ChemicalBook > CAS DataBase List > 2,6-Dimethylbenzyl alcohol

2,6-Dimethylbenzyl alcohol

Product Name
2,6-Dimethylbenzyl alcohol
CAS No.
62285-58-9
Chemical Name
2,6-Dimethylbenzyl alcohol
Synonyms
RARECHEM AL BD 0363;6-Dimethylbenzyl alcohol;2,6-DIMETHYLBENZYL ALCOHOL;2,6-DIMETHYL-BENZENEMETHANOL;2,6-Dimethylbenzylalcohol,98%;(2,6-DIMETHYL-PHENYL)-METHANOL;Benzenemethanol, 2,6-dimethyl-;2,6-Dimethylbenzyl alcohol ,97%
CBNumber
CB5322097
Molecular Formula
C9H12O
Formula Weight
136.19
MOL File
62285-58-9.mol
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2,6-Dimethylbenzyl alcohol Property

Melting point:
81-82 °C(Solv: ligroine (8032-32-4))
Boiling point:
120°C 12mm
Density 
1.002±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
14.38±0.10(Predicted)
form 
Solid
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Safety

Safety Statements 
24/25
HS Code 
29062990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
D481050
Product name
(2,6-Dimethylphenyl)methanol
Packaging
100mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD50915
Product name
2,6-Dimethylbenzyl alcohol
Packaging
2g
Price
$89.16
Updated
2021/12/16
AK Scientific
Product number
X8348
Product name
2,6-Dimethylbenzylalcohol
Packaging
1g
Price
$38
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD50915
Product name
2,6-Dimethylbenzyl alcohol
Packaging
1g
Price
$55.7
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD50915
Product name
2,6-Dimethylbenzyl alcohol
Packaging
5G
Price
$183.75
Updated
2021/12/16
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2,6-Dimethylbenzyl alcohol Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

632-46-2

62285-58-9

Synthesis of 2,6-dimethylbenzyl alcohol: The synthesis of 2,6-dimethylbenzyl alcohol was carried out with reference to the method of Beaulieu et al. (2000) but the original method was unsuccessful, so it was changed to a different reducing agent. 2,6-dimethylbenzoic acid (1.00 g, 6.65 mmol) was suspended in anhydrous THF (10 mL) under nitrogen protection and a THF solution of BH3 (SMe2) was slowly added. The reaction mixture was heated under reflux conditions for 16 h. The reaction was subsequently quenched with saturated ammonium chloride solution (5 mL) and 2 M HCl (10 mL) (note: there was a violent gas release during the reaction). The organic layer was separated and the aqueous layer was extracted three times with ethyl acetate (45 mL each time). The organic extracts were combined, washed twice sequentially with saturated sodium bicarbonate solution (20 mL each time), dried over anhydrous Na2SO4, concentrated under reduced pressure, and finally purified by silica gel column chromatography to give 2,6-dimethylbenzyl alcohol (0.50 g, 51% yield) as a white solid.1H NMR (400 MHz, CDCl3): δ7.08 (m, 3H, Ph-H), δ7.08 (m, 3H, Ph-H), δ7.08 (m, 3H, 2H), δ7.08 (m, 3H, 2H, 2H). 4.70 (s, 2H, Ph-CH2), 4.05 (br s, 1H, OH), 2.40 (s, 6H, CH3).

References

[1] Bioorganic and Medicinal Chemistry, 1996, vol. 4, # 12, p. 2167 - 2178
[2] Patent: US2016/193181, 2016, A1. Location in patent: Paragraph 1161-1162
[3] Patent: WO2008/131368, 2008, A2. Location in patent: Page/Page column 116-117
[4] Tetrahedron, 2001, vol. 57, # 30, p. 6375 - 6382
[5] ChemMedChem, 2016, vol. 11, # 23, p. 2607 - 2620

2,6-Dimethylbenzyl alcohol Preparation Products And Raw materials

Raw materials

Sodium nitrite Hydrogen bromide Tetrahydrofuran Diethyl ether Cuprous bromide Lithium Aluminum Hydride 2,6-Dimethylaniline Bromoethane Magnesium

Preparation Products

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View Lastest Price from 2,6-Dimethylbenzyl alcohol manufacturers

Career Henan Chemical Co
Product
2,6-Dimethylbenzyl alcohol 62285-58-9
Price
US $1.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
100KG
Release date
2018-12-21

62285-58-9, 2,6-Dimethylbenzyl alcoholRelated Search:

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  • RARECHEM AL BD 0363
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  • 2,6-Dimethylbenzylalcohol,98%
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  • 62285-58-9
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