2-chloro-3-nitro-6-phenylpyridine

Product Name: 2-chloro-3-nitro-6-phenylpyridine
CAS No.: 187242-88-2
Chemical Name: 2-chloro-3-nitro-6-phenylpyridine
Synonyms: EOS-60527;2-chloro-3-nitro-6-phenylpyridine;Pyridine, 2-chloro-3-nitro-6-phenyl-
CBNumber: CB52616246
Molecular Formula: C11H7ClN2O2
Formula Weight: 234.64
MOL File: 187242-88-2.mol

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2-chloro-3-nitro-6-phenylpyridine Property

Boiling point:: 376.1±37.0 °C(Predicted)
Density: 1.366±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: -4.20±0.10(Predicted)
Appearance: Light yellow to yellow Solid
InChI: InChI=1S/C11H7ClN2O2/c12-11-10(14(15)16)7-6-9(13-11)8-4-2-1-3-5-8/h1-7H
InChIKey: FEXPVVIOGUUGJM-UHFFFAOYSA-N
SMILES: C1(Cl)=NC(C2=CC=CC=C2)=CC=C1[N+]([O-])=O

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FC153688
Product name: 2-chloro-3-nitro-6-phenylpyridine
Packaging: 250mg
Price: $67.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC153688
Product name: 2-chloro-3-nitro-6-phenylpyridine
Packaging: 500mg
Price: $115
Updated: 2021/12/16

AK Scientific

Product number: 9768AF
Product name: 2-Chloro-3-nitro-6-phenylpyridine
Packaging: 1g
Price: $130
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC153688
Product name: 2-chloro-3-nitro-6-phenylpyridine
Packaging: 1g
Price: $201.25
Updated: 2021/12/16

AK Scientific

Product number: 9768AF
Product name: 2-Chloro-3-nitro-6-phenylpyridine
Packaging: 5g
Price: $290
Updated: 2021/12/16

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2-chloro-3-nitro-6-phenylpyridine Chemical Properties,Usage,Production

Synthesis

16013-85-7

98-80-6

187242-88-2

Preparation of 2-chloro-3-nitro-6-phenylpyridine: To an anhydrous 1,4-dioxane solution of 2,6-dichloro-3-nitropyridine (1.00 g, 5.18 mmol) was added phenylboronic acid (0.695 g, 5.70 mmol), cesium carbonate (2 M aqueous solution, 7.5 mL, 15 mmol) and tetrakis(triphenylphosphine)palladium (0.025 g, 0.02 mmol). The reaction mixture was displaced three times with nitrogen and heated in a microwave reactor at 100 °C for 10 min. After completion of the reaction, it was cooled to room temperature and the reaction solution was poured into water and extracted with ethyl acetate. The organic phases were combined, washed sequentially with water and saturated saline, dried over anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: 5% ethyl acetate/hexane) to afford the target compound 2-chloro-3-nitro-6-phenylpyridine (0.5 g, 41% yield). LC-MS (m/z): 235 [M+H]+.

References

[1] Patent: US2008/242685, 2008, A1. Location in patent: Page/Page column 16

2-chloro-3-nitro-6-phenylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-chloro-3-nitro-6-phenylpyridine Suppliers

China 55 India 1 United Kingdom 1 United States 3 Global 60

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View Lastest Price from 2-chloro-3-nitro-6-phenylpyridine manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-chloro-3-nitro-6-phenylpyridine 187242-88-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-chloro-3-nitro-6-phenylpyridine 187242-88-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

187242-88-2, 2-chloro-3-nitro-6-phenylpyridineRelated Search:

2-chloro-3-nitro-6-phenylpyridine

EOS-60527

Pyridine, 2-chloro-3-nitro-6-phenyl-

187242-88-2