Methyl 4-bromo-2-(trifluoromethyl)benzoate
Application- Product Name
- Methyl 4-bromo-2-(trifluoromethyl)benzoate
- CAS No.
- 957207-58-8
- Chemical Name
- Methyl 4-bromo-2-(trifluoromethyl)benzoate
- Synonyms
- Methyl 4-bromo-2-(trifluoromethyl)benzoate;4-Bromo-2-(trifluoromethyl)benzoic acid methyl ester;Benzoic acid, 4-bromo-2-(trifluoromethyl)-, methyl ester
- CBNumber
- CB52516575
- Molecular Formula
- C9H6BrF3O2
- Formula Weight
- 283.04
- MOL File
- 957207-58-8.mol
Methyl 4-bromo-2-(trifluoromethyl)benzoate Property
- Boiling point:
- 274.2±40.0 °C(Predicted)
- Density
- 1.598±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M293850
- Product name
- Methyl4-Bromo-2-(trifluoromethyl)benzoate
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- M293850
- Product name
- Methyl4-Bromo-2-(trifluoromethyl)benzoate
- Packaging
- 2.5g
- Price
- $200
- Updated
- 2021/12/16
- Product number
- FB67934
- Product name
- 4-Bromo-2-(trifluoromethyl)benzoic acid methyl ester
- Packaging
- 1g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- 2823-B-02
- Product name
- Methyl 4-bromo-2-(trifluoromethyl)benzoate
- Packaging
- 1g
- Price
- $61
- Updated
- 2021/12/16
- Product number
- FB67934
- Product name
- 4-Bromo-2-(trifluoromethyl)benzoic acid methyl ester
- Packaging
- 2g
- Price
- $80
- Updated
- 2021/12/16
Methyl 4-bromo-2-(trifluoromethyl)benzoate Chemical Properties,Usage,Production
Application
Methyl 4-bromo-2-trifluoromethylbenzoate can be used as an organic intermediate and a pharmaceutical intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical analysis processes.
Synthesis
67-56-1
320-31-0
957207-58-8
Synthesis of methyl 4-bromo-2-(trifluoromethyl)benzoate (107): 4-bromo-2-(trifluoromethyl)benzoic acid (106; 1.6 g, 5.95 mmol) was dissolved in 20 mL of methanol. 2 mL of thionyl chloride was added slowly. After addition, the reaction mixture was stirred at 60 °C for 12 h and subsequently concentrated. To the residue was added 20 mL of ethyl acetate. The mixture was washed sequentially with saturated aqueous sodium bicarbonate and saturated brine, dried over anhydrous sodium sulfate and concentrated to give 1.6 g methyl 4-bromo-2-(trifluoromethyl)benzoate (107) as a yellow liquid. Yield 85%. LCMS: m/z 282.7 [M + H]+, tR = 1.79 min.
References
[1] Patent: US2012/28952, 2012, A1. Location in patent: Page/Page column 18-19
[2] Patent: WO2017/31213, 2017, A1. Location in patent: Paragraph 00419
[3] Patent: WO2013/175053, 2013, A1. Location in patent: Page/Page column 120-121
Methyl 4-bromo-2-(trifluoromethyl)benzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 4-bromo-2-(trifluoromethyl)benzoate manufacturers
- Product
- Methyl 4-bromo-2-(trifluoromethyl)benzoate 957207-58-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg; 2kg；10kg; 100kg
- Release date
- 2019-08-30