3-NITRO-2-PYRIDINESULFENYL CHLORIDE
- Product Name
- 3-NITRO-2-PYRIDINESULFENYL CHLORIDE
- CAS No.
- 68206-45-1
- Chemical Name
- 3-NITRO-2-PYRIDINESULFENYL CHLORIDE
- Synonyms
- NPYS-CL;OxytocinImpurity16;3-nitro-2-pyridinesulfenyl;2-(chlorosulfanyl)-3-nitropyridine;3-NITRO-2-PYRIDINESULFENYL CHLORIDE;2-Pyridinesulfenyl chloride, 3-nitro-;3-Nitropyridin-2-yl hypochlorothioite;(3-nitropyridin-2-yl)sulfanyl]chlorane;(3-nitropyridin-2-yl) thiohypochlorite;3-Nitro-2-pyridinesulfenyl chloride 95%
- CBNumber
- CB5384130
- Molecular Formula
- C5H3ClN2O2S
- Formula Weight
- 190.61
- MOL File
- 68206-45-1.mol
3-NITRO-2-PYRIDINESULFENYL CHLORIDE Property
- Melting point:
- 205 °C (dec.) (lit.)
- Boiling point:
- 376.8±27.0 °C(Predicted)
- Density
- 1.58±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- solubility
- dichloromethane: soluble(lit.)
- pka
- -3.72±0.29(Predicted)
Safety
- Hazard Codes
- C
- Risk Statements
- 34
- Safety Statements
- 26-27-36/37/39-45
- RIDADR
- UN 3261 8/PG 2
- WGK Germany
- 3
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P363Wash contaminated clothing before reuse.
N-Bromosuccinimide Price
- Product number
- 303232
- Product name
- 3-Nitro-2-pyridinesulfenyl chloride
- Purity
- 95%
- Packaging
- 1g
- Price
- $230
- Updated
- 2024/03/01
- Product number
- B506343
- Product name
- [(3-nitropyridin-2-yl)sulfanyl]chlorane
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 0378AQ
- Product name
- 3-Nitro-2-pyridinesulfenyl chloride
- Packaging
- 1g
- Price
- $289
- Updated
- 2021/12/16
- Product number
- CHM0115401
- Product name
- 3-NITRO-2-PYRIDINESULFENYL CHLORIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $795.56
- Updated
- 2021/12/16
3-NITRO-2-PYRIDINESULFENYL CHLORIDE Chemical Properties,Usage,Production
Uses
3-Nitro-2-pyridinesulfenyl chloride (NpysCl) was employed as the starting material for the synthesis of N-, O- and S-Npys-protected amino acid.
General Description
The 3-nitro-2-pyridinesulphenyl (Npys) moiety is useful as a protecting-activating group for cysteine, particularly in the synthesis of cyclic and unsymmetrical disulfides. The stability of NpysCl was studied in various solvents.
Purification Methods
The chloride crystallises as yellow needles from CH2Cl2. When pure, it is stable for several weeks at room temperature, and no decomposition was observed after 6 months at <0o. It is moisture sensitive. UV (MeCN) has at 231nm max ( 12,988), 264nm ( 5,784) and 372nm ( 3,117). [NMR and UV: Matsuda & Aiba Chem Lett 951 1978, Wagner et al. Chem Ber 75 935 1942.]
3-NITRO-2-PYRIDINESULFENYL CHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-NITRO-2-PYRIDINESULFENYL CHLORIDE Suppliers
- Tel
- --
- Fax
- --
- tech@kokusan-chem.co.jp
- Country
- Japan
- ProdList
- 1658
- Advantage
- 51
View Lastest Price from 3-NITRO-2-PYRIDINESULFENYL CHLORIDE manufacturers
- Product
- 3-NITRO-2-PYRIDINESULFENYL CHLORIDE 68206-45-1
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- customise
- Release date
- 2018-08-09