(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE
- Product Name
- (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE
- CAS No.
- 1026-05-7
- Chemical Name
- (2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE
- Synonyms
- ASISCHEM N44996;AKOS BBS-00005674;2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-aMine;4-Quinolinamine, 1,2,3,4-tetrahydro-2-methyl-N-phenyl-;Quinaldine,4-anilino-1,2,3,4-tetrahydro- (6CI,7CI,8CI);(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE;N-(2-METHYL-1,2,3,4-TETRAHYDRO-4-QUINOLINYL)-N-PHENYLAMINE;Propanedinitrile,2-(3-cyano-4,5,5-trimethyl-2(7H)-furanylidene)-
- CBNumber
- CB5278343
- Molecular Formula
- C16H18N2
- Formula Weight
- 238.33
- MOL File
- 1026-05-7.mol
(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Property
- Melting point:
- 126 °C
- Boiling point:
- 400.4±44.0 °C(Predicted)
- Density
- 1.097±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 4.16±0.60(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- P000564070
- Product name
- 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- P000564070
- Product name
- 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $88
- Updated
- 2021/12/16
- Product number
- 7665AC
- Product name
- 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
- Packaging
- 250mg
- Price
- $212
- Updated
- 2021/12/16
- Product number
- P000564070
- Product name
- 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $220
- Updated
- 2021/12/16
- Product number
- 080572
- Product name
- 2-Methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine
- Packaging
- 500mg
- Price
- $252
- Updated
- 2021/12/16
(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Chemical Properties,Usage,Production
Synthesis
15727-49-8
1026-05-7
General procedure for the synthesis of 2-methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine from 2-phenylaminopropionic acid: 2-phenylaminopropionic acid (66 mg, 0.4 mmol) and 4?molecular sieves (100 mg) were added to a 10 mL reaction vial, dried with an air pump, and then 200 μL of a reaction vial containing an organic photocatalyst, DPZ (0.28 mg 0.0008 mmol) in toluene solution. Subsequently, 4 mL of purified water was added, the reaction mixture was dried with chloroform, and the mouth of the flask was sealed with a rubber stopper and a balloon filled with dry air was inserted. The reaction flask was placed in a 25°C incubator and the reaction was stirred for 15 h under the illumination of two 1 W blue LEDs. Upon completion of the reaction, about 2/3 of the solvent was removed by distillation using a rotary evaporator. Purification by column chromatography (eluent: hexane/ethyl acetate, 60:30:1) afforded 2-methyl-N-phenyl-1,2,3,4-tetrahydroquinolin-4-amine (39.1 mg, 82% yield) as a colorless oily liquid.
References
[1] Patent: CN108017579, 2018, A. Location in patent: Paragraph 0008; 0011; 0012
(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Preparation Products And Raw materials
Raw materials
Preparation Products
(2-METHYL-1,2,3,4-TETRAHYDRO-QUINOLIN-4-YL)-PHENYL-AMINE Suppliers
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