ChemicalBook > CAS DataBase List > 1,10-Phenanthrolin-5-amine

1,10-Phenanthrolin-5-amine

Product Name: 1,10-Phenanthrolin-5-amine
CAS No.: 54258-41-2
Chemical Name: 1,10-Phenanthrolin-5-amine
Synonyms: 5-AMinophenanthroline;5-AMino-o-phenanthroline;10-Phenanthrolin-5-amine;1,1-Phenanthrolin-5-amine;5-amino-1,10-phenanroline;Amine-1,10-Phenanthrolin;1,10-phenanthrolin-5-amine;Amino-1,1,0-phenanthroline;5-Amine-1,1-phenanthroline;5-AMine-1,10-phenanthroline
CBNumber: CB5363511
Molecular Formula: C12H9N3
Formula Weight: 195.22
MOL File: 54258-41-2.mol

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1,10-Phenanthrolin-5-amine Property

Melting point:: 254-258 °C (lit.)
Boiling point:: 197-198 °C
Density: 1.333±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: DMSO (Sparingly), Methanol (Sparingly)
form: Solid
pka: 5.20±0.10(Predicted)
color: Yellow to Orange
InChIKey: DKPSSMOJHLISJI-UHFFFAOYSA-N

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Safety

Hazard Codes: Xn
Risk Statements: 22-41-43
Safety Statements: 26-36/37/39
WGK Germany: 3
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 631507
Product name: 1,10-Phenanthrolin-5-amine
Purity: 97%
Packaging: 1g
Price: $187
Updated: 2025/07/31

Sigma-Aldrich

Product number: 631507
Product name: 1,10-Phenanthrolin-5-amine
Purity: 97%
Packaging: 5g
Price: $590
Updated: 2025/07/31

TCI Chemical

Product number: A2977
Product name: 5-Amino-1,10-phenanthroline
Purity: >98.0%(GC)
Packaging: 1g
Price: $90
Updated: 2025/07/31

TRC

Product number: P295030
Product name: 1,10-Phenanthrolin-5-amine
Packaging: 5g
Price: $150
Updated: 2021/12/16

Usbiological

Product number: 019356
Product name: 1,10-Phenanthrolin-5-amine
Packaging: 5g
Price: $460
Updated: 2021/12/16

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1,10-Phenanthrolin-5-amine Chemical Properties,Usage,Production

Chemical Properties

Brown to Orange Solid

Uses

1,10-Phenanthrolin-5-amine can be used in the synthesis of bis-[1,10]phenanthrolin-5-yl-pyromellitic diimide (Bphen-PMD), which can find applications in organic light-emitting devices.

Uses

1,10-Phenanthrolin-5-amine is a potential fluorescent label for DNA detection. 1,10-Phenanthrolin-5-amine is used as a mediator for glucose oxidase for development of biosensors and biofuel cells

Synthesis

4199-88-6

54258-41-2

4) Add 0.64 g (6.0 mmol) of 10% palladium-carbon catalyst, 4.85 g of 80% (mass fraction) hydrazine hydrate, and 20.0 mL of anhydrous ethanol to a 250 mL three-neck flask. A reflux condenser was installed and the two remaining ports were sealed with glass stoppers. The device was placed on a DF-101S heated thermostatic magnetic stirrer with the oil bath temperature set to 72 °C and stirring was initiated. Subsequently, 2.03 g (9 mmol) of 5-nitro-1,10-phenanthroline was added to the flask, followed by 40 mL of anhydrous ethanol to ensure complete dissolution (total ethanol volume of 60 mL). The dissolved 5-nitro-1,10-phenanthroline solution was quickly poured into a three-necked flask after the oil bath temperature reached 72 °C. After the reaction lasted for 10 hours, the heating was stopped and left for about 1 hour to ensure complete dissolution of 5-nitro-1,10-phenanthroline. The oil bath was again heated to 60°C. If any precipitate redissolved in the system, the three-necked flask was immediately removed, the solution was poured into a thermal filter, and the residue was washed with anhydrous ethanol about five times. The filtrate was collected and concentrated using a rotary evaporator to remove the solvent, yielding a yellow solid. The solid was dried in a vacuum oven at 60 °C for 12 hours. Finally, the product was recrystallized with anhydrous ethanol, filtered and dried under vacuum at 60 °C for 12 h to give 1.28 g of yellow-brown solid powder, 5-amino-1,10-phenanthroline (Phen-NH2), in 72.9% yield.

References

[1] Chemical Communications, 2006, # 43, p. 4539 - 4541
[2] European Journal of Inorganic Chemistry, 2008, # 10, p. 1559 - 1564
[3] Tetrahedron Letters, 2007, vol. 48, # 18, p. 3135 - 3139
[4] Journal of the American Chemical Society, 2003, vol. 125, # 40, p. 12062 - 12063
[5] Patent: US2007/276104, 2007, A1

1,10-Phenanthrolin-5-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,10-Phenanthrolin-5-amine manufacturers

Shanghai UCHEM Inc.

Product: 5-Amino-1,10-phenanthroline 54258-41-2
Price: US $37.00-577.00/g
Min. Order: 1g
Purity: 0.98
Supply Ability: 10kg
Release date: 2023-10-17

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1,10-Phenanthrolin-5-amine 97% 54258-41-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

Career Henan Chemical Co

Product: 10-Phenanthrolin-5-amine 54258-41-2
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1000KGS
Release date: 2019-12-20

54258-41-2, 1,10-Phenanthrolin-5-amineRelated Search:

2-methyl-1,10-phenanthroline 5-METHYL-1,10-PHENANTHROLINE 5-CHLORO-1,10-PHENANTHROLINE Bathocuproine 1,10-Phenanthroline-4-carboxaldehyde 2-Bromo-1,10-phenanthroline Neocuproine 3,4,7,8-Tetramethyl-1,10-phenanthroline o-Phenanthroline 1,10-Phenanthrolin-5-amine 5-Nitro-1,10-phenanthroline 5-NITRO-1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID 5-Isothiocyanato-1,10-phenanthroline 2,9-DI-N-BUTYL-5-PICRYLAMINO-1,10-PHENANTHROLINE 2 9-DIMETHYL-5-PICRYLAMINO-O-PHEN- 5-NITRO-1,10-PHENANTHROLINE FERROUS PERCHLORATE TRIS(DIBENZOYLMETHANE) MONO(5-AMINOPHENANTHROLINE)EUROPIUM (III) 5-NITRO-1,10-PHENANTHROLINE FERROUS SULFATE

(1,10)PHENANTHROLIN-5-YLAMINE

Amino-1,1,0-phenanthroline

1,10-phenanthrolin-5-amine

5-AMINO-1,10-PHENANTHROLINE

1,10-Phenanthrolin-5-amine,(1,10)-Phenanthrolin-5-ylamine

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5-AMinophenanthroline

5-AMine-1,10-phenanthroline

1,10-Phenanthrolin-5-aMine 97%

5-amino-1,10-phenanroline

1,1-Phenanthrolin-5-amine

10-Phenanthrolin-5-amine

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1,10-phenanthroline-5-amine

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54258-41-2

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