ChemicalBook > CAS DataBase List > 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

Product Name: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE
CAS No.: 400-67-9
Chemical Name: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE
Synonyms: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE;2-CHLORO-4-NITRO-6-(TRIFLUOROMETHYL)ANILINE;2-Amino-3-chloro-5-nitrobenzotrifluoride98%;2-Amino-3-chloro-5-nitrobenzotrifluoride 98%;2-Chloro-4-nitro-6-trifluoromethyl-phenylamine;Benzenamine,2-chloro-4-nitro-6-(trifluoromethyl)-;Benzenamine, 2-Chloro-4-nitro-6-trifluoromethylphenylamine;2-AMino-3-chloro-5-nitrobenzotrifluoride[2-chloro-4-nitro-6-(trifluoroMethyl)aniline]
CBNumber: CB5307854
Molecular Formula: C7H4ClF3N2O2
Formula Weight: 240.57
MOL File: 400-67-9.mol

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2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE Property

Melting point:: 115-116 °C(Solv: acetic acid (64-19-7))
Boiling point:: 286.0±35.0 °C(Predicted)
Density: 1.614±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: -3.90±0.46(Predicted)
CAS DataBase Reference: 400-67-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
Hazard Note: Irritant
HS Code: 2921490090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: A604213
Product name: 2-Amino-3-chloro-5-nitrobenzotrifluoride
Packaging: 500mg
Price: $155
Updated: 2021/12/16

TRC

Product number: A604213
Product name: 2-Amino-3-chloro-5-nitrobenzotrifluoride
Packaging: 50mg
Price: $45
Updated: 2021/12/16

ChemScene

Product number: CS-D0129
Product name: Benzenamine,2-Chloro-4-nitro-6-trifluoromethylphenylamine
Purity: >97.0%
Packaging: 5g
Price: $114
Updated: 2021/12/16

AK Scientific

Product number: 5304AB
Product name: 2-Amino-3-chloro-5-nitrobenzotrifluoride
Packaging: 25g
Price: $784
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0018270
Product name: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE
Purity: 95.00%
Packaging: 1G
Price: $788.87
Updated: 2021/12/16

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2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE Chemical Properties,Usage,Production

Uses

2-Amino-3-chloro-5-nitrobenzotrifluoride is a useful intermediate for the preparation of monoazo dyes.

Synthesis

121-01-7

400-67-9

General procedure for the synthesis of 2-chloro-4-nitro-6-(trifluoromethyl)aniline from 2-amino-5-nitrobenzotrifluoride: 4-nitro-2-(trifluoromethyl)aniline (15 g) and N-chlorosuccinimide (10.7 g) were dissolved in acetonitrile (100 ml) in a sealed microwaveable reaction flask and heated to 150°C for 15 minutes. After completion of the reaction, the mixture was cooled to room temperature and poured into a mixture of 5% sodium hydroxide solution (500 ml) and ethyl acetate (400 ml). The organic phase was separated, dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. Purification by fast column chromatography afforded 17.0 g (97% yield) of 2-chloro-4-nitro-6-(trifluoromethyl)aniline as a yellow solid.LC-MS (m/z) 240 (MH+); tR=4.76, (UV, ELSD) purity 97% and 96%, respectively.1H NMR (500 MHz, DMSO-d6) δ: 7.15 (s , 2H), 8.15 (d, 1H), 8.40 (d, 1H).

References

[1] Patent: WO2006/29623, 2006, A1. Location in patent: Page/Page column 60-61
[2] Patent: WO2005/87754, 2005, A1. Location in patent: Page/Page column 46
[3] Industrial and Engineering Chemistry, 1953, vol. 45, p. 1730,1732
[4] Industrial and Engineering Chemistry, 1954, vol. 46, p. 2213,2218, 2219

2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE Suppliers

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View Lastest Price from 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE 400-67-9
Price: US $1.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200000KG
Release date: 2024-07-24

Career Henan Chemical Co

Product: 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE 400-67-9
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200KG
Release date: 2020-02-20

400-67-9, 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDERelated Search:

5-AMINO-2-CHLORO-4-NITROBENZOTRIFLUORIDE 4-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE 3-AMINO-4-CHLORO-5-NITROBENZOTRIFLUORIDE 2-AMINO-5-CHLORO-3-NITROBENZOTRIFLUORIDE,2-Amino-5-chloro-3-nitrobenzotrifluoride98% 4-AMINO-2-CHLORO-5-NITROBENZOTRIFLUORIDE 2-CHLORO-6-METHYL-4-NITROANILINE 3-AMINO-5-CHLOROBENZOTRIFLUORIDE 2-AMINO-3-CHLOROBENZOTRIFLUORIDE 3-Chloro-5-nitrobenzotrifluoride 2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

2-Amino-3-chloro-5-nitrobenzotrifluoride 98%

2-Amino-3-chloro-5-nitrobenzotrifluoride98%

2-AMino-3-chloro-5-nitrobenzotrifluoride[2-chloro-4-nitro-6-(trifluoroMethyl)aniline]

2-Chloro-4-nitro-6-trifluoromethyl-phenylamine

2-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE

2-CHLORO-4-NITRO-6-(TRIFLUOROMETHYL)ANILINE

Benzenamine, 2-Chloro-4-nitro-6-trifluoromethylphenylamine

Benzenamine,2-chloro-4-nitro-6-(trifluoromethyl)-

400-67-9