)-N-methyl-, 1,1-dimethylethyl ester
  • 3-[Boc(methyl)aminomethyl]azetidine,95%
  • N-Boc-1-(3-azetidinyl)-N-methylmethanamine
  • 1,1-Dimethylethyl N-(3-azetidinylmethyl)-N-methylcarbamate
  • 1053655-53-0