6-BroMopyridine-2-sulfonaMide

Product Name: 6-BroMopyridine-2-sulfonaMide
CAS No.: 856013-04-2
Chemical Name: 6-BroMopyridine-2-sulfonaMide
Synonyms: 6-BroMopyridine-2-sulfonaMide;2-Pyridinesulfonamide, 6-bromo-
CBNumber: CB52628672
Molecular Formula: C5H5BrN2O2S
Formula Weight: 237.07
MOL File: 856013-04-2.mol

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6-BroMopyridine-2-sulfonaMide Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB141691
Product name: 6-Bromopyridine-2-sulfonamide
Packaging: 50mg
Price: $51
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB141691
Product name: 6-Bromopyridine-2-sulfonamide
Packaging: 100mg
Price: $89
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB141691
Product name: 6-Bromopyridine-2-sulfonamide
Packaging: 250mg
Price: $177.5
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367861
Product name: 6-BROMOPYRIDINE-2-SULFONAMIDE
Purity: 95.00%
Packaging: 5MG
Price: $500.27
Updated: 2021/12/16

AK Scientific

Product number: 3298AC
Product name: 6-Bromopyridine-2-sulfonamide
Packaging: 1g
Price: $533
Updated: 2021/12/16

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6-BroMopyridine-2-sulfonaMide Chemical Properties,Usage,Production

Synthesis

1135871-89-4

856013-04-2

b) 6-Bromo-N-(tert-butyl)pyridine-2-sulfonamide (478 mg, 1.63 mmol) was dissolved in trifluoroacetic acid (TFA, 2 mL), and the reaction mixture was stirred for 3 hours at 60 °C. After completion of the reaction, TFA was evaporated under reduced pressure and the residue was treated with a solvent mixture of petroleum ether and ethyl ether (Et2O) to precipitate a brown solid. The solid was collected by filtration and ground three times with ether to give the final white solid product 6-bromopyridine-2-sulfonamide (125 mg, 32% yield). The product was characterized by 1H NMR (DMSO-d6, ppm): 7.98 (t, J=7.5 Hz, 1H), 7.91 (dd, J=7.5 and 1.2 Hz, 1H), 7.87 (dd, J=7.5 and 0.9 Hz, 1H).

References

[1] Patent: WO2009/39553, 2009, A1. Location in patent: Page/Page column 87

6-BroMopyridine-2-sulfonaMide Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BroMopyridine-2-sulfonaMide Suppliers

China 36 India 1 United Kingdom 1 United States 6 Global 44

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856013-04-2, 6-BroMopyridine-2-sulfonaMideRelated Search:

6-BroMopyridine-2-sulfonaMide

2-Pyridinesulfonamide, 6-bromo-

856013-04-2