ChemicalBook > CAS DataBase List > 5-Azazindole-3-carboxyaldehyde.

5-Azazindole-3-carboxyaldehyde.

Product Name
5-Azazindole-3-carboxyaldehyde.
CAS No.
933717-10-3
Chemical Name
5-Azazindole-3-carboxyaldehyde.
Synonyms
2-c]pyridine-3-carbaldehyde;5-Azazindole-3-carboxyaldehyde.;Pyrrolo[3,2-c]pyridine-3-carbaldehyde;1H-Pyrrolo[3,2-c]pyridine-3-carbaldehyde
CBNumber
CB52526189
Molecular Formula
C8H6N2O
Formula Weight
146.15
MOL File
933717-10-3.mol
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5-Azazindole-3-carboxyaldehyde. Property

Density 
1.368
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
Appearance
White to yellow Solid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR321326
Product name
1H-Pyrrolo[3,2-c]pyridine-3-carbaldehyde
Purity
97%
Packaging
1g
Price
$135
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0101094
Product name
3-FORMYL-5-AZAINDOLE
Purity
95.00%
Packaging
1G
Price
$420
Updated
2021/12/16
Apolloscientific
Product number
OR321326
Product name
1H-Pyrrolo[3,2-c]pyridine-3-carbaldehyde
Purity
97%
Packaging
5g
Price
$454
Updated
2021/12/16
AK Scientific
Product number
W9607
Product name
1H-Pyrrolo[3,2-c]pyridine-3-carboxaldehyde
Packaging
1g
Price
$220
Updated
2021/12/16
Matrix Scientific
Product number
076299
Product name
1H-Pyrrolo[3,2-c]pyridine-3-carboxaldehyde
Purity
95+%
Packaging
1g
Price
$230
Updated
2021/12/16
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5-Azazindole-3-carboxyaldehyde. Chemical Properties,Usage,Production

Synthesis

271-34-1

4885-02-3

933717-10-3

General procedure for the synthesis of 5-azaindole-3-carboxaldehyde from 5-azaindole and 1,1-dichlorodimethyl ether: 5-azaindole (0.400 g; 3.386 mmol) was dissolved in a solvent mixture of 1,2-dichloroethane (10 mL) and nitromethane (10 mL) and cooled to 0 °C. The reaction was followed by the addition of aluminum trichloride (1.544 mL; 16.92 mmol). Under argon protection, 1,1-dichlorodimethyl ether (1.544 mL; 16.92 mmol) was slowly added dropwise, followed by batchwise addition of aluminum trichloride (1.5500 g; 11.25 mmol), which was controlled to be completed within 1 hour. Upon completion of the reaction, the reaction was quenched by the addition of water and saturated sodium bicarbonate solution. The reaction mixture was extracted with a solvent mixture of dichloromethane and ethanol (9:1, 6 x 100 mL, v/v). The organic layers were combined, washed with saturated brine, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to afford the crude product 1H-pyrrolo[3,2-c]pyridine-3-carboxaldehyde (0.333 g, 67% yield), which can be used directly in subsequent reactions without further purification. The product was characterized as follows: ESI/APCI(+): m/z 147 [M+H]+; ESI/APCI(-): m/z 145 [M-H]-. 1H NMR (DMSO-d6) δ: 10.00 (1H, s), 9.29 (1H, s), 8.42 (1H, s), 8.35 (1H, d), 7.53 (1H, d). .

References

[1] Patent: WO2013/45516, 2013, A1. Location in patent: Page/Page column 201

5-Azazindole-3-carboxyaldehyde. Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Azazindole-3-carboxyaldehyde. manufacturers

Career Henan Chemical Co
Product
5-Azazindole-3-carboxyaldehyde. 933717-10-3
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg; 2kg；10kg; 100kg
Release date
2019-08-30

933717-10-3, 5-Azazindole-3-carboxyaldehyde.Related Search:

5-AZAINDOLE-2-CARBOXYLIC ACID 1H-Pyrrolo[3,2-c]pyridine-3-carboxylic acid Methyl ester 2-Amino-3-bromo-5-nitrobenzonitrile TERT-BUTYL METHYL MALONATE AMMONIUM CERIUM(IV) SULFATE TETRAHYDRATE 5-Chlorofuran-2-carboxylic acid Anastrozole

  • 5-Azazindole-3-carboxyaldehyde.
  • 1H-Pyrrolo[3,2-c]pyridine-3-carbaldehyde
  • 2-c]pyridine-3-carbaldehyde
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  • Heterocycle-Pyridine series