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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl

Product Name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
CAS No.
1233200-57-1
Chemical Name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Synonyms
3-Bromo-5'-phenyl-1,1';3-Bromo-5'-phenyl-m-terphenyl;5'-(3-Bromophenyl)-m-terphenyl;3',5'-Diphenyl-3-broMobiphenyl;1-(3-BROMOPHENYL)-3,5-DIPHENYLBENZENE;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl;5'-(3-Bromophenyl)-1,1':3',1''-terphenyl;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl>
CBNumber
CB52717404
Molecular Formula
C24H17Br
Formula Weight
385.3
MOL File
1233200-57-1.mol
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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Property

Melting point:
112.0 to 116.0 °C
Boiling point:
497.8±14.0 °C(Predicted)
Density 
1.278±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
color 
White to Light yellow
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Safety

HS Code 
2903.99.8001
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4888
Product name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity
>98.0%(GC)
Packaging
1g
Price
$37
Updated
2025/07/31
TCI Chemical
Product number
B4888
Product name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity
>98.0%(GC)
Packaging
5g
Price
$182
Updated
2025/07/31
TRC
Product number
B997463
Product name
3-Bromo-5''-phenyl-1,1'':3'',1''''-terphenyl
Packaging
50mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
6003AL
Product name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Packaging
100g
Price
$1200
Updated
2021/12/16
Ambeed
Product number
A491976
Product name
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
Purity
97%
Packaging
250mg
Price
$16
Updated
2021/12/16
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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Chemical Properties,Usage,Production

Synthesis

591-18-4

1036378-83-2

1233200-57-1

GENERAL STEPS: Compound I-8 (50 g, 140 mmol) and 2-([1,1':3',1''-terphenyl]-5'-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (43.7 g, 154 mmol) were dissolved in 0.45 L of tetrahydrofuran (THF), and tetrakis(triphenylphosphine)palladium was added under nitrogen protection ( 1.62 g, 1.40 mmol). Subsequently, saturated aqueous potassium carbonate solution (48.4 g, 350 mmol) was added and the reaction mixture was heated to reflux at 80 °C for 12 hours. After completion of the reaction, the reaction solution was poured into water and the organic phase was extracted with dichloromethane (DCM). The organic phase was dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The resulting residue was purified by fast column chromatography to afford the target product 3-bromo-5'-phenyl-1,1':3',1''-terphenyl (Compound I-15, 41.5 g, 77% yield).

References

[1] Patent: KR2015/117173, 2015, A. Location in patent: Paragraph 0239-0241
[2] Patent: KR2016/19747, 2016, A. Location in patent: Paragraph 0234-0237

3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Suppliers

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1233200-57-1, 3-Bromo-5'-phenyl-1,1':3',1''-terphenylRelated Search:


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