(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE

Product Name: (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE
CAS No.: 1026-05-7
Chemical Name: (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE
Synonyms: ASISCHEM N44996;AKOS BBS-00005674;2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-aMine;4-Quinolinamine, 1,2,3,4-tetrahydro-2-methyl-N-phenyl-;Quinaldine,4-anilino-1,2,3,4-tetrahydro- (6CI,7CI,8CI);(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE;N-(2-METHYL-1,2,3,4-TETRAHYDRO-4-QUINOLINYL)-N-PHENYLAMINE;Propanedinitrile,2-(3-cyano-4,5,5-trimethyl-2(7H)-furanylidene)-
CBNumber: CB5278343
Molecular Formula: C16H18N2
Formula Weight: 238.33
MOL File: 1026-05-7.mol

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(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Property

Melting point:: 126 °C
Boiling point:: 400.4±44.0 °C(Predicted)
Density: 1.097±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 4.16±0.60(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Ark Pharm

Product number: P000564070
Product name: 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
Purity: 95+%
Packaging: 100mg
Price: $55
Updated: 2021/12/16

Ark Pharm

Product number: P000564070
Product name: 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
Purity: 95+%
Packaging: 250mg
Price: $88
Updated: 2021/12/16

AK Scientific

Product number: 7665AC
Product name: 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
Packaging: 250mg
Price: $212
Updated: 2021/12/16

Ark Pharm

Product number: P000564070
Product name: 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
Purity: 95+%
Packaging: 1g
Price: $220
Updated: 2021/12/16

Matrix Scientific

Product number: 080572
Product name: 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
Packaging: 500mg
Price: $252
Updated: 2021/12/16

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(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Chemical Properties,Usage,Production

Synthesis

15727-49-8

1026-05-7

General procedure for the synthesis of 2-methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine from 2-phenylaminopropionic acid: 2-phenylaminopropionic acid (66 mg, 0.4 mmol) and 4?molecular sieves (100 mg) were added to a 10 mL reaction vial, dried with an air pump, and then 200 μL of a reaction vial containing an organic photocatalyst, DPZ (0.28 mg 0.0008 mmol) in toluene solution. Subsequently, 4 mL of purified water was added, the reaction mixture was dried with chloroform, and the mouth of the flask was sealed with a rubber stopper and a balloon filled with dry air was inserted. The reaction flask was placed in a 25°C incubator and the reaction was stirred for 15 h under the illumination of two 1 W blue LEDs. Upon completion of the reaction, about 2/3 of the solvent was removed by distillation using a rotary evaporator. Purification by column chromatography (eluent: hexane/ethyl acetate, 60:30:1) afforded 2-methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine (39.1 mg, 82% yield) as a colorless oily liquid.

References

[1] Patent: CN108017579, 2018, A. Location in patent: Paragraph 0008; 0011; 0012

(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Suppliers

China 17 Germany 1 India 2 Russia 1 United States 8 Global 29

SynAsst Chemical.

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Energy Chemical

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Hangzhou Taorui Biotechnology Co., Ltd

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1026-05-7, (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINERelated Search:

AKOS BBS-00005675 (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE AKOS BBS-00005685 AKOS BBS-00005684 AKOS BBS-00005686 1-(4-(O-TOLUIDINO)-2,8-DIMETHYL-3,4-DIHYDROQUINOLIN-1(2H)-YL)BUTAN-1-ONE 4-ANILINO-1-BENZOYL-2-METHYL-1,2,3,4-TETRAHYDROQUINOLINE AKOS BBS-00005690 1-(4-(O-TOLUIDINO)-2,8-DIMETHYL-3,4-DIHYDROQUINOLIN-1(2H)-YL)PENTAN-1-ONE AKOS BBS-00005691 2-METHYL-N-PHENYL-1-(P-TOLYLSULFONYL)-1,2,3,4-TETRAHYDROQUINOLIN-4-AMINE (4-(O-TOLUIDINO)-2,8-DIMETHYL-3,4-DIHYDROQUINOLIN-1(2H)-YL)(3-FLUOROPHENYL)METHANONE N-(2-METHYL-1-OCTANOYL-1,2,3,4-TETRAHYDROQUINOLIN-4-YL)-4-NITRO-N-PHENYLBENZAMIDE AKOS BBS-00005683 AKOS BBS-00005688 2-(3,4-DIMETHOXYPHENYL)-1-(2-METHYL-4-(PHENYLAMINO)-3,4-DIHYDROQUINOLIN-1(2H)-YL)ETHANONE AKOS BBS-00005689 (4-(O-TOLUIDINO)-2,8-DIMETHYL-3,4-DIHYDROQUINOLIN-1(2H)-YL)(P-TOLYL)METHANONE

AKOS BBS-00005674

(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE

Quinaldine,4-anilino-1,2,3,4-tetrahydro- (6CI,7CI,8CI)

ASISCHEM N44996

N-(2-METHYL-1,2,3,4-TETRAHYDRO-4-QUINOLINYL)-N-PHENYLAMINE

2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-aMine

4-Quinolinamine, 1,2,3,4-tetrahydro-2-methyl-N-phenyl-

Propanedinitrile,2-(3-cyano-4,5,5-trimethyl-2(7H)-furanylidene)-

1026-05-7