2-METHYL-5-NITRONICOTINIC ACID
- Product Name
- 2-METHYL-5-NITRONICOTINIC ACID
- CAS No.
- 59290-81-2
- Chemical Name
- 2-METHYL-5-NITRONICOTINIC ACID
- Synonyms
- IFLAB-BB F2124-0617;2-METHYL-5-NITRONICOTINIC ACID;2-Methyl-5-nitro-3-pyridinecarboxylic acid;2-methyl-5-nitropyridine-3-carboxylic acid;3-Pyridinecarboxylicacid, 2-Methyl-5-nitro-
- CBNumber
- CB5405581
- Molecular Formula
- C7H6N2O4
- Formula Weight
- 182.13
- MOL File
- 59290-81-2.mol
2-METHYL-5-NITRONICOTINIC ACID Property
- Melting point:
- 215-215.5 °C
- Boiling point:
- 370.1±42.0 °C(Predicted)
- Density
- 1.477±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 2.47±0.10(Predicted)
- Appearance
- Light brown to brown Solid
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M342178
- Product name
- 2-Methyl-5-nitro-3-pyridinecarboxylicacid
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- W7225
- Product name
- 2-Methyl-5-nitro-3-pyridinecarboxylicacid
- Packaging
- 250mg
- Price
- $116
- Updated
- 2021/12/16
- Product number
- W7225
- Product name
- 2-Methyl-5-nitro-3-pyridinecarboxylicacid
- Packaging
- 1g
- Price
- $208
- Updated
- 2021/12/16
- Product number
- 027200
- Product name
- 2-Methyl-5-nitronicotinic acid
- Packaging
- 500mg
- Price
- $252
- Updated
- 2021/12/16
- Product number
- CS-W000762
- Product name
- 2-methyl-5-nitronicotinicacid
- Purity
- >97.0%
- Packaging
- 1g
- Price
- $397
- Updated
- 2021/12/16
2-METHYL-5-NITRONICOTINIC ACID Chemical Properties,Usage,Production
Synthesis
51984-71-5
59290-81-2
General procedure for the synthesis of 2-methyl-5-nitronicotinic acid from ethyl 2-methyl-5-nitronicotinate: compound D4 (300 g, 1.4 mol) was dissolved in a mixture of 800 mL hydrochloric acid and 800 mL water. The reaction mixture was heated under reflux conditions for 1 hour. Upon completion of the reaction, it was cooled to room temperature, the reaction solution was diluted with 2.0 L of water and slowly neutralized with the addition of solid sodium bicarbonate to pH=5.0. During this process, a precipitate was gradually formed. The mixture was further cooled and the precipitate was collected by filtration. After drying, brown solid D5 (223 g, 85.7% yield) was obtained. The product was characterized by 1H NMR (DMSO-d6, 300 MHz): δ = 2.84 (s, 3H), 8.74-8.75 (d, 1H), 9.35-9.36 (d, 1H), 13.90 (s, 1H).LC-MS analysis showed that the [M-1]+ peak was located at 180.9.
References
[1] Patent: WO2008/88881, 2008, A1. Location in patent: Page/Page column 33-34
[2] Journal of the American Chemical Society, 1953, vol. 75, p. 737
[3] Patent: WO2007/56016, 2007, A2. Location in patent: Page/Page column 105
2-METHYL-5-NITRONICOTINIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
2-METHYL-5-NITRONICOTINIC ACID Suppliers
- Tel
- 18210857532; 18210857532
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- +86-21-68182121
- Fax
- +86-21-68182121
- Country
- China
- ProdList
- 882
- Advantage
- 52
- Tel
- 4009903999 13355009207
- Fax
- 0539-6365991
- 3007715519@qq.com
- Country
- China
- ProdList
- 18729
- Advantage
- 57
- Tel
- 021-20958197 20965099
- Fax
- 021-20960837
- sales@skychemical.com
- Country
- China
- ProdList
- 1183
- Advantage
- 57
- Tel
- 18270980682
- Fax
- 021 51613951
- mlcheng@sunwaypharm.cn
- Country
- China
- ProdList
- 8669
- Advantage
- 57
- Tel
- 0531-81313138 13066006660
- Fax
- QQ: 3366077777
- chibapharm@foxmail.com
- Country
- China
- ProdList
- 3991
- Advantage
- 55
- Tel
- 021-60343070
- Fax
- 021-35122006
- Country
- China
- ProdList
- 12740
- Advantage
- 55
- Tel
- 021-021-56795766
- Fax
- +86-21-56795266
- sales@worldyachem.com
- Country
- China
- ProdList
- 9476
- Advantage
- 58
- Tel
- 021-61317773
- Fax
- 021-61486878
- sales@aspirebio.com
- Country
- China
- ProdList
- 2880
- Advantage
- 58
- Tel
- 021-60455363 18019463053
- Fax
- 50966098
- sales@coolpharm.com
- Country
- China
- ProdList
- 12346
- Advantage
- 58
- Tel
- Fax
- -
- xg01_gj@163.com
- Country
- China
- ProdList
- 9484
- Advantage
- 50
- Tel
- 0573-11111111-1111 18969316891
- Fax
- -
- richmol@163.com
- Country
- China
- ProdList
- 449
- Advantage
- 50
- Tel
- 021-33926058 18030239092
- Fax
- +86-21-33926078
- xuxin@fenhechem.com
- Country
- China
- ProdList
- 159
- Advantage
- 55
- Tel
- 021-20960837,QQ1332204249
- Fax
- 021-20960837
- sales@skychemical.com
- Country
- China
- ProdList
- 3341
- Advantage
- 55
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 13003356808
- Fax
- QQ:1485751188
- 1485751188@qq.com
- Country
- China
- ProdList
- 403
- Advantage
- 55
- Tel
- 微信 17321281695 18019252918
- Fax
- 021-31261685
- sale@amkchem.com
- Country
- China
- ProdList
- 9405
- Advantage
- 55
- Tel
- 025-87782433 18021532344
- Fax
- 025-87782433
- 1345332203@qq.com
- Country
- China
- ProdList
- 4135
- Advantage
- 58
- Tel
- 028-65791793 18140026355
- Fax
- QQ568470422
- 568470422@qq.com
- Country
- China
- ProdList
- 9997
- Advantage
- 58
- Tel
- 025-58851090 15955137747
- Fax
- (6)02557626880
- sales01@aikonchem.com
- Country
- China
- ProdList
- 15949
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58
- Tel
- 028-84641798 18782128315
- 3302391190@qq.com
- Country
- China
- ProdList
- 9800
- Advantage
- 55
- Tel
- +8618530059196
- sale04@alfachem.cn
- Country
- China
- ProdList
- 11784
- Advantage
- 58
- Tel
- +86-0571-88938639 +8617705817739
- Fax
- +86-571-88938652，+86-571- 88492614
- info@dycnchem.com
- Country
- China
- ProdList
- 52846
- Advantage
- 58
- Tel
- +8617735180244
- mike_yan@xuanranglobal.com
- Country
- CHINA
- ProdList
- 4017
- Advantage
- 58
- Tel
- 13981836672
- 2560370848@qq.com
- Country
- China
- ProdList
- 2807
- Advantage
- 58
- Tel
- +8618523575427
- sales@conier.com
- Country
- China
- ProdList
- 49975
- Advantage
- 58
- Tel
- 021-58461859 15821823057
- service@aiviche.com
- Country
- China
- ProdList
- 49312
- Advantage
- 58
- Tel
- +86-0371-86658258 +8613203830695
- Fax
- 0086-371-86658258
- factory@coreychem.com
- Country
- China
- ProdList
- 29798
- Advantage
- 58
- Tel
- +8613580539051
- joe@yuhengpharm.com
- Country
- CHINA
- ProdList
- 21142
- Advantage
- 58
- Tel
- 0371-0371-55153829 18003835034
- 2853979819@qq.com
- Country
- China
- ProdList
- 9998
- Advantage
- 58
- Tel
- 19033008971 13182942551 19331071838
- wang666xt@163.com
- Country
- China
- ProdList
- 429
- Advantage
- 58
- Tel
- 2383948258 19172820304
- 2383948258@qq.com
- Country
- China
- ProdList
- 12987
- Advantage
- 58
- Tel
- 010-60605840 15801484223;
- psaitong@jm-bio.com
- Country
- China
- ProdList
- 29757
- Advantage
- 58
- Tel
- 400-8210725 4008210725
- malulu@leyan.com
- Country
- China
- ProdList
- 40000
- Advantage
- 58
- Tel
- 16650708709
- Fax
- qq:778660296
- hnyingchuang@163.com
- Country
- China
- ProdList
- 3966
- Advantage
- 58
- Tel
- 400-6005915
- sales@picasso-e.com
- Country
- China
- ProdList
- 39665
- Advantage
- 58
- Tel
- 19713077352
- 1038096457@qq.com
- Country
- China
- ProdList
- 2640
- Advantage
- 58
- Tel
- 029-81145920 17391631969
- 1046@dideu.com
- Country
- China
- ProdList
- 9996
- Advantage
- 58
- Tel
- 010-50973130 17801761073
- Gsiyu@solarbio.com
- Country
- China
- ProdList
- 50464
- Advantage
- 58
- Tel
- 13611612777
- 3627377363@qq.com
- Country
- China
- ProdList
- 4015
- Advantage
- 58
- Tel
- 021-57520305 13795461237
- zhuruyan@jskchem.com
- Country
- China
- ProdList
- 49234
- Advantage
- 58
- Tel
- 4000255188
- marketing@pharmablock.com
- Country
- China
- ProdList
- 9126
- Advantage
- 58
- Tel
- 400-6206333 13167063860
- anhua.mao@aladdin-e.com
- Country
- China
- ProdList
- 48457
- Advantage
- 58
- Tel
- 028-65791793 18140026355
- 568470422@qq.com
- Country
- China
- ProdList
- 9459
- Advantage
- 58
- Tel
- 021-60936350
- scbt@scbt.com
- Country
- China
- ProdList
- 6594
- Advantage
- 58
- Tel
- +86-512-68323658 +86-18168183658
- sales1@artkmedchem.com
- Country
- China
- ProdList
- 39002
- Advantage
- 58
- Tel
- +8618058761490
- info@gihichemicals.com
- Country
- China
- ProdList
- 49934
- Advantage
- 58
- Tel
- +86-85511178;
- peter68@ptchemgroup.com
- Country
- China
- ProdList
- 35425
- Advantage
- 58
- Tel
- 15017560539
- Country
- CHINA
- ProdList
- 142
- Advantage
- 58
View Lastest Price from 2-METHYL-5-NITRONICOTINIC ACID manufacturers
- Product
- 2-METHYL-5-NITRONICOTINIC ACID 59290-81-2
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02