ChemicalBook > CAS DataBase List > 2-HYDROXYMETHYL-1,3-DIOXOLANE

2-HYDROXYMETHYL-1,3-DIOXOLANE

Product Name
2-HYDROXYMETHYL-1,3-DIOXOLANE
CAS No.
5694-68-8
Chemical Name
2-HYDROXYMETHYL-1,3-DIOXOLANE
Synonyms
1,3-dioxane-2-methanol;1,3-Dioxolane-2-methanol;2-HYDROXYMETHYL-1,3-DIOXOLANE;2-HydroxyMethyl-1,3-dioxolaneC4H8O3
CBNumber
CB5439179
Molecular Formula
C4H8O3
Formula Weight
104.1
MOL File
5694-68-8.mol
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2-HYDROXYMETHYL-1,3-DIOXOLANE Property

Boiling point:
97 °C
Density 
1.164±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
14.83±0.10(Predicted)
form 
liquid
color 
Colourless to light yellow
InChI
InChI=1S/C4H8O3/c5-3-4-6-1-2-7-4/h4-5H,1-3H2
InChIKey
ZAGUSKAXELYWCE-UHFFFAOYSA-N
SMILES
O1CCOC1CO
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Safety

RIDADR 
UN1993
HS Code 
2909200090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC
Product number
D495680
Product name
(1,3-Dioxolan-2-yl)methanol
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
2093AL
Product name
2-Hydroxymethyl-1,3-dioxolane
Packaging
10g
Price
$512
Updated
2021/12/16
Chemenu
Product number
CM195866
Product name
(1,3-dioxolan-2-yl)methanol
Purity
95%
Packaging
10g
Price
$539
Updated
2021/12/16
Alichem
Product number
5694688
Product name
(1,3-Dioxolan-2-yl)methanol
Packaging
10g
Price
$564.48
Updated
2021/12/16
Ambeed
Product number
A220670
Product name
(1,3-Dioxolan-2-yl)methanol
Purity
95%
Packaging
25g
Price
$665
Updated
2021/12/16
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2-HYDROXYMETHYL-1,3-DIOXOLANE Chemical Properties,Usage,Production

Synthesis

71516-48-8

5694-68-8

General procedure for the synthesis of 1,3-dioxane-2-methanol from the compound (CAS: 71516-48-8): (66b) Preparation of 1,3-dioxan-2-ylmethanol: To a solution of 2-((benzyloxy)methyl)-1,3-dioxan-2-ylmethanol (3.01 g, 15.5 mmol) in methanol (100 mL), obtained in the previous step (66a), was Palladium hydroxide (20 wt% Pd (dry basis) carbon, wet (up to 50% water)) (300 mg) was added. The reaction mixture was stirred at room temperature for 15 hours under hydrogen atmosphere. Upon completion of the reaction, the gas in the reaction vessel was displaced with nitrogen, the catalyst was removed by filtration through diatomaceous earth and washed with methanol. The filtrate was concentrated and dried under reduced pressure to afford 1,3-dioxane-2-methanol (1.57 g, 97.3% yield) as a light yellow oil.1H NMR (400 MHz, CDCl3) δ ppm: 1.89 (1H, br s), 3.66-3.72 (2H, m), 3.88-4.08 (4H, m), 5.01 (1H, t, J = 3 Hz).

References

[1] Patent: US2007/10542, 2007, A1. Location in patent: Page/Page column 82

2-HYDROXYMETHYL-1,3-DIOXOLANE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-HYDROXYMETHYL-1,3-DIOXOLANE manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
2-HYDROXYMETHYL-1,3-DIOXOLANE 5694-68-8
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000KGS
Release date
2025-03-19

5694-68-8, 2-HYDROXYMETHYL-1,3-DIOXOLANERelated Search:

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  • 2-HYDROXYMETHYL-1,3-DIOXOLANE
  • 1,3-Dioxolane-2-methanol
  • 2-HydroxyMethyl-1,3-dioxolaneC4H8O3
  • 1,3-dioxane-2-methanol
  • 5694-68-8