2-broMo-3-Methoxybenzaldehyde
- Product Name
- 2-broMo-3-Methoxybenzaldehyde
- CAS No.
- 10401-18-0
- Chemical Name
- 2-broMo-3-Methoxybenzaldehyde
- Synonyms
- 2-broMo-3-Methoxybenzaldehyde;Benzaldehyde, 2-bromo-3-methoxy-;2-Bromo-3-methoxybenzaldehyde 95%
- CBNumber
- CB52694039
- Molecular Formula
- C8H7BrO2
- Formula Weight
- 215.04
- MOL File
- 10401-18-0.mol
2-broMo-3-Methoxybenzaldehyde Property
- Melting point:
- 69.5-70 °C(Solv: benzene (71-43-2); ligroine (8032-32-4))
- Boiling point:
- 277.6±20.0 °C(Predicted)
- Density
- 1.522±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder
- color
- Pale lemon
Safety
- HS Code
- 2912490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
N-Bromosuccinimide Price
- Product number
- FB168551
- Product name
- 2-Bromo-3-methoxybenzaldehyde
- Packaging
- 50mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- OR400081
- Product name
- 2-Bromo-3-methoxybenzaldehyde
- Purity
- 95%
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 2615-9-27
- Product name
- 2-Bromo-3-methoxybenzaldehyde
- Packaging
- 250mg
- Price
- $144
- Updated
- 2021/12/16
- Product number
- FB168551
- Product name
- 2-Bromo-3-methoxybenzaldehyde
- Packaging
- 100mg
- Price
- $160
- Updated
- 2021/12/16
- Product number
- FB168551
- Product name
- 2-Bromo-3-methoxybenzaldehyde
- Packaging
- 250mg
- Price
- $250
- Updated
- 2021/12/16
2-broMo-3-Methoxybenzaldehyde Chemical Properties,Usage,Production
Synthesis
196081-71-7
74-88-4
10401-18-0
To a mixed solution of N,N-dimethylformamide (60 mL) of 2-bromo-3-hydroxybenzaldehyde (1.30 g, 6.50 mmol) and potassium carbonate (2.70 g, 19.5 mmol) was added iodomethane (0.80 g, 12.9 mmol). The reaction mixture was stirred at room temperature for 16 h. After completion of the reaction, it was diluted with ethyl acetate (60 mL). The mixture was washed with saturated aqueous ammonium chloride solution (2 x 50 mL), the organic phase was dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated under reduced pressure and the residue was purified by column chromatography using a 0 to 30% ethyl acetate/hexane gradient elution to afford 2-bromo-3-methoxybenzaldehyde as a yellow oil (1.50 g, quantitative yield). Mass spectrum (electrospray positive ion mode) m/z 215.1 ([M+H]+).
References
[1] Patent: US2018/162868, 2018, A1. Location in patent: Paragraph 1413-1414
[2] Journal of the American Chemical Society, 2017, vol. 139, # 9, p. 3360 - 3363
[3] Patent: US2016/75711, 2016, A1. Location in patent: Paragraph 0586-0587
[4] Journal of Organic Chemistry, 2018, vol. 83, # 10, p. 5791 - 5800
2-broMo-3-Methoxybenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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