6-Chloro-2-iodo-benzaldehyde
- Product Name
- 6-Chloro-2-iodo-benzaldehyde
- CAS No.
- 51738-07-9
- Chemical Name
- 6-Chloro-2-iodo-benzaldehyde
- Synonyms
- 6-Chloro-2-iodo-benzadehyde;2-Chloro-6-iodobenzaldehyde;6-Chloro-2-iodo-benzaldehyde;Benzaldehyde, 2-chloro-6-iodo-
- CBNumber
- CB52583106
- Molecular Formula
- C7H4ClIO
- Formula Weight
- 266.46
- MOL File
- 51738-07-9.mol
6-Chloro-2-iodo-benzaldehyde Property
- Boiling point:
- 289.6±25.0 °C(Predicted)
- Density
- 1.971±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- Appearance
- Off-white to light yellow Solid
Safety
- HS Code
- 2913000090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 2374DP
- Product name
- 2-Chloro-6-iodobenzaldehyde
- Packaging
- 100mg
- Price
- $112
- Updated
- 2021/12/16
- Product number
- 2374DP
- Product name
- 2-Chloro-6-iodobenzaldehyde
- Packaging
- 1g
- Price
- $251
- Updated
- 2021/12/16
- Product number
- 2615-M-03
- Product name
- 2-Chloro-6-iodobenzaldehyde
- Packaging
- 1g
- Price
- $288
- Updated
- 2021/12/16
- Product number
- 2615-M-03
- Product name
- 2-Chloro-6-iodobenzaldehyde
- Packaging
- 5G
- Price
- $960
- Updated
- 2021/12/16
- Product number
- A201275
- Product name
- 2-Chloro-6-iodobenzaldehyde
- Purity
- 95%
- Packaging
- 100mg
- Price
- $42
- Updated
- 2021/12/16
6-Chloro-2-iodo-benzaldehyde Chemical Properties,Usage,Production
Synthesis
945543-21-5
51738-07-9
b) Synthesis of 2-chloro-6-iodobenzaldehyde: 5.14 mL (72.4 mmol) of dimethylsulfoxide dissolved in 15 mL of methylene chloride was slowly added dropwise over 20 min to 3.11 mL (36.2 mmol) of oxalyl chloride dissolved in 40 mL of methylene chloride at -78 °C. The reaction mixture was continued to be stirred at -78°C for 15 minutes before 8.10 g (3.02 mmol) of a solution of 2-chloro-6-iodobenzyl alcohol dissolved in 40 mL of methylene chloride was added dropwise over 30 minutes. After the dropwise addition was completed, the mixture continued to be stirred at -78°C for 45 minutes. Subsequently, 20.9 mL (151 mmol) of triethylamine was slowly added to gradually warm the reaction mixture to room temperature. Upon completion of the reaction, it was quenched by the addition of water and the organic and aqueous phases were separated. The organic phase was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to afford 8.35 g (100% yield) of a yellow crystalline solid 2-chloro-6-iodobenzaldehyde, which was used directly in the next reaction without further purification. Mass spectrometry (EI) data: 268.0 (44%), 266.0 (100%) (M+) .
References
[1] Patent: US2007/197621, 2007, A1. Location in patent: Page/Page column 58
[2] Organic Letters, 2018, vol. 20, # 2, p. 345 - 348
6-Chloro-2-iodo-benzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-Chloro-2-iodo-benzaldehyde manufacturers
- Product
- 6-Chloro-2-iodo-benzaldehyde 51738-07-9
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2019-12-20