3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Product Name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- CAS No.
- 1233200-57-1
- Chemical Name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Synonyms
- 3-Bromo-5'-phenyl-1,1';3-Bromo-5'-phenyl-m-terphenyl;5'-(3-Bromophenyl)-m-terphenyl;3',5'-Diphenyl-3-broMobiphenyl;1-(3-BROMOPHENYL)-3,5-DIPHENYLBENZENE;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl;5'-(3-Bromophenyl)-1,1':3',1''-terphenyl;3-Bromo-5'-phenyl-1,1':3',1''-terphenyl>
- CBNumber
- CB52717404
- Molecular Formula
- C24H17Br
- Formula Weight
- 385.3
- MOL File
- 1233200-57-1.mol
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Property
- Melting point:
- 112.0 to 116.0 °C
- Boiling point:
- 497.8±14.0 °C(Predicted)
- Density
- 1.278±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B4888
- Product name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $37
- Updated
- 2025/07/31
- Product number
- B4888
- Product name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $182
- Updated
- 2025/07/31
- Product number
- B997463
- Product name
- 3-Bromo-5''-phenyl-1,1'':3'',1''''-terphenyl
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 6003AL
- Product name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Packaging
- 100g
- Price
- $1200
- Updated
- 2021/12/16
- Product number
- AS021651
- Product name
- 3-Bromo-5'-phenyl-1,1':3',1''-terphenyl
- Purity
- 97%
- Packaging
- 5g
- Price
- $112
- Updated
- 2021/12/16
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Chemical Properties,Usage,Production
Synthesis
591-18-4
1036378-83-2
1233200-57-1
GENERAL STEPS: Compound I-8 (50 g, 140 mmol) and 2-([1,1':3',1''-terphenyl]-5'-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (43.7 g, 154 mmol) were dissolved in 0.45 L of tetrahydrofuran (THF), and tetrakis(triphenylphosphine)palladium was added under nitrogen protection ( 1.62 g, 1.40 mmol). Subsequently, saturated aqueous potassium carbonate solution (48.4 g, 350 mmol) was added and the reaction mixture was heated to reflux at 80 °C for 12 hours. After completion of the reaction, the reaction solution was poured into water and the organic phase was extracted with dichloromethane (DCM). The organic phase was dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The resulting residue was purified by fast column chromatography to afford the target product 3-bromo-5'-phenyl-1,1':3',1''-terphenyl (Compound I-15, 41.5 g, 77% yield).
References
[1] Patent: KR2015/117173, 2015, A. Location in patent: Paragraph 0239-0241
[2] Patent: KR2016/19747, 2016, A. Location in patent: Paragraph 0234-0237
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Preparation Products And Raw materials
Raw materials
Preparation Products
3-Bromo-5'-phenyl-1,1':3',1''-terphenyl Suppliers
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