ChemicalBook > CAS DataBase List > N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine

N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine

Product Name: N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine
CAS No.: 499128-71-1
Chemical Name: N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine
Synonyms: FPB;fppbj;N-2BP-PBr;Compound bleach;[1,1'-Biphenyl]-4-;N-(4-Bromophenyl-N;N,N-Bis(4-biphenyL;)-N-(4-bromophenyL;N-(4-BroMophenyl)-N,N-;4-Bromo-4',4''-diphenyltriphenylamine
CBNumber: CB52582497
Molecular Formula: C30H22BrN
Formula Weight: 476.41
MOL File: 499128-71-1.mol

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N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine Property

Melting point:: 172-174℃
Boiling point:: 625.7±55.0 °C(Predicted)
Density: 1.296
storage temp.: Sealed in dry,Room Temperature
solubility: slightly sol. in Tetrahydrofuran
form: powder to crystal
pka: -3.76±0.50(Predicted)
color: White to Almost white

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Safety

HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B4550
Product name: N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine
Purity: >98.0%(HPLC)(N)
Packaging: 5g
Price: $50
Updated: 2025/07/31

TCI Chemical

Product number: B4550
Product name: N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine
Purity: >98.0%(HPLC)(N)
Packaging: 25g
Price: $148
Updated: 2025/07/31

Usbiological

Product number: 355739
Product name: FPB
Packaging: 48Tests
Price: $588
Updated: 2021/12/16

AK Scientific

Product number: 8403AL
Product name: N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine
Packaging: 100mg
Price: $72
Updated: 2021/12/16

Arctom

Product number: AS019082
Product name: N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine
Purity: ≥95%
Packaging: 10g
Price: $99
Updated: 2021/12/16

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N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine Chemical Properties,Usage,Production

Synthesis

589-87-7

102113-98-4

499128-71-1

The general procedure for the synthesis of N-(4-bromophenyl)-N,N-bis(1,1'-biphenyl-4-yl)amine from p-bromoiodobenzene and bis(4-biphenyl)amine was as follows: bis(4-biphenyl)amine (23.7 g, 73.8 mmol) was added to a round-bottomed flask, followed by the addition of p-bromoiodobenzene (20.9 g, 73.8 mmol), sodium tert-butanolate (10.7 g, 111 mmol), p-butylpropanol (0.33 g, 1.47 mmol), and ultrasonically deoxygenated toluene (1.5 L). 111 mmol), palladium acetate (0.33 g, 1.47 mmol), and ultrasonically deoxygenated toluene (1.5 L). The mixture was heated to reflux overnight under nitrogen protection. After completion of the reaction, the reaction solution was cooled and extracted with ethyl acetate and water. The organic layer was separated and dried with anhydrous magnesium sulfate. The solvent was removed by distillation under reduced pressure to give the crude product. The crude product was purified by column chromatography using silica gel as stationary phase and dichloromethane/hexane as eluent to afford the target product N-(4-bromophenyl)-N,N-bis(1,1'-biphenyl-4-yl)amine (28.8 g, 82% yield).

References

[1] Patent: CN107652189, 2018, A. Location in patent: Paragraph 0068; 0069-0071
[2] Patent: CN107739377, 2018, A. Location in patent: Paragraph 0075-0078
[3] Patent: CN107986975, 2018, A. Location in patent: Paragraph 0074-0075
[4] Patent: CN108148016, 2018, A. Location in patent: Paragraph 0082; 0083; 0084
[5] Patent: EP2292603, 2011, A1. Location in patent: Page/Page column 25

N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine 499128-71-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-27

Shanghai Daken Advanced Materials Co.,Ltd

Product: [1,1'-Biphenyl]-4-amine,N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)- 499128-71-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 150KG /month
Release date: 2021-11-19

Shanghai UCHEM Inc.

Product: N-(4-Bromophenyl)-N,N-bis(1,1'-biphenyl-4-yl)amine 499128-71-1
Price: US $56.00-378.00/g
Min. Order: 25g
Purity: 0.98
Supply Ability: 10kg
Release date: 2023-12-14

499128-71-1, N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMineRelated Search:

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N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine

N-[1,1'-Biphenyl]-4-yl-N-(4-bromophenyl)-[1,1'-biphenyl]-4-amine

N-(4-BroMophenyl)-N,N-

N-(4-BroMophenyl)-N , N-bis(1 , l'-biphenyl-yl)aMine

N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine

[1,1'-Biphenyl]-4-amine,N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)

N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine

N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine(BBAPBr)

N-(4-Bromophenyl-N

N-2BP-PBr

[1,1'-Biphenyl]-4-

Compound bleach

N-(4-bromophenyl)-4-phenyl-N-(4-phenylphenyl)aniline

N-(4-Biphenylyl)-N-(4-bromophenyl)-4-biphenylamine

FPB

N-([1,1'-bipehenyl]-4-yl)-N-(4-bromophenyl)-[1,1'-biphenyl]-4-amine

N,N-Bis(4-biphenylyl)-N-(4-bromophenyl)amine&gt

N,N-Bis(4-biphenyL

)-N-(4-bromophenyL

4-Bromo-4',4''-diphenyltriphenylamine

N-(4-BroMophenyl)-N,N-bis(1,1'-biphenyl-4-yl)aMine ISO 9001：2015 REACH

[1,1'-Biphenyl]-4-amine, N-[1,1'-biphenyl]-4-yl-N-(4-bromoph...

N-([1,1'-biphenyl]-4-yl)-N-(4-bromophenyl)-[1,1'-biphenyl]-4-amine

fppbj

N-(4-Bromophenyl)-N,N-bis(biphenyl)amine

499128-71-1

C30H22BrN

OLED materials,pharm chemical,electronic