3-AMINO-5-CHLOROBENZOTRIFLUORIDE
- Product Name
- 3-AMINO-5-CHLOROBENZOTRIFLUORIDE
- CAS No.
- 69411-05-8
- Chemical Name
- 3-AMINO-5-CHLOROBENZOTRIFLUORIDE
- Synonyms
- 3-AMINO-5-CHLOROBENZOTRIFLORIDE;3-AMINO-5-CHLOROBENZOTRIFLUORIDE;3-CHLORO-5-(TRIFLUOROMETHYL)ANILINE;3-Chloro-5-trifluoromethylbenzenamine;Benzenamine, 3-chloro-5-(trifluoromethyl)-;3-chloro-5-(trifluoromethyl)aniline hydrochloride;3-AMINO-5-CHLORO-1-TRIFLUOROMETHYLBENZENE HYDROCHLORIDE;3-AMino-5-chlorobenzotrifluoride[3-Chloro-5-(trifluoroMethyl)aniline]
- CBNumber
- CB3230275
- Molecular Formula
- C7H5ClF3N
- Formula Weight
- 195.57
- MOL File
- 69411-05-8.mol
3-AMINO-5-CHLOROBENZOTRIFLUORIDE Property
- Boiling point:
- 218.2±40.0 °C(Predicted)
- Density
- 1.43
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 2.32±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
- CAS DataBase Reference
- 69411-05-8(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi
- Risk Statements
- 20/21/22-36/37/38-36-36/38
- Safety Statements
- 26-36/37/39-36/37
- RIDADR
- 2810
- Hazard Note
- Irritant
- HazardClass
- 6.1
- HS Code
- 29214300
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H331Toxic if inhaled
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C598140
- Product name
- 3-Chloro-5-trifluoromethylaniline
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C598140
- Product name
- 3-Chloro-5-trifluoromethylaniline
- Packaging
- 5g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 3830-7-X2
- Product name
- 3-Amino-5-chlorobenzotrifluoride
- Packaging
- 1g
- Price
- $16
- Updated
- 2021/12/16
- Product number
- 054382
- Product name
- 3-Amino-5-chlorobenzotrifluoride
- Purity
- 97%
- Packaging
- 5g
- Price
- $28
- Updated
- 2021/12/16
- Product number
- J90678
- Product name
- 3-Chloro-5-trifluoromethylaniline
- Packaging
- 5g
- Price
- $29
- Updated
- 2021/12/16
3-AMINO-5-CHLOROBENZOTRIFLUORIDE Chemical Properties,Usage,Production
Synthesis
401-93-4
69411-05-8
General procedure for the synthesis of 3-amino-5-chlorobenzotrifluoride from 3-chloro-5-nitrobenzotrifluoride: To a stirred mixture of 3-chloro-5-nitrobenzotrifluoride (2.90 g, 12.9 mmol) in 120 mL of ethyl acetate (EtOAc) was added stannous chloride dihydrate (SnCl2-2H2O, 12.0 g, 51.6 mmol). The reaction mixture was heated to reflux and kept for 3 hours and then cooled to room temperature. Subsequently, the reaction mixture was diluted with 100 mL of EtOAc and washed with 2.5 N sodium hydroxide (NaOH) solution (1 × 150 mL). After separation of the aqueous layer, the aqueous layer was back-extracted with EtOAc (1 × 200 mL). All EtOAc layers were combined, washed with brine (1 × 40 mL), dried over anhydrous magnesium sulfate (MgSO4), filtered, and concentrated under reduced pressure to give 2.51 g of the target product 3-amino-5-chlorobenzotrifluoride (yellow solid) in quantitative yield.HPLC analytical conditions: a Chromolith SpeedROD column (4.6 × 50 mm), a mobile phase containing Chromolith SpeedROD column (4.6×50 mm), mobile phase was 10-90% aqueous methanol containing 0.2% phosphoric acid at a flow rate of 4 mL/min, detection wavelength 220 nm, and retention time (RT) 2.57 min. Mass spectrum (electrospray ionization, ES): m/z = 196 [M + H]+.
References
[1] Patent: WO2009/3077, 2008, A1. Location in patent: Page/Page column 135
[2] Patent: US2003/158409, 2003, A1
[3] Patent: US2002/10181, 2002, A1
[4] Patent: US5599814, 1997, A
3-AMINO-5-CHLOROBENZOTRIFLUORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-AMINO-5-CHLOROBENZOTRIFLUORIDE manufacturers
- Product
- 3-AMINO-5-CHLOROBENZOTRIFLUORIDE 69411-05-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-18
- Product
- 3-Chloro-5-(trifluoromethyl)aniline 69411-05-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 50mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-08
- Product
- 3-AMINO-5-CHLOROBENZOTRIFLUORIDE 69411-05-8
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-07-10