3,4-dichloropyridazine

Product Name: 3,4-dichloropyridazine
CAS No.: 1677-80-1
Chemical Name: 3,4-dichloropyridazine
Synonyms: 3,4-dichloropyridazine;Pyridazine, 3,4-dichloro-;3,4-dichloropyridazine ISO 9001：2015 REACH
CBNumber: CB52553798
Molecular Formula: C4H2Cl2N2
Formula Weight: 148.98
MOL File: 1677-80-1.mol

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3,4-dichloropyridazine Property

Boiling point:: 125 °C(Press: 3-4 Torr)
Density: 1.493±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -0.89±0.10(Predicted)
Appearance: light gray solid

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: D475795
Product name: 3,4-dichloropyridazine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD146446
Product name: 3,4-Dichloropyridazine
Packaging: 50mg
Price: $170
Updated: 2021/12/16

Apolloscientific

Product number: OR925203
Product name: 3,4-Dichloropyridazine
Packaging: 500mg
Price: $482
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD146446
Product name: 3,4-Dichloropyridazine
Packaging: 250mg
Price: $500
Updated: 2021/12/16

Apolloscientific

Product number: OR925203
Product name: 3,4-Dichloropyridazine
Packaging: 1g
Price: $713
Updated: 2021/12/16

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3,4-dichloropyridazine Chemical Properties,Usage,Production

Synthesis

1677-79-8

1677-80-1

General procedure for the synthesis of 3,4-dichloropyridazine from 4-chloro-3-pyridazinone: 4-chloro-3-pyridazinone (25 g, 0.19 mol) was dissolved in acetonitrile (200 ml). Subsequently, phosphoryl chloride (73 g, 0.48 mol) was added to the solution and the reaction mixture was refluxed at 80 °C for 3 hours. After the completion of the reaction was monitored by TLC, the reaction solution was cooled to room temperature and slowly poured into ice water (200 ml). The pH of the mixture was adjusted to 7-8 with sodium bicarbonate and then extracted twice with ethyl acetate (300 ml). The organic phases were combined, washed with saturated brine (400 ml) and dried over anhydrous sodium sulfate. The organic phases were concentrated under reduced pressure and the resulting crude product was purified by column chromatography to give 3,4-dichloropyridazine (18.0 g, 0.12 mol) in about 64% yield.

References

[1] Patent: CN104211644, 2016, B. Location in patent: Paragraph 0042-048

3,4-dichloropyridazine Preparation Products And Raw materials

Raw materials

Preparation Products

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3,4-dichloropyridazine Suppliers

China 61 India 1 United Kingdom 1 United States 7 Global 70

Yangzhou Haihao Biotechnology Co.,Ltd

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View Lastest Price from 3,4-dichloropyridazine manufacturers

Dideu Industries Group Limited

Product: 3,4-dichloropyridazine 1677-80-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-11-08

Career Henan Chemical Co

Product: 3,4-dichloropyridazine 1677-80-1
Price: US $8.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 100kg
Release date: 2019-08-05

1677-80-1, 3,4-dichloropyridazineRelated Search:

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3,4-dichloropyridazine

Pyridazine, 3,4-dichloro-

3,4-dichloropyridazine ISO 9001：2015 REACH

1677-80-1