Phenylphosphonic dichloride

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Phenylphosphonic dichloride

Product Name: Phenylphosphonic dichloride
CAS No.: 824-72-6
Chemical Name: Phenylphosphonic dichloride
Synonyms: P,P-DICHLOROPHENYLPHOSPHINE OXIDE;BPOD;DICHLOROPHENYLPHOSPHINE OXIDE;PHENYLPHOSPHONYL DICHLORIDE;phenylphosphonic;Benzenephosphonyl chloride;AURORA KA-1395;phosphonic dichL;Phenylphosphonic dic;Phenylphosphorylchloride
CBNumber: CB5411511
Molecular Formula: C6H5Cl2OP
Formula Weight: 194.98
MOL File: 824-72-6.mol

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Phenylphosphonic dichloride Property

Melting point:: 3 °C(lit.)
Boiling point:: 258 °C(lit.)
Density: 1.375 g/mL at 25 °C(lit.)
vapor pressure: 2.36Pa at 25℃
refractive index: n20/D 1.559(lit.)
Flash point:: >230 °F
storage temp.: Store below +30°C.
solubility: Miscible with benzene, chloroform, dimethyl sulfoxide and carbon tetrachloride.
form: Liquid
color: Clear yellow to brown
Specific Gravity: 1.394 (25℃)
Water Solubility: reacts
Sensitive: Moisture Sensitive
λmax: 267nm(Cyclohexane)(lit.)
BRN: 1072240
Dielectric constant: 26.0
InChIKey: IBDMRHDXAQZJAP-UHFFFAOYSA-N
LogP: 1.089 at 20℃
CAS DataBase Reference: 824-72-6(CAS DataBase Reference)
NIST Chemistry Reference: Phosphonic dichloride, phenyl-(824-72-6)
EPA Substance Registry System: Phosphonic dichloride, P-phenyl- (824-72-6)

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Safety

Hazard Codes: C
Risk Statements: 14-34-37
Safety Statements: 26-45-8-36/37/39
RIDADR: UN 3265 8/PG 2
WGK Germany: 3
TSCA: Yes
HazardClass: 8
PackingGroup: II
HS Code: 29310095
Toxicity: LD50 orally in Rabbit: 681 mg/kg

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 389560
Product name: Phenylphosphonic dichloride
Purity: technical grade, 90%
Packaging: 100ml
Price: $86.3
Updated: 2024/03/01

Sigma-Aldrich

Product number: 8.18248
Product name: Dichlorophenylphosphine oxide
Purity: for synthesis
Packaging: 100mL
Price: $108
Updated: 2024/03/01

Sigma-Aldrich

Product number: 389560
Product name: Phenylphosphonic dichloride
Purity: technical grade, 90%
Packaging: 500ml
Price: $214.8
Updated: 2024/03/01

TCI Chemical

Product number: P0334
Product name: Phenylphosphonic Dichloride
Purity: >98.0%(T)
Packaging: 25mL
Price: $25
Updated: 2021/12/16

TCI Chemical

Product number: P0334
Product name: Phenylphosphonic Dichloride
Purity: >98.0%(T)
Packaging: 500mL
Price: $214
Updated: 2021/12/16

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Phenylphosphonic dichloride Chemical Properties,Usage,Production

Chemical Properties

Colorless to light yellow liqui

Uses

Phenylphosphonic dichloride is used in the preparation of 2-phenyl-[1,3,2]dioxaphosphepane-2-oxide. Further, it acts as an effective reagent for the chlorinative dehydration of some heterocycles.

Synthesis Reference(s)

Tetrahedron Letters, 33, p. 7473, 1992 DOI: 10.1016/S0040-4039(00)60798-0

Purification Methods

Fractionally distil it using a very efficient or a spinning band column. [Lecher et al. J Am Chem Soc 76 1045 1954, NMR: Müller et al. J Am Chem Soc 78 3557 1956, Van Wazer et al. J Am Chem Soc 78 5715 1956, IR: Daasch & Smith Anal Chem 23 853 1951, Beilstein 16 IV 1074.]

Phenylphosphonic dichloride Preparation Products And Raw materials

Raw materials

Preparation Products

4-BIPHENYLSULFONYL CHLORIDE DIMETHYL 4-CHLOROPYRIDINE-2,6-DICARBOXYLATE Methyl 6-methoxyformamido-4-chloropyridin-2-ylcarbamate ,97% 2,6-DIAMINO-4-CHLOROPYRIDINE 4-CHLOROPYRIDINE-2,6-DICARBOHYDRAZIDE 4-CHLORO-PYRIDINE-2,6-DICARBOXYLIC ACID 1,3-Dichloroisoquinoline Phenylphosphonic acid

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View Lastest Price from Phenylphosphonic dichloride manufacturers

Hebei Chuanghai Biotechnology Co,.LTD

Product: Phenylphosphonic Dichloride 824-72-6
Price: US $10.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 10 ton
Release date: 2024-08-20

Career Henan Chemical Co

Product: Phenylphosphonic dichloride 824-72-6
Price: US $1000.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2018-07-24

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organophosphorus compound

Ligand