ChemicalBook > CAS DataBase List > FMOC-LYS(ALOC)-OH

FMOC-LYS(ALOC)-OH

Product Name: FMOC-LYS(ALOC)-OH
CAS No.: 146982-27-6
Chemical Name: FMOC-LYS(ALOC)-OH
Synonyms: FMOC-LYS(ALOC)-OH;Fmoc-L-Lys(Alloc);FMOC-LYS(ALLOC)-OH;FMOC-L-LYS(ALOC)-OH;FMOC-L-LYS(ALLOC)-OH;FMOC-LYSINE(ALOC)-OH;FMOC-N-E-ALLOC-L-LYSINE;nα-fmoc-nε-alloc-l-lysine;Fmoc-Lys(Alloc)-OH 98%min;FMOC-N-EPSILON-ALLOC-L-LYSINE
CBNumber: CB5292327
Molecular Formula: C25H28N2O6
Formula Weight: 452.5
MOL File: 146982-27-6.mol

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FMOC-LYS(ALOC)-OH Property

Melting point:: 87-91°C
Boiling point:: 689.7±55.0 °C(Predicted)
Density: 1.237±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
solubility: Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
pka: 3.88±0.21(Predicted)
form: Solid
color: White to off-white
optical activity: [α]20/D 12±1°, c = 1% in DMF
BRN: 5893081
InChIKey: OJBNDXHENJDCBA-QFIPXVFZSA-N
SMILES: C(O)(=O)[C@H](CCCCNC(OCC=C)=O)NC(OCC1C2=C(C=CC=C2)C2=C1C=CC=C2)=O
CAS DataBase Reference: 146982-27-6(CAS DataBase Reference)

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Safety

Safety Statements: 22-24/25
WGK Germany: 3
HS Code: 2924 29 70

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 8.52124
Product name: Fmoc-Lys(Alloc)-OH
Purity: Novabiochem?
Packaging: 5G
Price: $95.9
Updated: 2025/07/31

Sigma-Aldrich

Product number: 8.52124
Product name: Fmoc-Lys(Alloc)-OH
Purity: Novabiochem?
Packaging: 25g
Price: $545
Updated: 2025/07/31

Sigma-Aldrich

Product number: 8.52124
Product name: Fmoc-Lys(Alloc)-OH
Purity: Novabiochem<SUP>®</SUP>
Packaging: 100 g
Price: $2050
Updated: 2025/07/31

Sigma-Aldrich

Product number: 8.52124
Product name: Fmoc-Lys(Alloc)-OH
Purity: Novabiochem<SUP>®</SUP>
Packaging: 100 g
Price: $2050
Updated: 2025/07/31

Sigma-Aldrich

Product number: 47583
Product name: Fmoc-Lys(Alloc)-OH
Purity: ≥95.0% (HPLC)
Packaging: 1g
Price: $44.05
Updated: 2025/07/31

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FMOC-LYS(ALOC)-OH Chemical Properties,Usage,Production

Chemical Properties

White powder

Uses

FMOC-LYS(ALOC)-OH is most often used in peptide synthesis.

reaction suitability

reaction type: Fmoc solid-phase peptide synthesis

Synthesis

105047-45-8

2937-50-0

146982-27-6

The general procedure for the synthesis of N-[(9H-fluoren-9-ylmethoxy)carbonyl]-N'-[(2-propenyloxy)carbonyl]-L-lysine from (S)-2-((9H-fluoren-9-ylmethoxy)methoxy)carbonyl)amino)-6-aminohexanoic acid and allyl chloroformate was as follows: Example L1c: 25 g (61.7 mmol) of (S)-6-amino-2-(9H-fluoren-9-ylmethoxycarbonylamino)-hexanoic acid was dissolved in 275 mL of dioxane and mixed with 25 mL of 25% potassium carbonate solution, followed by the addition of 6.55 mL of allyl chloroformate. The reaction mixture was stirred at 23°C for 20 hours. Upon completion of the reaction, the reaction solution was diluted with water and extracted with methyl tert-butyl ether. The aqueous phase was separated, acidified with 2N hydrochloric acid and extracted with dichloromethane several times. The dichloromethane phase was combined and dried with sodium sulfate. After filtration, the solvent was removed under reduced pressure to afford 26.3 g (58.1 mmol, 94%) of N-[(9H-fluoren-9-methoxy)carbonyl]-N'-[(2-propenyloxy)carbonyl]-L-lysine, and the product could be used for subsequent reactions without further purification.

References

[1] Patent: US2005/234247, 2005, A1. Location in patent: Page/Page column 15
[2] ChemBioChem, 2010, vol. 11, # 8, p. 1083 - 1092

FMOC-LYS(ALOC)-OH Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from FMOC-LYS(ALOC)-OH manufacturers

Hefei Lbao Physical & Chemical Science Co.,Ltd

Product: Fmoc-Lys(Alloc)-OH 146982-27-6
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: Customise
Release date: 2025-10-09

Shanghai Joiny Pharmaceutical Co.,LTD

Product: N-Fmoc-N'-allyoxycarbonyl-L-lysine 146982-27-6
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 1000kg
Release date: 2025-09-22

Sichuan HongRi Pharma-Tech Co.,Ltd

Product: Fmoc-L-Lys(Alloc)-OH 146982-27-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1T
Release date: 2024-03-06

146982-27-6, FMOC-LYS(ALOC)-OHRelated Search:

Tert-butyl bis(2-chloroethyl)carbamate Fmoc-S-acetamidomethyl-L-cysteine Fmoc-D-Lys(ipr,Boc)-OH FMOC-LYS(MCA)-OH N(ALPHA)-FMOC-N(EPSILON)-DABCYL-L-LYSINE Fmoc-Lys(nicotinoyl)-OH FMOC-LYS(5-FAM)-OH Fmoc-HoLys(N3)-OH Nalpha-FMOC-L-Tryptophan FMOC-D-Lys(BOC)-OH Fmoc-O-trityl-L-serine Boc-Lys(Boc)-OH Fmoc-Trp(Boc)-OH Fmoc-Lys(Boc)-OH Fmoc-D-Trp(Boc)-OH Fmoc-O-tert-butyl-D-threonine L-Fmoc-Aspartic acid alpha-tert-butyl ester FMOC-L-TYR(ALL)-OH

N-ALPHA-(9-FLUORENYLMETHYLOXYCARBONYL)-N-EPSILON-ALLYL-OXYCARBONYL-L-LYSINE

N-ALPHA-(9-FLUORENYLMETHOXYCARBONYL)-N-EPSILON-ALLYLOXYCARBONYL-L-LYSINE

N-ALPHA-FMOC-N-EPSILON-ALLYLOXYCARBONYL-L-LYSINE

N-ALPHA-FMOC-N-EPSILON-ALLOC-L-LYSINE

FMOC-LYS(ALLOC)-OH

FMOC-LYS(ALOC)-OH

FMOC-LYSINE(ALOC)-OH

FMOC-L-LYS(ALLOC)-OH

FMOC-L-LYS(ALOC)-OH

FMOC-N-EPSILON-ALLOC-L-LYSINE

FMOC-N-EPSILON-ALLYLOXYCARBONYL-L-LYSINE

N-α-Fmoc-N-ε-allyoxycarbonyl-L-lysine

nα-fmoc-nε-alloc-l-lysine

FMOC-(ALLYLOXYCARBONYL)-LYSINE

FMOC-N-E-ALLOC-L-LYSINE

N-.ALPHA.-FMOC-N-.EPSILON.-ALLYOXYCARBONYL-L-LYSINE

N-Fmoc-N-allyloxycarbonyl L-lysine

N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N6-[(2-propen-1-yloxy)carbonyl]-L-Lysine

FMoc-Lys(Alloc)-OH N-α-FMoc-N-ε-allyoxycarbonyl-L-lysine

(2S)-6-{[(allyloxy)carbonyl]aMino}-2-{[(9H-fluoren-9-ylMethoxy)carbonyl]aMino}hexanoic acid

N^e-Allyloxycarbonyl-N^a-FMoc-L-lysine, 95%

(S)-2-((((9H-fFuoren-9-yl)Methoxy)carbonyl)aMino)-6-(((allyloxy)carbonyl)aMino)hexanoic acid

L-Lysine, N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N6-[(2-propen-1-yloxy)carbonyl]-

Fmoc-Lys(Alloc)-OH >=95.0% (HPLC)

Nα-Fmoc-Nε-allyloxycarbonyl-L-lysine≥ 99.9% (HPLC, Chiral purity)

Nepsilon-Allyloxycarbonyl-Nalpha-Fmoc-L-lysine

(9H-Fluoren-9-yl)MethOxy]Carbonyl L-Lys(Alloc)-OH

N2-Fmoc-N6-[(allyloxy)carbonyl]-L-lysine

Fmoc-L-Lys(Alloc)

(2S)-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-6-{[(prop-2-en-1-yloxy)carbonyl]amino}hexanoic acid

N6-[(Allyloxy)carbonyl]-N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-lysine

Nepsilon-Alloc-Nalpha-Fmoc-L-lysine

Nα-Fmoc-Nε-allyloxycarbonyl-L-lysine

N - [(9h fluorene-9-methoxy) carbonyl] - n '- [(2-propenoxy) carbonyl] - l-lysine

(S)-2-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-6-(((allyloxy)carbonyl)amino)hexanoic acid

Fluorene methoxycarbonyl-lysine(ALLOC)

Fmoc-Lys(Alloc)-OH 98%min

146982-27-6

1146982-27-6

Analytical Standards

Alphabetic

Analytical Chromatography Product Catalog

FM - FZ

peptides

Lysine [Lys, K]

Fmoc-Amino Acids and Derivatives

Amino Acids